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103946-54-9

Basic Information
CAS No.: 103946-54-9
Name: 4'-METHYL-2,2'-BIPYRIDINE-4-CARBOXYLIC ACID
Article Data: 34
Molecular Structure:
Molecular Structure of 103946-54-9 (4'-METHYL-2,2'-BIPYRIDINE-4-CARBOXYLIC ACID)
Formula: C12H10N2O2
Molecular Weight: 214.224
Synonyms: 4-Carboxy-4'-methyl-2,2'-bipyridine;4-Methyl-2,2'-bipyridine-4'-carboxylic acid;
EINECS: 145-896-5
Density: 1.26 g/cm3
Melting Point: 280 °C
Boiling Point: 497.4 °C at 760 mmHg
Flash Point: 254.6 °C
PSA: 63.08000
LogP: 2.15020
Synthetic route
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With selenium(IV) oxide; sulfuric acid98%
Stage #1: 4,4'-dimethyl-2,2'-bipyridines With selenium(IV) oxide In 1,4-dioxane for 30h; Reflux;
Stage #2: With silver nitrate; sodium hydroxide In ethanol; water for 24h;
77%
Stage #1: 4,4'-dimethyl-2,2'-bipyridines With selenium(IV) oxide In 1,4-dioxane for 16h; Oxidation; Heating;
Stage #2: With silver(l) oxide Oxidation;
72%
104704-09-8

4'-methyl-2,2'-bipyridine-4-carboxylaldehyde

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With silver nitrate; sodium hydroxide In ethanol for 24h; Darkness;82%
With silver nitrate; sodium hydroxide In ethanol; water at 20℃;80%
Stage #1: 4'-methyl-2,2'-bipyridine-4-carboxylaldehyde With silver nitrate In ethanol for 0.333333h;
Stage #2: With sodium hydroxide In ethanol at 25℃; for 15h; Darkness;
80%
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

A

6813-38-3

2,2'-Bipyridine-4,4'-dicarboxylic acid

B

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With potassium permanganate; sulfuric acid for 12h; Heating;A 45%
B 4%
With manganese(II) sulfate; potassium permanganate In pyridine; water for 120h; Ambient temperature;A n/a
B 7%
With sodium hydroxide; selenium(IV) oxide; silver nitrate 1.) 1,4-dioxane, reflux, 24 h, 2.) EtOH, water, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
With chromium(VI) oxide; periodic acid In dichloromethane; acetonitrile at 20℃; for 16h; Overall yield = 0.099 g;A 35 %Spectr.
B 6 %Spectr.
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

A

104704-09-8

4'-methyl-2,2'-bipyridine-4-carboxylaldehyde

B

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With selenium(IV) oxide In 1,4-dioxane for 72h;A 29%
B n/a
108-89-4

picoline

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: manganese(IV) oxide; palladium on activated charcoal / neat (no solvent) / 168 h / 140 °C
2.1: selenium(IV) oxide / 1,4-dioxane / 24 h / Reflux
2.2: 20 °C
View Scheme
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With selenium(IV) oxide; sulfuric acid98%
Stage #1: 4,4'-dimethyl-2,2'-bipyridines With selenium(IV) oxide In 1,4-dioxane for 30h; Reflux;
Stage #2: With silver nitrate; sodium hydroxide In ethanol; water for 24h;
77%
Stage #1: 4,4'-dimethyl-2,2'-bipyridines With selenium(IV) oxide In 1,4-dioxane for 16h; Oxidation; Heating;
Stage #2: With silver(l) oxide Oxidation;
72%
104704-09-8

4'-methyl-2,2'-bipyridine-4-carboxylaldehyde

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With silver nitrate; sodium hydroxide In ethanol for 24h; Darkness;82%
With silver nitrate; sodium hydroxide In ethanol; water at 20℃;80%
Stage #1: 4'-methyl-2,2'-bipyridine-4-carboxylaldehyde With silver nitrate In ethanol for 0.333333h;
Stage #2: With sodium hydroxide In ethanol at 25℃; for 15h; Darkness;
80%
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

A

6813-38-3

2,2'-Bipyridine-4,4'-dicarboxylic acid

B

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With potassium permanganate; sulfuric acid for 12h; Heating;A 45%
B 4%
With manganese(II) sulfate; potassium permanganate In pyridine; water for 120h; Ambient temperature;A n/a
B 7%
With sodium hydroxide; selenium(IV) oxide; silver nitrate 1.) 1,4-dioxane, reflux, 24 h, 2.) EtOH, water, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
With chromium(VI) oxide; periodic acid In dichloromethane; acetonitrile at 20℃; for 16h; Overall yield = 0.099 g;A 35 %Spectr.
B 6 %Spectr.
1134-35-6

4,4'-dimethyl-2,2'-bipyridines

A

104704-09-8

4'-methyl-2,2'-bipyridine-4-carboxylaldehyde

B

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
With selenium(IV) oxide In 1,4-dioxane for 72h;A 29%
B n/a
108-89-4

picoline

103946-54-9

4'-methyl-2,2'-bipyridine-4-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: manganese(IV) oxide; palladium on activated charcoal / neat (no solvent) / 168 h / 140 °C
2.1: selenium(IV) oxide / 1,4-dioxane / 24 h / Reflux
2.2: 20 °C
View Scheme
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Chemistry

Molecular Formula: C12H10N2O2
Molecular Weight: 214.22 g/mol
Index of Refraction: 1.608
Density: 1.26 g/cm3
Flash Point: 254.6 °C
Enthalpy of Vaporization: 80.61 kJ/mol
Boiling Point: 497.4 °C at 760 mmHg
Vapour Pressure: 1.03E-10 mmHg at 25 °C
Structure of 4'-Methyl-2,2'-bipyridine-4-carboxylic acid (CAS NO.103946-54-9):
                       
Product Category of 4'-Methyl-2,2'-bipyridine-4-carboxylic acid (CAS NO.103946-54-9): API intermediates

Specification

 4'-Methyl-2,2'-bipyridine-4-carboxylic acid (CAS NO.103946-54-9) also can be called [2,2'-bipyridine]-4-carboxylic acid, 4'-methyl- .