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1064662-40-3

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Basic Information
CAS No.: 1064662-40-3
Name: Imidazo[1,2-a]pyridine-6-carboxamide, 2-(4-cyanophenyl)-N,N-bis(3-methylbutyl)-3-[3-(1-pyrrolidinyl)propyl]-, hydrochloride (1:1)
Article Data: 1
Molecular Structure:
Molecular Structure of 1064662-40-3 (Imidazo[1,2-a]pyridine-6-carboxamide, 2-(4-cyanophenyl)-N,N-bis(3-methylbutyl)-3-[3-(1-pyrrolidinyl)propyl]-, hydrochloride (1:1))
Formula: C32H43N5O.ClH
Molecular Weight: 550.187
PSA: 64.64000
LogP: 7.17568
Related products
Synthetic route
123-75-1

pyrrolidine

1064662-32-3

methanesulfonic acid 3-[6-[bis-(3-methyl-butyl)-carbamoyl]-2-(4-cyanophenyl)imidazo[1,2a]pyridin-3-yl]-propyl ester

1064662-40-3

2-(4-cyano-phenyl)-3-(3-pyrrolidin-1-yl-propyl)-imidazo[1,2-a]pyridine-6-carboxylic acid bis-(3-methyl-butyl)-amide hydrochloride

Conditions
ConditionsYield
Stage #1: pyrrolidine; methanesulfonic acid 3-[6-[bis-(3-methyl-butyl)-carbamoyl]-2-(4-cyanophenyl)imidazo[1,2a]pyridin-3-yl]-propyl ester In acetonitrile at 50℃;
Stage #2: With hydrogenchloride
1064662-31-2

2-(4-Cyano-phenyl)-3-(3-hydroxy-propyl)-imidazo[1,2-a]pyridine-6-carboxylic acid bis-(3-methyl-butyl)-amide

1064662-40-3

2-(4-cyano-phenyl)-3-(3-pyrrolidin-1-yl-propyl)-imidazo[1,2-a]pyridine-6-carboxylic acid bis-(3-methyl-butyl)-amide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 1 h / 0 - 20 °C
2: acetonitrile / 50 °C
View Scheme
1064662-28-7

3-[6-[bis-(3-methyl-butyl)-carbamoyl]-2-(4-cyano-phenyl)-imidazo[1,2-a]pyridin-3-yl]-propionic acid

1064662-40-3

2-(4-cyano-phenyl)-3-(3-pyrrolidin-1-yl-propyl)-imidazo[1,2-a]pyridine-6-carboxylic acid bis-(3-methyl-butyl)-amide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C
1.2: 0.17 h / 0 °C
2.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C
3.1: acetonitrile / 50 °C
View Scheme
1064662-27-6

3-[6-[bis-(3-methyl-butyl)-carbamoyl]-2-(4-cyano-phenyl)-imidazo[1,2-a]pyridin-3-yl]-propionic acid ethyl ester

1064662-40-3

2-(4-cyano-phenyl)-3-(3-pyrrolidin-1-yl-propyl)-imidazo[1,2-a]pyridine-6-carboxylic acid bis-(3-methyl-butyl)-amide hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: lithium hydroxide; water / tetrahydrofuran / 48 h / 0 - 20 °C
1.2: brine / pH 6
2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C
2.2: 0.17 h / 0 °C
3.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C
4.1: acetonitrile / 50 °C
View Scheme
Raw Materials
123-75-1
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    Xuzhou Jinhe?Technology Co., Ltd. is an enterprise mainly engaged in pharmaceutical R&D outsourcing services. Taking advantage of rich professional experience and resource advantages in chemical synthesis, pharmaceutical chemistry and biotechnology,

    Xuzhou Jinhe Technology Co., Ltd. is an enterprise mainly engaged in pharmaceutical R&D outsourcing services. Taking advantage of rich professional experience and resource advantag

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