Detail of "1125-99-1"

CAS Number:
1125-99-1
Name:
Pyrrolidine,1-(1-cyclohexen-1-yl)-
Superlist Name:
1-Pyrrolidino-1-cyclohexene
Molecular Structure:
Formula:
C10H17 N
Molecular Weight:
151.25
Synonyms:
1-(1-Cyclohexen-1-yl)pyrrolidine;1-(1-Cyclohexenyl)pyrrolidine; 1-(1-Pyrrolidino)-1-cyclohexene;1-(1-Pyrrolidinyl)cyclohexene; 1-(Pyrrolidine-1-yl)-1-cyclohexene;1-Pyrrolidino-1-cyclohexene; 1-Pyrrolidinocyclohexene; Cyclohexanonepyrrolidine enamine; N-(1-Cyclohexen-1-yl)pyrrolidine;N-(1-Cyclohexenyl)pyrrolidine; NSC 29652
EINECS:
214-414-6
Density:
0.94
Boiling Point:
114-115 ºC (15 mmHg)
Flash Point:
39 ºC
Hazard Symbols:
Risk Codes:
R10;R20/21/22;R36/37/38
Safety:
Hazard Codes Xi
Risk Statements 10-36/37/38-20/21/22
Safety Statements 16-26-36/37/39
RIDADR UN 1993 3/PG 3

WGK Germany 3

HazardClass 3
PackingGroup III
Details

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1-Pyrrolidino-1-cyclohexene

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1-(Cyclohexen-1-yl)pyrrolidine

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Preparation of t-butyl 3-oxopent-4-enoate and its use as a Nazarov reagent: Preparation of t-butyl 3-oxopent-4-enoate and its use as a Nazarov reagent. Ohta, Shunsaku; Shimabayashi, Akihiro; Hatano, Satoru; Okamoto, Masao (Kyoto Coll. Pharm., Kyoto 607, Japan). Synthesis, (9), 715-16 (English) 1983. CODEN: SYNTBF. ISSN: 0039-7881. 1125-99-1 and 88023-67-0 which are cas registry numbers of chemicals are mentioned. DOCUMENT TYPE: Journal CA Section: 23 (Aliphatic Compounds) The reaction of LiCH2CO2CMe3 with ClCH2CH2CO2Et gave ClCH2CH2COCH2CO2CMe3, which was dehydrochlorinated with Et3N to give 84% Nazarov reagent H2C:CHCOCH2CO2CMe3 (I). Cyclization of I with cyclohexanone pyrrolidine enamine gave 73% II. .

New syntheses with a-acylketenimines and a-acylketenes: New syntheses with a-acylketenimines and a-acylketenes. Capuano, Lilly; Djokar, Keramatollah; Schneider, Nicole; Wamprecht, Christian (Fachber. 13, Org. Chem., Univ. Saarlandes, Saarbruecken D-6600, Fed. Rep. Ger.). Liebigs Ann. Chem., (3), 183-7 (German) 1987. 1125-99-1 is also in the experiment. CODEN: LACHDL. ISSN: 0170-2041. DOCUMENT TYPE: Journal CA Section: 28 (Heterocyclic Compounds (More Than One Hetero Atom)) RCOCR1:C:NR2 (R = R1 = Ph, 4-ClC6H4, 4-MeC6H4, 4-MeOC6H4, Me, R2 = 4-ClC6H4, 4-MeC6H4; R = Me, R1 = Et, R2 = Ph) were prepd. by treating RCOCN2COR1 with Ph3P:NR2 and were converted to various pyran, oxazine, oxathiin, thiazine, thiopyrimidinone, pyrazole, and thiolane derivs. RCOCR1:CO, prepd. by thermal rearrangement of RCOCN2COR1, were treated in situ with thioureas to give acylacetylthioureas which cyclized readily to thiouracils. .