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112-70-9

Basic Information
CAS No.: 112-70-9
Name: 1-Tridecanol
Article Data: 42
Molecular Structure:
Molecular Structure of 112-70-9 (1-Tridecanol)
Formula: C13H28 O
Molecular Weight: 200.365
Synonyms: NSC 5252;Tridecyl alcohol; n-Tridecan-1-ol; n-Tridecanol; n-Tridecyl alcohol
EINECS: 203-998-8
Density: 0.822 g/mL at 25 °C(lit.)
Melting Point: 29-34 °C(lit.)
Boiling Point: 272.1 °C at 760 mmHg
Flash Point: 121.1 °C
Solubility: chloroform: 0.1 g/mL, clear,insoluble in water
Appearance: white solid.
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: Mildly toxic by ingestion and skin contact. A skin irritant. Combustible when exposed to heat or flame. To fight fire, use mist, spray, dry chemical, foam. When heated to decomposition it emits acrid smoke and irritating fumes. See also ALCOHOL, DENATURED; ALCOHOLS, C6-12; ALCOHOLS, C9-11; ALCOHOLS, C12-13, ETHOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED; ALCOHOLS, C12-16, ETHOXYLATED; ALCOHOLS, C14-15, ETHOXYLATED; ALCOHOLS, C16-18, ETHOXYLATED; ALCOHOLS, C8-10, ETHOXYLATED PROPOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED PROPOXYLATED; ALCOHOLS, N.O.S..
PSA: 20.23000
LogP: 4.28970
Synthetic route
638-53-9

tridecanoic acid

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With hydrogen; Rh/Al2O3; molybdenum hexacarbonyl In 1,2-dimethoxyethane at 150℃; under 76000 Torr; for 16h;97%

C13H25Cl3O

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With lithium borohydride; sodium hydroxide In isopropyl alcohol Temperature; Jocic Reaction; Heating; Inert atmosphere;95%
1731-88-0

methyl tridecanoate

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
Stage #1: methyl tridecanoate With bis(acetylacetonato)dioxidomolybdenum(VI); 1,1,3,3-Tetramethyldisiloxane; Triphenylphosphine oxide In toluene at 100℃; for 20h; Inert atmosphere; Sealed tube;
Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran; toluene for 2h; Inert atmosphere;
94%
1436673-44-7

C18H36O2

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With methanol; toluene-4-sulfonic acid at 20℃; for 2h;90%
32466-55-0

(E)-tridec-2-enoic acid

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With hydrogen; Rh/Al2O3; molybdenum hexacarbonyl In 1,2-dimethoxyethane at 150℃; under 76000 Torr; for 16h;89%
110023-67-1

1-Methyl-4-(1-methylsulfanyl-tridecane-1-sulfinyl)-benzene

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate In 1,4-dioxane; water Irradiation;80%
28267-29-0

ethyl tridecanoate

112-70-9

tridecan-1-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether at 0 - 20℃;79%
With ethanol; sodium
130340-56-6

2-(3-carboxypropyl)-5-(12-hydroxydodecyl)thiophene

A

629-76-5

pentadecanol

B

112-70-9

tridecan-1-ol

C

36653-82-4

1-Hexadecanol

D

62643-46-3

20-hydroxyeicosanoic acid

Conditions
ConditionsYield
With Raney nickel W-2 In ethanol for 2h; Heating; Further byproducts given;A 2.8%
B 3.5%
C 12.6%
D 65%
130340-56-6

2-(3-carboxypropyl)-5-(12-hydroxydodecyl)thiophene

A

112-70-9

tridecan-1-ol

B

112-72-1

1-Tetradecanol

C

36653-82-4

1-Hexadecanol

D

62643-46-3

20-hydroxyeicosanoic acid

Conditions
ConditionsYield
With Raney nickel W-2 In ethanol for 2h; Heating; Further byproducts given;A 3.5%
B 6%
C 12.6%
D 65%
130340-56-6

2-(3-carboxypropyl)-5-(12-hydroxydodecyl)thiophene

A

112-70-9

tridecan-1-ol

B

112-72-1

1-Tetradecanol

C

117197-09-8

tridecyl hexanoate

D

62643-46-3

20-hydroxyeicosanoic acid

Conditions
ConditionsYield
With Raney nickel W-2 In ethanol for 2h; Heating; Further byproducts given;A 3.5%
B 6%
C 0.5%
D 65%
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Chemistry

IUPAC Name: Tridecan-1-ol
Synonyms : N-Tridecanol ; N-Tridecyl alcohol ; Rarechem al bd 0158 ; Tridecanol ; Tridecyl alcohol ; 1-Hydroxytridecane ; C13 linear primary alcohol ; N-Tridecan-1-ol
Product Categories: 1-Alkanols;Biochemistry;Higher Fatty Acids & Higher Alcohols;Monofunctional & alpha,omega-Bifunctional Alkanes;Monofunctional Alkanes;Saturated Higher Alcohols
CAS NO: 112-70-9
Molecular Formula: C13H28O
Molecular Weight: 200.36
Molecular Structure:
EINECS: 203-998-8
BRN : 1739991
Mol File: 112-70-9.mol
Index of Refraction: 1.443
Surface Tension: 30.6 dyne/cm
Density: 0.832 g/cm3
Flash Point: 121.1 °C
Enthalpy of Vaporization: 59.25 kJ/mol
Boiling Point: 272.1 °C at 760 mmHg
Vapour Pressure: 0.000807 mmHg at 25°C
Melting point: 29-34 °C(lit.)
Appearance: 1-Tridecanol (CAS NO.112-70-9) is white low melting solid.
Solubility: 1-Tridecanol (CAS NO.112-70-9) is soluble in alcohol and ether, insoluble in water.

Uses

 1-Tridecanol (CAS NO.112-70-9) is used raw materials in production of lubricants, surfactants, pesticides, and ink solvents.

Toxicity Data With Reference

1.    

skn-rbt 410 mg open MLD

    UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 10/14 ,1964.
2.    

orl-rat LD50:17,200 mg/kg

    NPIRI*    Raw Material Data Handbook, Vol.1: Organic Solvents, 1974. 1 (1974),114.
3.    

skn-rbt LD50:5600 mg/kg

    NPIRI*    Raw Material Data Handbook, Vol.1: Organic Solvents, 1974. 1 (1974),114.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Hazard Codes IrritantXi
Risk Statements 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements 26-36
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing.
WGK Germany 3
RTECS YD4200000
 

Specification

1.General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear. During a fire, irritating and highly toxic gases may be generated by thermal decomposition or combustion.
Extinguishing Media: In case of fire, use water, dry chemical, chemical foam, or alcohol-resistant foam. 
2.Handling: Wash thoroughly after handling. Remove contaminated clothing and wash before reuse. Avoid contact with eyes, skin, and clothing. Avoid ingestion and inhalation.
Storage: Store 1-Tridecanol (CAS NO.112-70-9) in a cool, dry place. Keep container closed when not in use.