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1032900-25-6

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Basic Information
CAS No.: 1032900-25-6
Name: Ceritinib (LDK378)
Article Data: 27
Molecular Structure:
Molecular Structure of 1032900-25-6 (Ceritinib (LDK378))
Formula: C28H36ClN5O3S
Molecular Weight: 558.145
Synonyms: Ceritinib; LDK 378; 5-chloro-n4-(2-((1-methylethyl)sulfonyl)phenyl)-n2-(5-methyl-2-(1-methylethoxy)-4-(4-piperidinyl)phenyl)-2,4-pyrimidinediamine
EINECS: 811-457-8
Density: 1.251±0.06 g/cm3(Predicted)
Boiling Point: 720.7±70.0 °C(Predicted)
PSA: 116.85000
LogP: 7.26640
Related products
Synthetic route

C35H40ClN5O3S

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen at 35℃; under 7500.75 Torr;97.9%
1032903-64-2

4-(4-{5-chloro-4-[2-(propane-2-sulfonyl)phenylamino]pyrimidin-2-ylamino}-5-isopropoxy-2-methylphenyl)piperidine-1-carboxylic acid tert-butyl ester

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
With hydrogenchloride In ethyl acetate at 20℃; for 2h;97%
With trifluoroacetic acid In tetrahydrofuran at 0 - 22℃; for 5h; Temperature;90.1%
With trifluoroacetic acid at 20℃; for 1h;39%
With trifluoroacetic acid In dichloromethane
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
2: sodium hydrogencarbonate / water; ethyl acetate
View Scheme

5-chloro-N2-(2-isopropoxy-5-methyl-4-(piperidin-4-yl)phenyl)-N4-(2-(propane-2-sulfonyl)phenyl)pyrimidine-2,4-diamine dihydrochloride

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
With sodium hydroxide In water at 0 - 5℃; pH=8;96%
With sodium hydroxide In ethanol; water; isopropyl alcohol at 55℃; Large scale;93%
With sodium hydroxide In ethanol; water at 20 - 50℃; for 2h; Temperature; Inert atmosphere;90%
761440-16-8

2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-4-pyrimidinamine

5-chloro-N2-[2-isopropoxy-5-methyl-4-(piperidin-4-yl)phenyl]-N4-[2-(isopropylsulfonyl)phenyl]pyrimidine-2,4-diamine dihydrochloride

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Stage #1: 2-chloro-N-(2-(isopropylsulfonyl)phenyl)-5-methyl-pyrimidin-4-amine; 5-chloro-N2-[2-isopropoxy-5-methyl-4-(piperidin-4-yl)phenyl]-N4-[2-(isopropylsulfonyl)phenyl]pyrimidine-2,4-diamine dihydrochloride In isopropyl alcohol for 16h; Reflux; Large scale;
Stage #2: With sodium hydroxide In ethanol; water; isopropyl alcohol at 55℃; Large scale;		93%
In ethanol; water; isopropyl alcohol for 16h; Reflux; Large scale;93%
In 1,2-dimethoxyethane for 5h; Inert atmosphere; Reflux;74%
70398-95-7

2-isopropylsulfonylchlorobenzene

C24H34ClN5O3

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Stage #1: 2-isopropylsulfonylchlorobenzene; C24H34ClN5O3 With tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate In toluene at 85 - 90℃; for 2h;
Stage #2: With hydrogenchloride In ethanol; water at 45℃; for 1h;		92.6%

C36H42ClN5O5S

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
With trifluoroacetic acid In tetrahydrofuran at 8 - 30℃; for 5h; Temperature;91.3%
900174-43-8

1-bromo-2-(isopropylsulfonyl)benzene

C24H34ClN5O3

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Stage #1: 1-bromo-2-(isopropylsulfonyl)benzene; C24H34ClN5O3 With palladium diacetate; caesium carbonate; triphenylphosphine In tetrahydrofuran at 65 - 70℃; for 8h;
Stage #2: With trifluoroacetic acid In dichloromethane at 25 - 30℃; for 3h;		90.2%
761440-16-8

2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-4-pyrimidinamine

1035230-24-0

5-chloro-N2-(2-isopropoxy-5-methyl-4-(piperidin-4-yl)phenyl)-N4-((2-isopropylsulfonyl)phenyl)pyrimidine-2,4-diamine

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Stage #1: 5-chloro-N2-(2-isopropoxy-5-methyl-4-(piperidin-4-yl)phenyl)-N4-((2-isopropylsulfonyl)phenyl)pyrimidine-2,4-diamine With hydrogenchloride In water; isopropyl alcohol at 25 - 30℃; for 1.5h; Buchwald-Hartwig Coupling;
Stage #2: 2-chloro-N-(2-(isopropylsulfonyl)phenyl)-5-methyl-pyrimidin-4-amine In water; isopropyl alcohol for 44h; Reflux;		75.4%
With N-ethyl-N,N-diisopropylamine at 80℃; Inert atmosphere;2.5 g
With toluene-4-sulfonic acid In isopropyl alcohol at 85℃;
761440-16-8

2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-4-pyrimidinamine

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium diacetate; XPhos; caesium carbonate / tetrahydrofuran
2: trifluoroacetic acid / dichloromethane
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; isopropyl alcohol / 75 - 77 °C / Large scale
2: sodium hydroxide / acetone; water / 20 - 55 °C / pH 12.0
View Scheme
Multi-step reaction with 3 steps
1: bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate / toluene / 0.33 h / 150 °C / Microwave irradiation
2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3: sodium hydrogencarbonate / water; ethyl acetate
View Scheme
1032903-63-1

4-(4-amino-5-isopropoxy-2-methylphenyl)-piperidine-1-carboxylic acid tert-butyl ester

1032900-25-6

5-chloro-N2-{5-methyl-4-(piperidin-4-yl)-2-[(propan-2-yl)oxy]phenyl}-N4-[2-(propane-2-sulfonyl)phenyl]pyrimidine-2,4-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium diacetate; XPhos; caesium carbonate / tetrahydrofuran
2: trifluoroacetic acid / dichloromethane
View Scheme
Multi-step reaction with 3 steps
1: bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate / toluene / 0.33 h / 150 °C / Microwave irradiation
2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3: sodium hydrogencarbonate / water; ethyl acetate
View Scheme
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C
2.1: isopropyl alcohol / 16 h / Reflux; Large scale
2.2: 55 °C / Large scale
View Scheme
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    Shanghai Upbio Tech Co.,Ltd (Former Onchem (China)Co.,Ltd) is a comprehensive manufacturer and an international distribution of chemicals throughout the world, The predecessor of

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+8619003195089

    Address:Haida Business Center, Xiangdu District

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    Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

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    Business Type:Lab/Research institutions

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:Room 401, Floor 4, Building 3-1, Guandong Science and Technology Industrial Park, Jiayuan Road, Guandong Street, Donghu Hi tech Development Zone, Wuhan

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    Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Address:Economic Developed Zone of Taizhou Zhejiang China

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    Ceritinib

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85378921

    Address:Jintong international Building, No.113,Huayuangang Street, Gong shu District, Hangzhou,Zhejiang, China.

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    A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

    T&W GROUP was established in 2007, headquartered in Shanghai, China. By integrating people, technology and potential, we endeavor to work for a better life. We are in the business

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-61551611

    Address:601, No. 1, 2277 Nong, Zu Chongzhi Road, Zhangjiang Hightech. Park, Pudong

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    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    low price high quality high purity good sevice stock Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Active Pharmaceutical Ingr

    Shanghai Send Pharmaceutical Technology Co., Ltd(Send Pharm) is a high-tech company specializing in R&D and manufacturing of APIs and pharmaceutical intermediates, and also provi

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-50266790 +8613585868794

    Address:No.3399 Kangxin Road Pudong District Shanghai,China

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    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

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    Product name: Ceritinib CAS No.: 1032900-25-6 Molecule Formula：C28H36ClN5O3S Molecule Weight：No Purity: 99.0% Package: 25kg/drum Description：White crystalline powder Manufacture Standards：Enterprise Standard TESTI

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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