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105-74-8

Basic Information
CAS No.: 105-74-8
Name: Dilauroyl peroxide
Article Data: 14
Molecular Structure:
Molecular Structure of 105-74-8 (Dilauroyl peroxide)
Formula: C24H46O4
Molecular Weight: 398.627
Synonyms: Lauroylperoxide (8CI);Alperox C;Alperox F;Bis(1-oxododecyl) peroxide;Didodecanoylperoxide;Dodecanoyl peroxide;LYP 97;LYP 97F;Laurox W 40;Laurox W 40GD4;Laurydol;Lup LP;NSC 670;Peroyl L;
EINECS: 203-326-3
Density: 0.923 g/cm3
Melting Point: 53-57 °C(lit.)
Boiling Point: 467.3 °C at 760 mmHg
Flash Point: 194.9 °C
Solubility: Soluble in oils and organic solvents. Slightly soluble in alcohol. Insoluble in water.
Appearance: white powder
Hazard Symbols: OxidizingO
Risk Codes: 7
Safety: 14-3/7-36/37/39-14A-37/39-36
Transport Information: UN 3106 5.2
PSA: 52.60000
LogP: 7.82960
Synthetic route
112-16-3

n-dodecanoyl chloride

105-74-8

dilauryl peroxide

Conditions
ConditionsYield
With dihydrogen peroxide; sodium hydroxide In 2-Methylpentane; water at 16 - 18℃; for 0.666667h;99.1%
With tetrahydrofuran; sodium peroxide
With pyridine; diethyl ether; water; dihydrogen peroxide
1120-16-7

lauric acid amide

105-74-8

dilauryl peroxide

Conditions
ConditionsYield
Stage #1: lauric acid amide With benzyl methyl ether; zinc(II) chromate; 3-methylpentane In water at 26℃; for 2h;
Stage #2: With lead(IV) tetraacetate; sodium sulfate In water at 55℃; for 3h; Temperature; Time;
98.6%
112-16-3

n-dodecanoyl chloride

2388-12-7

peroxylaurinoic acid

105-74-8

dilauryl peroxide

143-07-7

lauric acid

undecanol-5, undecanol-6

undecanol-5, undecanol-6

105-74-8

dilauryl peroxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: SOCl2 / Heating
2: H2O2, pyridine / diethyl ether; H2O / 1 h
View Scheme
143-07-7

lauric acid

105-74-8

dilauryl peroxide

Conditions
ConditionsYield
Stage #1: lauric acid With dmap; dihydrogen peroxide In dichloromethane at -15℃; for 0.166667h; Inert atmosphere;
Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at -15 - 10℃; for 1.5h; Inert atmosphere;
With dmap; dihydrogen peroxide; dicyclohexyl-carbodiimide In dichloromethane at -15℃; for 1.5h;
Stage #1: lauric acid With dmap; dihydrogen peroxide In dichloromethane at -15℃; for 0.166667h;
Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at -15 - -10℃;
470-17-7

isoalantolactone

105-74-8

dilauryl peroxide

C26H43N3O2

Conditions
ConditionsYield
With iron(II) triflate; trimethylsilylazide In 1,2-dimethoxyethane at 35℃; for 2h; Inert atmosphere; Schlenk technique;99%
105-74-8

dilauryl peroxide

93765-84-5

2,4-dibromo-5-fluorotoluene

1,5-dichloro-2-fluoro-4-(trichloromethyl)benzene

Conditions
ConditionsYield
In chlorine97.6%
105-74-8

dilauryl peroxide

536-74-3

phenylacetylene

4-phenyl-1-undecyl-1H-1,2,3-triazole

Conditions
ConditionsYield
With trimethylsilylazide; copper(l) chloride In dichloromethane at 50℃; for 10h; Catalytic behavior; Solvent; Reagent/catalyst; Schlenk technique; regioselective reaction;97%
105-74-8

dilauryl peroxide

1746-23-2

4-tert-Butylstyrene

C23H38

Conditions
ConditionsYield
With iron(III) trifluoromethanesulfonate In tetrahydrofuran at 90℃; for 3h; Schlenk technique; Inert atmosphere; diastereoselective reaction;96%
271-44-3

benzimidazole

105-74-8

dilauryl peroxide

1-undecyl-1H-indazole

Conditions
ConditionsYield
With 1,10-Phenanthroline; copper(I) bromide In 1,4-dioxane at 60℃; for 18h; Reagent/catalyst; Temperature; Inert atmosphere; Schlenk technique;96%
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Chemistry


IUPAC Name: Dodecanoyl dodecaneperoxoate
Canonical SMILES: CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC
InChI: InChI=1S/C24H46O4/c1-3-5-7-9-11-13-15-17-19-21-23(25)27-28-24(26)22-20-18-16-14-12-10-8-6-4-2/h3-22H2,1-2H3
Empirical Formula: C24H46O4
Molecular Weight: 398.6196
EINECS: 203-326-3
Classification Code: Skin / Eye Irritant; Tumor data
Melting Point: 53-57 °C(lit.)
storage temp.: Refrigerator (+4 °C)
Index of Refraction: 1.453
Molar Refractivity: 116.78 cm3
Molar Volume: 431.6 cm3
Surface Tension: 33.2 dyne/cm
Density: 0.923 g/cm3
Flash Point: 194.9 °C
Enthalpy of Vaporization: 72.93 kJ/mol
Boiling Point: 467.3 °C at 760 mmHg
Vapour Pressure of Lauroyl peroxide (CAS NO.105-74-8): 6.56E-09 mmHg at 25 °C

Uses

  Lauroyl peroxide (CAS NO.105-74-8) is used as initiator used for high-pressure polyethylene and food used in bleaching agent.

Toxicity Data With Reference

1.    

eye-rbt 500 mg/24H MLD

    28ZPAK    Sbornik Vysledku Toxixologickeho Vysetreni Latek A Pripravku Marhold, J.V.,Institut Pro Vychovu Vedoucicn Pracovniku Chemickeho Prumyclu Praha,Czechoslovakia.: 1972,53.

Consensus Reports

IARC Cancer Review: Group 3 IMEMDT    IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man . 7 , 1987,p. 56.(World Health Organization, Internation Agency for Research on Cancer,Lyon, France.: ) (Single copies can be ordered from WHO Publications Centre U.S.A., 49 Sheridan Avenue, Albany, NY 12210) ; Animal Inadequate Evidence IMEMDT    IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man . 36 , 1985,p. 315.(World Health Organization, Internation Agency for Research on Cancer,Lyon, France.: ) (Single copies can be ordered from WHO Publications Centre U.S.A., 49 Sheridan Avenue, Albany, NY 12210) . Reported in EPA TSCA Inventory.

Safety Profile

Questionable carcinogen with experimental tumorigenic data. A powerful oxidizing agent. It is a corrosive irritant to the eyes and mucous membranes and can cause burns. A dangerous fire hazard. When heated to decomposition it emits acrid smoke and fumes.
Hazard Codes: OxidizingO
Risk Statements: 7
R7: May cause fire
Safety Statements: 14-3/7-36/37/39
S14: Keep away from ... (incompatible materials to be indicated by the manufacturer)
S3/7: Keep container tightly closed in a cool place
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection 
RIDADR: UN 3106 5.2
WGK Germany: 1
RTECS: OF2625000
HazardClass: 5.2
PackingGroup: II

Standards and Recommendations

DFG MAK: Mild skin effects

Specification

  Lauroyl peroxide (CAS NO.105-74-8), its Synonyms are Dilauroyl peroxide ; Dilauryl peroxide ; Dodecanoyl peroxide ; Dyp-97F ; Laurydol ; Peroxide, bis(1-oxododecyl)- ; Peroxide, didodecanoyl ; Peroxyde de lauroyle . It is white solid with a faint soapy odor.