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Basic Information
CAS No.: 109-61-5
Name: Propyl chloroformate
Article Data: 22
Molecular Structure:
Molecular Structure of 109-61-5 (Propyl chloroformate)
Formula: C4H7ClO2
Molecular Weight: 122.551
Synonyms: Formicacid, chloro-, propyl ester (6CI,7CI,8CI);Propyl carbonochloridate;Propylchlorocarbonate;Chlorocarbonicacidpropylester;
EINECS: 203-687-7
Density: 1.119 g/cm3
Melting Point: <-70oC
Boiling Point: 116.2 °C at 760 mmHg
Flash Point: 29.1 °C
Appearance: colorless liquid
Hazard Symbols: ToxicT
Risk Codes: 10-23-34
Safety: 26-36-45
Transport Information: UN 2740 6.1/PG 1
PSA: 26.30000
LogP: 1.77180
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Chemistry

The Molecular formula of Propyl chloroformate (109-61-5): C4H7ClO2
The Molecular Weight of Propyl chloroformate (109-61-5): 122.55
The Molecular Structure of Propyl chloroformate (109-61-5):

Density: 1.119 g/cm
Boiling point: 116.2 °C at 760 mmHg
Flash point: 29.1 °C   
Solubility in water: insoluble
Air & Water Reactions: Highly flammable. Water (moisture in air or soil) reacts with generation of heat and hydrochloric acid.
Index of Refraction: 1.411
Molar Refractivity: 27.2 cm  
Polarizability: 10.78 10-24cm3 
Surface Tension: 29.2 dyne/cm  
Enthalpy of Vaporization: 35.46 kJ/mol 
Vapour Pressure: 18.4 mmHg at 25°C       
Appearance: A colorless liquid  
IUPAC name: propyl carbonochloridate 
InChI
InChI=1/C4H7ClO2/c1-2-3-7-4(5)6/h2-3H2,1H3
Smiles
O(C(=O)Cl)CCC 
Synonyms: Chlorocarbonicacidpropylester ; Chloro-formicacipropylester ; Formic acid, chloro-, propyl ester ; Propyl chloridocarbonate ; N-propyl chloroformate ; Propyl chloroformate   

Uses

The PROPYL CHLOROCARBONATE(109-61-5) is used as a flotation agent and reagent in organic synthesis.N-propyl chloroformate is a bactericide Propamocarb intermediates.

Production

Its preparation method is to add light through gas tank n-propanol, start stirring, and then pass into the flow meter phosgene phosgene, Tung-ray air temperature is 30 ℃ or so and continue to pass phosgene for a number of hours, close to the finish line sampling and analysis , compliance to cease pass phosgene, cooling, and then pass rush emptied of nitrogen gas and hydrogen chloride, phosgene and sabotage, sampling and analysis for the product. Reaction equation: CH3CH2CH2OH + COCl2 → ClCOOCH2CH2CH3
 

Toxicity Data With Reference

1.    

orl-mus LD50:650 mg/kg

    37ASAA    Kirk-Othmer Encyclopedia of Chemical Technology. 4 (1978),758.
2.    

ihl-mus LD50:319 ppm/1H

    37ASAA    Kirk-Othmer Encyclopedia of Chemical Technology. 4 (1978),758.
3.    

skn-mus LD50:10 mg/kg

    37ASAA    Kirk-Othmer Encyclopedia of Chemical Technology. 4 (1978),758.

Consensus Reports

EPA Extremely Hazardous Substances List. Reported in EPA TSCA Inventory.

Safety Profile

Poison by skin contact. Moderately toxic by ingestion and inhalation. A corrosive irritant to skin, eyes, and mucous membranes. Flammable when exposed to heat or flame, can react vigorously with oxidizing materials. When heated to decomposition it emits toxic fumes of Cl. Used as a reactive intermediate to polymerization initiators.
Hazard Codes: T
T: Toxic
Risk Statements
R10: Flammable.
R23: Toxic by inhalation.
R34: Causes burns.
Safety Statements
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36: Wear suitable protective clothing .
S45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
RIDADR: UN 2740 6.1/PG 1
WGK Germany: 1
RTECS: LQ6830000
HazardClass: 6.1(a)
PackingGroup: I

Standards and Recommendations

DOT Classification:  6.1; Label: Poison, Flammable Liquid, Corrosive