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103041-38-9

Basic Information
CAS No.: 103041-38-9
Name: N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER
Article Data: 11
Molecular Structure:
Molecular Structure of 103041-38-9 (N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER)
Formula: C10H14N2O2
Molecular Weight: 194.233
Synonyms: b-Alanine, N-2-pyridyl-, ethylester (6CI);
EINECS: -0
Density: 1.132 g/cm3
Melting Point: 48-50°C
Boiling Point: 337.812 °C at 760 mmHg
Flash Point: 158.103 °C
Appearance: off-white crystals
PSA: 51.22000
LogP: 1.51970
Synthetic route
504-29-0

2-aminopyridine

140-88-5

ethyl acrylate

103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In ethanol at 120℃; for 12h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Green chemistry; chemoselective reaction;94%
With acetic acid In acetic acid at 88℃; Product distribution / selectivity;86.7%
In acetic acid at 88℃; Product distribution / selectivity;86.7%
64-17-5

ethanol

104961-64-0

3-[(pyridin-2-yl)amino]propanoic acid

103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

Conditions
ConditionsYield
With thionyl chloride at 0 - 70℃; for 12h;69.2%
504-29-0

2-aminopyridine

98-29-3

4-tert-Butylcatechol

140-88-5

ethyl acrylate

A

103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

B

5439-14-5

3,4-dihydro-pyrido[1,2-a]pyrimidin-2-one

504-29-0

2-aminopyridine

140-88-5

ethyl acrylate

A

103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

B

5439-14-5

3,4-dihydro-pyrido[1,2-a]pyrimidin-2-one

103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

2-(chloromethyl)-1-methyl-1H-benzimidazole-6-carboxylic acid

ethyl 3-(2-(chloromethyl)-1-methyl-N-(pyridin-2-yl)-1H-benzimidazole-6-carboxamido)propanate

Conditions
ConditionsYield
With triethylamine In ethyl acetate at -10℃; Reagent/catalyst; Temperature; Solvent;97.7%
103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

99548-53-5

3-Bromo-4-ethylbenzoic acid

C18H20BrN3O3

Conditions
ConditionsYield
Stage #1: 3-Bromo-4-ethylbenzoic acid With thionyl chloride In tetrahydrofuran; N,N-dimethyl-formamide at -20 - 20℃; for 5h;
Stage #2: 2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate With pyridine In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 6h; Solvent; Reagent/catalyst;
97%
103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

41263-74-5

4-(methylamino)-3-nitrobenzoic acid

1187067-68-0

ethyl 3-[[4-(methylamino)-3-nitrobenzoyl](pyridin-2-yl)amino]propanoate hydrochloride

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 18h; Solvent; Reagent/catalyst;95.2%
103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

38818-50-7

4-chloro-3-nitro-benzoyl chloride

1620205-04-0

3-[(4-chloro-3-nitrobenzoyl)pyridin-2-yl-amino]propionic acid ethyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Solvent; Reagent/catalyst;87%
With N-ethyl-N,N-diisopropylamine In dichloromethane at -5 - 0℃; for 1h;
With triethylamine In dichloromethane at 20℃; for 1h; Solvent; Reagent/catalyst;16.3 g
103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

4-methylamino-3-nitrobenzoyl chloride hydrochloride

ethyl 3-[((4-methylamino-3-nitrobenzoyl)pyridin-2-yl)amino]propanoate

Conditions
ConditionsYield
Stage #1: 2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate; 4-methylamino-3-nitrobenzoyl chloride hydrochloride With triethylamine In toluene at 0 - 30℃; for 3h; Large scale;
Stage #2: In ethanol; toluene at 20 - 70℃; Large scale;
87%
103041-38-9

2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate

C10H8Cl2N2O

1307233-94-8

N-[[2-(chloromethyl)-1-methyl-1H-benzimidazol-5-yl]carbonyl]-N-2-pyridyl-β-alanine ethyl ester

Conditions
ConditionsYield
In ethyl acetate at 20℃; for 1h;85%
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    Product Name: N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER Synonyms: N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER;N-2-pyridinyl-β-Alanine,ethylester;ethyl 3-(pyridin-2-ylamino)propanoate;N-Pyridin-2-yl-beta-alanine ethyl ester;ethyl (2S)-2-[(pyridin-2-

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    Product Name: N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER Synonyms: Ethyl-3-(pyridine-2-ylamino)propanoate;N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER;N-2-pyridinyl-β-Alanine,ethylester;ethyl 3-(pyridin-2-ylamino)propanoate;N-Pyridin-2-yl-beta-alanine ethyl es

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  • Ethyl 3-(pyridin-2-ylamino)propanoate

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    Ethyl 3-(pyridin-2-ylamino)propanoate

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  • CAS 103041-38-9  N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER

  • Casno:

    103041-38-9

    CAS 103041-38-9 N-[2]PYRIDYL-B-ALANIN-ETHYL ESTER

    Min.Order: 1 Kilogram

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  • ETHYL 3-(PYRIDIN-2-YLAMINO) PROPANOATE

  • Casno:

    103041-38-9

    ETHYL 3-(PYRIDIN-2-YLAMINO) PROPANOATE

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

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Chemistry

Product Name: Ethyl 3-(pyridin-2-ylamino)propanoate (CAS NO.103041-38-9)

Molecular Formula: C10H14N2O2
Molecular Weight: 194.23g/mol
Mol File: 103041-38-9.mol
Boiling point: 337.812 °C at 760 mmHg
Flash Point: 158.103 °C
Density: 1.132 g/cm3
Index of Refraction: 1.545 
Molar Refractivity: 54.26 cm3 
Molar Volume: 171.623 cm3 
Surface Tension: 44.869 dyne/cm
Enthalpy of Vaporization: 58.11 kJ/mol