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10436-39-2

Basic Information
CAS No.: 10436-39-2
Name: Tetrachloropropene
Article Data: 33
Molecular Structure:
Molecular Structure of 10436-39-2 (Tetrachloropropene)
Formula: C3H2 Cl4
Molecular Weight: 179.861
Synonyms: Propene,1,1,2,3-tetrachloro- (6CI,7CI,8CI); 1,1,2,3-Tetrachloro-1-propene;1,1,2,3-Tetrachloropropene; 2,3,3-Trichloroallyl chloride; HCO 1230; HCO 1230xa
Density: 1.539g/cm3
Melting Point: 29-31°C(lit.)
Boiling Point: 173.8°Cat760mmHg
Flash Point: 62.3°C
Solubility: MISCIBLE
Appearance: clear colorless to yellowish liquid after melting
Hazard Symbols: Xi,C
Risk Codes: R37/38; R41; R36/37/38; R34
Safety: Poison by ingestion and skin contact. Moderately toxic by inhalation. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl. See also CHLORINATED HYDROCARBONS, ALIPHATIC.
PSA: 0.00000
LogP: 3.11070
Synthetic route
16714-68-4

1,1,2,2,3-pentachloropropane

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
With sodium hydroxide; cetylpyridinium bromide at 130℃; for 2h;97%
With potassium hydroxide
With sodium hydroxide
24425-97-6

1,1,1,2,2,3-hexachloropropane

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
With hydrogenchloride; zinc In 1,4-dioxane; water at 45℃; for 49h; Autoclave; Inert atmosphere;90%
1070-78-6

1,1,1,3-tetrachloropropane

A

21700-31-2

1,1,1,2,3-pentachloro-propane

B

2567-14-8

3,3-dichloroallyl chloride

C

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
With iron(III) chloride; chlorine at 82℃; under 1277.21 Torr; for 15.33h; Product distribution / selectivity;A 82.9%
B 3.4%
C 8.1%
21700-31-2

1,1,1,2,3-pentachloro-propane

A

10436-39-2

1,1,2,3-Tetrachloropropene

B

16500-91-7

2,3,3,3-tetrachloropropene

Conditions
ConditionsYield
With potassium hydroxide at 0℃;
With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h;
With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h;
With potassium hydroxide; Aliquat 336 In water at 8℃; for 3h;
16500-91-7

2,3,3,3-tetrachloropropene

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
at 180℃;
With aluminium trichloride at 0℃;
With antimonypentachloride
at 150 - 180℃;
67-56-1

methanol

3266-39-5

2,3,3-trichloro-2-propen-1-ol

A

80-63-7

methyl 2-chloroacrylate

B

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
With sulfuric acid; water 1) 105 deg C, 4 h, 2) 30 min; Yield given. Multistep reaction. Yields of byproduct given;
21700-31-2

1,1,1,2,3-pentachloro-propane

A

2233-00-3

3,3,3-trichloro-1-propene

B

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
at 400℃; under 750.075 Torr; for 0.0130556h; Inert atmosphere;
21700-31-2

1,1,1,2,3-pentachloro-propane

A

2252-87-1

2,3-dichloro-3,3-difluoroprop-1-ene

B

10436-39-2

1,1,2,3-Tetrachloropropene

C

666-27-3

1,1,2,3-tetrachloro-1-fluoro-propane

Conditions
ConditionsYield
With hydrogen fluoride at 290℃; under 750.075 Torr; for 3h; Inert atmosphere; tubular reactor;
74-99-7

prop-1-yne

A

10436-39-2

1,1,2,3-Tetrachloropropene

B

16500-91-7

2,3,3,3-tetrachloropropene

Conditions
ConditionsYield
Stage #1: prop-1-yne With chlorine at 60 - 80℃;
Stage #2: With chlorine; dibenzoyl peroxide at 40 - 50℃;
Stage #3: With sodium hydroxide at 40 - 50℃;
67-66-3

chloroform

75-35-4

1,1-Dichloroethylene

10436-39-2

1,1,2,3-Tetrachloropropene

Conditions
ConditionsYield
at 100 - 450℃; under 1018.63 Torr; Temperature; Reagent/catalyst; Pressure; Inert atmosphere;8.1 %Spectr.
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Chemistry

IUPAC Name: 1,1,2,3-Tetrachloroprop-1-ene
The MF of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is C3H2Cl4.

                                    
The MW of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is 179.86.
Synonyms of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2): Tetrachloropropene ; 1,1,2,3-Tetrachloropropene ; 1,1,2,3-Tetrachloro-1-propene ; 1,1,2,3-Tetrachloro-propen ; 2,3,3-Trichloroallyl chloride
Apperance: Colorless oily liquid
Index of Refraction: 1.512 
EINECS: 233-920-8
Density: 1.539 g/ml 
Flash Point: 62.3 °C
Boiling Point: 173.8 °C

Uses

  1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is Ye Yan fear herbicide intermediate and used for the synthesis of heat-resistant plastic.

Production

A dehydrochlorination: tirring 1,1,2,3 - Tetrachloro-propane,calcium hydroxide and a certain amount of water in the reactors, to a certain reaction temperature for several hours, add 1:1 hydrochloric acid and in to acidic deposition layered collection of mixed-bit three allyl chloride.
Secondary chloride: reaction equipment is the same chlorination, mixed with bits into three allyl chloride, were mixed with bits 5-chloropropane.
Second dehydrochlorination: Production equipment is the same dehydrochlorination in the reaction vessel into position five chlorine mixed with propane, adding calcium hydroxide, dehydrochlorination was four allyl chloride.
                         ClCH=CHCH2Cl+Cl2→ClCH2CHClCHCl2
                         ClCH2CHClCHCl2+OH-→ClCH2ClG=CHCl
                         ClCH2ClC=CHCl+Cl2→Cl2CHCCl2CH2Cl
                         Cl2CHCCl2CH2Cl+OH-→Cl2C=CClCH2Cl

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LC50 inhalation 3200mg/m3 (3200mg/m3)   Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979.
mouse LD50 oral 800mg/kg (800mg/kg) LIVER: OTHER CHANGES Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 43(4), Pg. 15, 1978.
rabbit LD50 oral 477mg/kg (477mg/kg)   Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979.
rabbit LD50 skin 400uL/kg (0.4mL/kg)   American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969.
rat LC50 inhalation 1500mg/m3 (1500mg/m3)   Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979.
rat LD50 oral 350mg/kg (350mg/kg)   American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by ingestion and skin contact. Moderately toxic by inhalation. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl. See also CHLORINATED HYDROCARBONS, ALIPHATIC.