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Basic Information
| CAS No.: | 110-58-7 |
|---|---|
| Name: | Amylamine |
| Article Data: | 130 |
| Molecular Structure: | |
|
|
|
| Formula: | C5H13N |
| Molecular Weight: | 87.1649 |
| Synonyms: | Pentylamine(8CI);1-Aminopentane;1-Pentylamine;Monoamylamine;Monopentylamine;NSC 7906;Norleucamine;n-Amylamine;n-Pentylamine;1-Pentanamine; |
| EINECS: | 203-780-2 |
| Density: | 0.755 g/cm3 |
| Melting Point: | -55 °C(lit.) |
| Boiling Point: | 105.5 °C at 760 mmHg |
| Flash Point: | 4.4 °C |
| Solubility: | soluble |
| Appearance: | clear colourless to very slightly yellow liquid |
| Hazard Symbols: |
 F, C
|
| Risk Codes: | 11-22-34-42/43-20/21/22 |
| Safety: | 16-26-36/37/39-45-33 |
| Transport Information: | UN 1106 3/PG 2 |
| PSA: | 26.02000 |
| LogP: | 1.83560 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With borane-ammonia complex; C15H30Cl2CoN3P In hexane at 120℃; for 16h; Sealed tube; Inert atmosphere; chemoselective reaction; | 86% |
| With hydrogen; sodium methylate; nickel In methanol hydrogen generated in situ electrochemically on Raney nickel electrode; | 72% |
| With lithium aluminium tetrahydride | 71% |
Conditions
| Conditions | Yield |
|---|---|
| With ammonia; hydrogen In methanol at 30℃; for 15h; Autoclave; | 94% |
| With ammonium hydroxide; ammonium acetate; hydrogen; [Ru(cod)Cl]2; trisodium tris(3-sulfophenyl)phosphine In toluene at 145℃; under 48754.9 Torr; for 10h; | 47 % Chromat. |
| With ammonium hydroxide; hydrogen at 65℃; under 11251.1 Torr; for 12h; Autoclave; Green chemistry; | |
| With pyridoxal 5'-phosphate; Amine transaminase 117; rac-methylbenzylamine; N-2-hydroxyethylpiperazine-N'-2-ethanesulfonic acid In water; dimethyl sulfoxide at 30℃; Reagent/catalyst; Enzymatic reaction; |
- 26330-06-3
pentyl azide
- 110-58-7
1-pentanamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen; MCM-silylamine Pd(II) In methanol at 20℃; for 2h; Reduction; | 90% |
- 1119-46-6
5-chloro-valeric acid
A
- 110-89-4
piperidine
B
- 675-20-7
piperidin-2-one
C
- 110-58-7
1-pentanamine
D
- 109-73-9
N-butylamine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 5-chloro-valeric acid With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry; Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry; | A 85% B 9% C 2% D 2% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide; benzyltrimethylazanium tribroman-2-uide In water at 70℃; for 2h; | 80% |
| With sodium hydroxide; sodium bromite In water at 75℃; for 0.5h; | 60% |
| With sodium hypochlorite |
Conditions
| Conditions | Yield |
|---|---|
| With carbonylchlorohydrido(4,5-bis((diisopropylphosphino)methyl)acridine)ruthenium(II); ammonia; water In 1,4-dioxane at 135℃; under 5700.38 Torr; for 30h; Inert atmosphere; | A 70.0 %Chromat. B n/a |
- 60169-95-1
N,N'-dipentyl-oxalamide
- 110-58-7
1-pentanamine
Conditions
| Conditions | Yield |
|---|---|
| With potassium tert-butylate; hydrogen; [Ru(PtBuNNHBn)H(CO)Cl] In toluene at 135℃; under 30003 Torr; for 24h; | 97 %Spectr. |
- 5775-76-8, 5780-42-7, 628-79-5
valeraldoxime
- 110-58-7
1-pentanamine
Conditions
| Conditions | Yield |
|---|---|
| With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
| With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
| With palladium on activated charcoal; acetic acid Hydrogenation; |
Conditions
| Conditions | Yield |
|---|---|
| With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
| With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
| With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; |
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h; | A 36% B 56% |
| With sodium hydroxide; sodium persulfate; copper dichloride In water at 85 - 90℃; for 7h; | A 36% B 56% |
| With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h; | A 36% B 52% |
| With sodium hydroxide; sodium persulfate; sodium chloride In water at 85 - 90℃; for 7h; | A 36% B 52% |
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Amylamine
Chemistry
Molecular Formula: C5H13N 
Molecular Weight: 87.16
Density: 0.755
Melting point: -50 oC
Boiling point: 104 oC
VAPOR DENSITY: 3.0
AUTOIGNITION: 435 oC
FLASH POINT: 20 oC
Refractive index: 1.41-1.412
Flash point: 4 oC
Water solubility: soluble
Soluble: alcohol
PHYSICAL STATE OF Amylamine (110-58-7): clear liquid
ODOR OF Amylamine (110-58-7): ammonia odor
Molecular Weight: 87.16
Density: 0.755
Melting point: -50 oC
Boiling point: 104 oC
VAPOR DENSITY: 3.0
AUTOIGNITION: 435 oC
FLASH POINT: 20 oC
Refractive index: 1.41-1.412
Flash point: 4 oC
Water solubility: soluble
Soluble: alcohol
PHYSICAL STATE OF Amylamine (110-58-7): clear liquid
ODOR OF Amylamine (110-58-7): ammonia odor
Uses
Amylamine (110-58-7) can be used for medicine, dyes, emulsifiers, thiofide, anticorrosive agent, flotation agent and so on.
Production
In the presence of catalyst, sodium azide reacts with caproic acid. After alkali neutralization, wet distillation and then extracting distillate by aether. Extract liquor is refined to Amylamine (110-58-7) by ectification.
Toxicity Data With Reference
| 1. | ipr-rat LDLo:37,500 µg/kg | FATOAO Farmakologiya i Toksikologiya (Moscow). 31 (1968),238. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Hazard Symbols: F;C (Flammable; Corrosive)
Risk Codes: R11;R20/21/22;R34 (Highly flammable; Harmful by inhalation, in contact with skin and if swallowed; Causes burns.)
Safety Description: S16;S26;S36/37/39;S45 (Keep away from sources of ignition; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice; Wear suitable protective clothing, gloves and eye/face protection; In case of accident or if you feel unwell, seek medical advice immediately)
Transport Information: UN 1106
Poison by intraperitoneal route. A corrosive. A flammable liquid. When heated to decomposition it emits toxic vapors of NOx.
Risk Codes: R11;R20/21/22;R34 (Highly flammable; Harmful by inhalation, in contact with skin and if swallowed; Causes burns.)
Safety Description: S16;S26;S36/37/39;S45 (Keep away from sources of ignition; In case of contact with eyes, rinse immediately with plenty of water and seek medical advice; Wear suitable protective clothing, gloves and eye/face protection; In case of accident or if you feel unwell, seek medical advice immediately)
Transport Information: UN 1106
Poison by intraperitoneal route. A corrosive. A flammable liquid. When heated to decomposition it emits toxic vapors of NOx.
Standards and Recommendations
DOT Classification: 8; Label: Corrosive, Flammable Liquid (UN 2734); DOT Class: 3; Label: Flammable Liquid, Corrosive (UN 2733)
PURITY (GC): 98.0% min
SPECIFIC GRAVITY: 0.75 - 0.76
MOISTURE: 0.1% max
COLOR (AHHA): 30 max
PURITY (GC): 98.0% min
SPECIFIC GRAVITY: 0.75 - 0.76
MOISTURE: 0.1% max
COLOR (AHHA): 30 max
Specification
STORAGE: Store with flammable liquids. Store outside or in a detached building. Keep separated from incompatible substances. Protect from physical damage. Avoid heat, flames, sparks and other sources of ignition.