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103343-47-1

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Basic Information
CAS No.: 103343-47-1
Name: 3-AMINO-5-PHENYL-1,3-DIHYDRO-2H-1,4-BENZODIAZEPIN-2-ONE
Article Data: 16
Molecular Structure:
Molecular Structure of 103343-47-1 (3-AMINO-5-PHENYL-1,3-DIHYDRO-2H-1,4-BENZODIAZEPIN-2-ONE)
Formula: C15H13 N3 O
Molecular Weight: 251.288
Synonyms: 2H-1,4-Benzodiazepin-2-one,3-amino-1,3-dihydro-5-phenyl-, (?à)-; 3-Amino-5-phenyl-1,3-dihydro-1,4-benzodiazepin-2-one;3-Amino-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one;3-Amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one
Density: 1.3g/cm3
Boiling Point: 456.7°Cat760mmHg
Flash Point: 230°C
PSA: 67.48000
LogP: 2.03480
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Synthetic route
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103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
With hydrogen bromide In acetic acid 1.) 70 deg C, 20 min, 2.) 80 deg C, 20 min;88%
With hydrogen bromide; acetic acid at 70℃; for 0.5h;33%
With sodium hydroxide; palladium on activated charcoal 1. HCO2H(95percent)-CH3OH(5:95 v/v), 45 gradC, 3h; 2. CH2Cl2; Yield given. Multistep reaction;

5-phenyl-1H-benzo[e][1,4]diazepine-2,3-dione 3-oxime

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
With hydrogen; Ru-carbon In methanol under 3000.24 Torr; Reduction;
161365-74-8

benzyl N-[[(2-benzoylphenyl)carbamoyl](1H-1,2,3-benzotriazol-1-yl)methyl]carbamate

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: NH3 / methanol; tetrahydrofuran / 18 h
1.2: 6.94 g / NH4OAc; AcOH / 18 h / 20 °C
2.1: 33 percent / HBr; AcOH / 0.5 h / 70 °C
View Scheme
Multi-step reaction with 3 steps
1: NH3 / tetrahydrofuran; CH2Cl2; methanol / 0.5 h
2: NH4OAc / acetic acid / Ambient temperature
3: 88 percent / HBr / acetic acid / 1.) 70 deg C, 20 min, 2.) 80 deg C, 20 min
View Scheme
Multi-step reaction with 4 steps
1: ammonia / methanol / 3 h / 20 °C
2: acetic acid; ammonium acetate / 16 h / 20 °C
3: acetic acid; hydrogen bromide / 0.5 h / 70 °C
4: ammonium hydroxide / water / pH 14 / Cooling with ice
View Scheme
Multi-step reaction with 4 steps
1: ammonia / methanol / 3 h / 20 °C
2: acetic acid; ammonium acetate / methanol / 16 h / 20 °C
3: acetic acid; hydrogen bromide / 0.5 h / 70 °C
4: ammonium hydroxide / water / pH 14 / Cooling with ice
View Scheme
108895-97-2

2-

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 7.0 g / NH4OAc; AcOH / 12 h / 20 °C
2: Pd(OAc)2; TEA; triethylsilane / CH2Cl2 / 3 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: NH4OAc / acetic acid / Ambient temperature
2: 88 percent / HBr / acetic acid / 1.) 70 deg C, 20 min, 2.) 80 deg C, 20 min
View Scheme
Multi-step reaction with 2 steps
1: CH3COONH4 / acetic acid / 2.5 h / 55 °C
2: 90percent aq. formic acid / 10percent Pd on C / methanol / 3 h / 40 - 50 °C
View Scheme
2835-77-0

(2-aminophenyl)(phenyl)methanone

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: isobutyl chloroformate; N-methylmorpholine / CH2Cl2 / 0.5 h / Heating
1.2: 86 percent / CH2Cl2 / 0.5 h / Heating
2.1: NH3(gas); mercuric chloride / tetrahydrofuran / 3 h / 0 - 20 °C
3.1: 7.0 g / NH4OAc; AcOH / 12 h / 20 °C
4.1: Pd(OAc)2; TEA; triethylsilane / CH2Cl2 / 3 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: pyridine
2: t-BuOK; iAmONO / tetrahydrofuran
3: H2 / Ru/C / methanol / 3000.24 Torr
View Scheme
Multi-step reaction with 4 steps
1: 1) N-methylmorpholine, isobutyl chloroformate / 1) CH2Cl2, 0 deg C, 15 min; 2) CH2Cl2, reflux, 20 min
2: NH3, HgCl2 / tetrahydrofuran / 3 h
3: CH3COONH4 / acetic acid / 2.5 h / 55 °C
4: 90percent aq. formic acid / 10percent Pd on C / methanol / 3 h / 40 - 50 °C
View Scheme
821800-04-8

[(2-benzoyl-phenylcarbamoyl)propylsulfanylmethyl]carbamic acid benzyl ester

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NH3(gas); mercuric chloride / tetrahydrofuran / 3 h / 0 - 20 °C
2: 7.0 g / NH4OAc; AcOH / 12 h / 20 °C
3: Pd(OAc)2; TEA; triethylsilane / CH2Cl2 / 3 h / 20 °C
View Scheme
100-47-0

benzonitrile

Cp2Zr(isoprene) (1)

Cp2Zr(isoprene) (1)

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: BCl3; AlCl3 / 1,2-dichloro-ethane
2: pyridine
3: t-BuOK; iAmONO / tetrahydrofuran
4: H2 / Ru/C / methanol / 3000.24 Torr
View Scheme
62-53-3

aniline

Wang resin-bound styrene 4

Wang resin-bound styrene 4

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: BCl3; AlCl3 / 1,2-dichloro-ethane
2: pyridine
3: t-BuOK; iAmONO / tetrahydrofuran
4: H2 / Ru/C / methanol / 3000.24 Torr
View Scheme
2898-08-0

2,3-dihydro-5-phenyl-1H-1,4-benzodiazepin-2-one

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: t-BuOK; iAmONO / tetrahydrofuran
2: H2 / Ru/C / methanol / 3000.24 Torr
View Scheme
106849-44-9

2-

103343-47-1

3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NH3, HgCl2 / tetrahydrofuran / 3 h
2: CH3COONH4 / acetic acid / 2.5 h / 55 °C
3: 90percent aq. formic acid / 10percent Pd on C / methanol / 3 h / 40 - 50 °C
View Scheme
Multi-step reaction with 3 steps
1: 100 percent / NH3 (g), HgCl2 / tetrahydrofuran / 3 h / 0 - 23 °C
2: 75 percent / NH4OAc / acetic acid / 12 h / 23 °C
3: 2. NaOH (40percent) / 10percent Pd/C / 1. HCO2H(95percent)-CH3OH(5:95 v/v), 45 gradC, 3h; 2. CH2Cl2
View Scheme
Multi-step reaction with 3 steps
1: 100 percent / NH3 (g), HgCl2 / tetrahydrofuran / 3 h / 0 - 23 °C
2: under neutral or basic cyclization conditions
3: 2. NaOH (40percent) / 10percent Pd/C / 1. HCO2H(95percent)-CH3OH(5:95 v/v), 45 gradC, 3h; 2. CH2Cl2
View Scheme
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    High Quality Best Price Storage:Store in dry, dark and ventilated place Application:Chemical Synthesis Intermediate

    Finetech Industry Limited is a company in England,which specializing in developing, manufacturing and marketing fine organic compounds and intermediates for the fine chemical and p

  • Finetech Industry Limited

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-27-87465837

    Address:wuhan

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  • 3-amino-1,3-dihydro-5-phenyl-2H-1,4-Benzodiazepin-2-one

  • Casno:

    103343-47-1

    3-amino-1,3-dihydro-5-phenyl-2H-1,4-Benzodiazepin-2-one

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four years Our key scienti

  • Debye Scientific

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+85221376140

    Address:Rm. 19C, Lockhart Ctr., 301-307 Lockhart Rd., Wan Chai

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  • 3-amino-5-phenyl-1,3-dihydro-1,4-benzodiazepin-2-one

  • Casno:

    103343-47-1

    3-amino-5-phenyl-1,3-dihydro-1,4-benzodiazepin-2-one

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    high purity Application:Drug intermediates Materials intermediates and active molecules

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

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