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1126-09-6

Basic Information
CAS No.: 1126-09-6
Name: Ethyl 4-piperidinecarboxylate
Article Data: 20
Molecular Structure:
Molecular Structure of 1126-09-6 (Ethyl 4-piperidinecarboxylate)
Formula: C8H15NO2
Molecular Weight: 157.213
Synonyms: ethyl piperidine-4-carboxylate;Isonipecoticacid, ethyl ester (6CI,7CI,8CI);4-(Ethoxycarbonyl)piperidine;4-Carboethoxypiperidine;Ethyl 4-piperidinecarboxylate;
EINECS: 214-416-7
Density: 1.003 g/cm3
Boiling Point: 204 °C at 760 mmHg
Flash Point: 83.3 °C
Solubility: miscible with water
Appearance: clear colorless to slightly brown liquid
Hazard Symbols: CorrosiveC,IrritantXi
Risk Codes: 34-36/37/38
Safety: 23-24/25-36-26
PSA: 38.33000
LogP: 0.87790
Synthetic route
498-94-2

isonipecotic acid

64-17-5

ethanol

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
With thionyl chloride at 0℃; for 48h; Reflux;94%
With sulfuryl dichloride In N,N-dimethyl-formamide at 80℃; for 6h; Inert atmosphere;92%
With thionyl chloride for 6h; Reflux;86.5%
69001-10-1

1-acetyl-piperidine-4-carboxylic acid ethyl ester

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
Stage #1: 1-acetyl-piperidine-4-carboxylic acid ethyl ester With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 0℃; for 2h; Inert atmosphere;
Stage #2: With ethylmagnesium bromide In diethyl ether; dichloromethane at -78℃; for 2h; Inert atmosphere; chemoselective reaction;
71%
498-94-2

isonipecotic acid

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
With hydrogenchloride
1570-45-2

isonicotinic acid ethylester

A

6457-49-4

4-piperidinemethanol

B

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
With sodium; butan-1-ol
1570-45-2

isonicotinic acid ethylester

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
With 1,4-dioxane; nickel at 175 - 180℃; under 91938.4 Torr; Hydrogenation;
With sodium tetrahydroborate; rhodium(III) chloride 40 deg C, ethanol; Yield given. Multistep reaction;
With hydrogen In neat (no solvent) at 50℃; under 760.051 Torr; for 36h; Temperature; Solvent;
1570-45-2

isonicotinic acid ethylester

71-36-3

butan-1-ol

sodium

sodium

A

6457-49-4

4-piperidinemethanol

B

1126-09-6

4-carbethoxypiperidine

1083159-13-0

O2-(2,4-dinitrophenyl) 1-[(4-ethoxycarbonyl)piperidin-1-yl]diazen-1-ium-1,2-diolate

1126-09-6

4-carbethoxypiperidine

Conditions
ConditionsYield
With GLUTATHIONE; diethylenetriaminopentaacetic acid In dimethyl sulfoxide at 37℃; pH=7.4; aq. phosphate buffer; Inert atmosphere;
1126-09-6

4-carbethoxypiperidine

98-88-4

benzoyl chloride

136081-74-8

ethyl 1-benzoyl-4-piperidine-carboxylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 20h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; for 0.333333h;99%
With triethylamine In dichloromethane at 20℃;93%
1126-09-6

4-carbethoxypiperidine

6457-49-4

4-piperidinemethanol

Conditions
ConditionsYield
Stage #1: 4-carbethoxypiperidine With lithium aluminium tetrahydride In tetrahydrofuran at 20℃;
Stage #2: With sodium hydroxide; water In tetrahydrofuran at 20℃; for 0.5h;
100%
Stage #1: 4-carbethoxypiperidine With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;
Stage #2: With ethanol; water In tetrahydrofuran at 0℃;
100%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;92%
872-85-5

pyridine-4-carbaldehyde

1126-09-6

4-carbethoxypiperidine

138030-54-3

1-Pyridin-4-ylmethyl-piperidine-4-carboxylic acid ethyl ester

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane molecular sieve;100%
Stage #1: pyridine-4-carbaldehyde; 4-carbethoxypiperidine In dichloromethane at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 5h;
99%
Stage #1: pyridine-4-carbaldehyde; 4-carbethoxypiperidine In dichloromethane for 0.166667h;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 23℃; for 16h;
91%
With borane pyridine In ethanol27%
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    ProductName:Ethyl 4-piperidinecarboxylate Synonyms:Ethyl piperidine-4-carboxylate;4-Piperidinecarboxylic acid, ethyl ester; Ethyl 4-Piperidinecarboxylate;Ethyl Isonipecotate;4-Piperidinecarboxylic Acid Ethyl Ester;Isonipecotic Acid Ethyl Ester;

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  • 1126-09-6  CAS NO.1126-09-6

  • Casno:

    1126-09-6

    1126-09-6 CAS NO.1126-09-6

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  • Ethyl isonipecotate

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    Ethyl isonipecotate

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Chemistry

IUPAC Name: Ethyl piperidine-4-carboxylate
Synonyms of Ethyl isonipecotate (CAS NO.1126-09-6): Isonipecoticacid, ethyl ester (6CI,7CI,8CI) ; 4-(Ethoxycarbonyl)piperidine ; Ethyl 4-piperidinecarboxylate
CAS NO: 1126-09-6
Molecular Formula: C8H15NO2
Molecular Weight: 157.21
Molecular Structure:
H bond acceptors: 3
H bond donors: 1
Freely Rotating Bonds: 3
Polar Surface Area: 29.54 Å2
Index of Refraction: 1.448
Molar Refractivity: 41.99 cm3
Molar Volume: 156.6 cm3
Surface Tension: 32 dyne/cm
Density: 1.003 g/cm3
Flash Point: 83.3 °C
Enthalpy of Vaporization: 44.02 kJ/mol
Boiling Point: 204 °C at 760 mmHg
Vapour Pressure: 0.27 mmHg at 25°C
Water Solubility: miscible
Appearance: clear colorless to slightly brown liquid
Product Categories of Ethyl isonipecotate (CAS NO.1126-09-6): Pharmaceutical Intermediates;Piperidines, Piperidones, Piperazines;pharmacetical;AMINOACIDS DERIVATIVES;Piperidine
SMILES: O=C(OCC)C1CCNCC1
InChI: InChI=1/C8H15NO2/c1-2-11-8(10)7-3-5-9-6-4-7/h7,9H,2-6H2,1H3
InChIKey: RUJPPJYDHHAEEK-UHFFFAOYAB
Std. InChI: InChI=1S/C8H15NO2/c1-2-11-8(10)7-3-5-9-6-4-7/h7,9H,2-6H2,1H3
Std. InChIKey: RUJPPJYDHHAEEK-UHFFFAOYSA-N

Safety Profile

Safety Information about Ethyl isonipecotate (CAS NO.1126-09-6):
Hazard Codes:CorrosiveC,IrritantXi
Risk Statements: 34-36/37/38
R34: Causes burns. 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 23-24/25-36-26
S23: Do not breathe vapour. 
S24/25: Avoid contact with skin and eyes. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 3
Hazard Note: Irritant
HS Code: 29333999

Specification

General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear. During a fire, irritating and highly toxic gases may be generated by thermal decomposition or combustion. Will burn if involved in a fire. Combustible liquid.
Extinguishing Media: Use foam, dry chemical, or carbon dioxide. 
Handling: Wash thoroughly after handling. Remove contaminated clothing and wash before reuse. Do not breathe dust, vapor, mist, or gas. Do not get in eyes, on skin, or on clothing. Use only in a chemical fume hood.
Storage: Keep away from sources of ignition. Store in a cool, dry place. Keep container closed when not in use. Store in a tightly closed container. Corrosives area.