Detail of "1100-10-3"

CAS Number:
1100-10-3
Name:
Benzenamine,4-nitro-N-(4-nitrophenyl)-N-phenyl-
Superlist Name:
Bis(4-nitrophenyl)phenylamine
Molecular Structure:
Formula:
C18H13 N3 O4
Molecular Weight:
335.31
Synonyms:
Triphenylamine,4,4'-dinitro- (6CI,7CI,8CI); 4,4'-Dinitrotriphenylamine;N,N-Bis(4-nitrophenyl)aniline
Melting Point:
196-198℃

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p-Nitrodiphenylamine synthesis: p-Nitrodiphenylamine synthesis. Sturm, Budd Harvey (Goodyear Tire and Rubber Co. , USA). Eur. Pat. Appl. EP 203878 A1 3 Dec 1986, 17 pp. DESIGNATED STATES: R: BE, DE, FR, GB, IT. (European Patent Organization) CODEN: EPXXDW. CLASS: ICM: C07C085-04. APPLICATION: EP 86-630090 9 May 1986. PRIORITY: US 85-735513 20 May 1985. DOCUMENT TYPE: Patent CA Section: 25 (Benzene, Its Derivatives, and Condensed Benzenoid Compounds) Section cross-reference(s): 67 The title compd. (I) was prepd. by condensation of p-halonitrobenzenes and formanilide (II) in the presence of a Zn salt as a catalyst, at atm. pressure to 300 KPa and 120°-250°. A mixt. 1314-98-3 and 1100-10-3 which are cas registry numbers of substances are two of reagents here. of 100 g p-NO2C6H4Cl and II (prepd. in situ) in the presence of 0.5 g Zn(OAc)2 and K2CO3 in PhMe was heated to 165° under azeotropic conditions to give 96.6% I. .