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112811-68-4

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Basic Information
CAS No.: 112811-68-4
Name: 3-OXO-3-(2,4,5-TRIFLUORO-3-METHOXY-PHENYL)-PROPIONIC ACID ETHYL ESTER
Article Data: 13
Molecular Structure:
Molecular Structure of 112811-68-4 (3-OXO-3-(2,4,5-TRIFLUORO-3-METHOXY-PHENYL)-PROPIONIC ACID ETHYL ESTER)
Formula: C12H11 F3 O4
Molecular Weight: 276.212
Synonyms: Ethyl2,4,5-trifluoro-3-methoxybenzoylacetate; Ethyl2-(2,4,5-trifluoro-3-methoxybenzoyl)acetate; Ethyl2-(3-methoxy-2,4,5-trifluorobenzoyl)acetate; Ethyl 3-methoxy-2,4,5-trifluoro-b-oxobenzenepropanoate
Density: 1.311±0.06 g/cm3(Predicted)
Melting Point: 59-60 °C
Boiling Point: 317.7±37.0 °C(Predicted)
PSA: 52.60000
LogP: 2.24840
Related products
Synthetic route
112811-67-3

diethyl 3-methoxy-2,4,5-trifluorobenzoylmalonate

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
With water; toluene-4-sulfonic acid for 16h; Heating / reflux;89%
With hydrogenchloride; water
With toluene-4-sulfonic acid In water for 3h; Reflux;17.3 g
With toluene-4-sulfonic acid In water for 9h;
1071-46-1

hydrogen ethyl malonate

112811-66-2

2,4,5-trifluoro-3-methoxybenzoyl chloride

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
With [2,2]bipyridinyl; n-butyllithium 1.) THF, hexane, from -20 deg C to -5 deg C, 2.) THF, hexane, -30 deg C, 2 h; Yield given. Multistep reaction;
Stage #1: 2,4,5-trifluoro-3-methoxybenzoyl chloride With n-butyllithium In tetrahydrofuran; hexane at -78℃;
Stage #2: hydrogen ethyl malonate In tetrahydrofuran; hexane; dichloromethane at -78 - 10℃;
Stage #1: hydrogen ethyl malonate With n-butyllithium In tetrahydrofuran at -50 - 0℃;
Stage #2: 2,4,5-trifluoro-3-methoxybenzoyl chloride In tetrahydrofuran at -50 - 20℃;
Stage #3: With hydrogenchloride In tetrahydrofuran; water

diethylmalonate potassium salt

112811-66-2

2,4,5-trifluoro-3-methoxybenzoyl chloride

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Stage #1: diethylmalonate potassium salt With triethylamine; magnesium chloride In acetonitrile at 20 - 25℃;
Stage #2: 2,4,5-trifluoro-3-methoxybenzoyl chloride With triethylamine In acetonitrile at 20℃; for 18h;
112811-65-1

3-methoxy-2,4,5-trifluorobenzoic acid

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C
2.1: n-BuLi / hexane; tetrahydrofuran / -78 °C
2.2: hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C
View Scheme
Multi-step reaction with 2 steps
1.1: (COCl)2; DMF / CH2Cl2
2.1: MgCl2; Et3N / acetonitrile / 20 - 25 °C
2.2: Et3N / acetonitrile / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: oxalyl chloride, DMF / CH2Cl2 / 18 h / Ambient temperature
2: 1.) n-BuLi, 2,2'-bipyridyl / 1.) THF, hexane, from -20 deg C to -5 deg C, 2.) THF, hexane, -30 deg C, 2 h
View Scheme
136897-64-8

methyl 3-methoxy-2,4,5-trifluorobenzoate

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: aq. NaOH / methanol
2.1: (COCl)2; DMF / CH2Cl2
3.1: MgCl2; Et3N / acetonitrile / 20 - 25 °C
3.2: Et3N / acetonitrile / 18 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: 61 percent / 1.0 N aq. NaOH / methanol / 3 h / Ambient temperature
2: oxalyl chloride, DMF / CH2Cl2 / 18 h / Ambient temperature
3: 1.) n-BuLi, 2,2'-bipyridyl / 1.) THF, hexane, from -20 deg C to -5 deg C, 2.) THF, hexane, -30 deg C, 2 h
View Scheme
112811-66-2

2,4,5-trifluoro-3-methoxybenzoyl chloride

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine; magnesium chloride / ethyl acetate
2: hydrogenchloride; water
View Scheme
Multi-step reaction with 2 steps
1.1: magnesium; tetrachloromethane / ethanol / 2.5 h / Reflux
1.2: 2 h
2.1: toluene-4-sulfonic acid / water / 3 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: magnesium ethylate / toluene
2: toluene-4-sulfonic acid / water / 9 h
View Scheme
6148-64-7

ethyl potassium malonate

112811-66-2

2,4,5-trifluoro-3-methoxybenzoyl chloride

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Stage #1: ethyl potassium malonate With magnesium chloride In ethyl acetate at 20℃; for 0.5h; Inert atmosphere;
Stage #2: With triethylamine In ethyl acetate at 20℃; for 0.5h; Inert atmosphere;
Stage #3: 2,4,5-trifluoro-3-methoxybenzoyl chloride In ethyl acetate for 2h; Inert atmosphere; Reflux;		21.3 g
With triethylamine
112811-64-0

2,4,5-trifluoro-3-methoxy-benzamide

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sulfuric acid / 3.5 h / 100 °C
2: thionyl chloride / 3 h
3: magnesium ethylate / toluene
4: toluene-4-sulfonic acid / water / 9 h
View Scheme
112811-63-9

3-methoxy-2,4,5-trifluorobenzonitrile

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sulfuric acid; water / 1 h / 110 °C
2: sulfuric acid / 3.5 h / 100 °C
3: thionyl chloride / 3 h
4: magnesium ethylate / toluene
5: toluene-4-sulfonic acid / water / 9 h
View Scheme
13332-24-6

1-bromo-2,4,5-trifluoro-3-methoxybenzene

112811-68-4

ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1-methyl-pyrrolidin-2-one / 4.5 h / 140 - 150 °C
2: sulfuric acid; water / 1 h / 110 °C
3: sulfuric acid / 3.5 h / 100 °C
4: thionyl chloride / 3 h
5: magnesium ethylate / toluene
6: toluene-4-sulfonic acid / water / 9 h
View Scheme
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    112811-68-4

    3-oxo-3-(2,4,5-trifluoro-3-methoxyphenyl)propanoic acid ethyl ester

    Min.Order: 10 Milligram

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    112811-68-4

    Ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

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    Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

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    112811-68-4

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    Chemical Technology Co.,LTD is a professional enterprise which engaged in pharmaceutical intermediates, material intermediates production research and development.Company foc

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  • ethyl 3-oxo-3-(2,4,5-trifluoro-3-Methoxyphenyl)propanoate

  • Casno:

    112811-68-4

    ethyl 3-oxo-3-(2,4,5-trifluoro-3-Methoxyphenyl)propanoate

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    Reply quotation within 2 hours.Guarantee the time of delivery. Update the progress of customization Weekly.High purity& High product customization success rate.Inquiries for other compounds are acceptable. Storage:refrigeration Package:1g,5g,10g,100g

    Shanghai Yuanding Chem. Sci. & Tech. Co., Ltd. was established in 2008, is mainly engaged in customizing services for Pharmaceutical intermediates and active molecular API for 15 y

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     China (Mainland)  |  Contact Details

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  • 3-Oxo-3-(2,4,5-trifluoro-3-methoxy-phenyl)-propionic acid ethyl ester

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    112811-68-4

    3-Oxo-3-(2,4,5-trifluoro-3-methoxy-phenyl)-propionic acid ethyl ester

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    Nanjing Norris Pharm Technology Co., Ltd., born in July, 2012, is a new company registered in Nanjing, Jiangsu Province,China. Norris grows tremendously since 2012.Till Dec.31,2015

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    Business Type:Lab/Research institutions

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  • Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

  • Casno:

    112811-68-4

    Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

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  • Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

  • Casno:

    112811-68-4

    Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

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    Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

  • Casno:

    112811-68-4

    Benzenepropanoic acid,2,4,5-trifluoro-3-methoxy-b-oxo-, ethyl ester

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant informationAppearance:White solid Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place P

    Nanjing Chemlin Chemical Industry Co., Ltd was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu P

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    China (Mainland)  |  Contact Details

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  • Ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

  • Casno:

    112811-68-4

    Ethyl 3-methoxy-2,4,5-trifluorobenzoylacetate

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

    Welcome to Capot . Established in 1996 ,Capot Chemical Co.,Ltd is a fine organics manufacturing facility which located in Hangzhou,P.R.China. We produce a wide range of organics,

  • Capot Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-571-85586718

    Address:join hands science park,NO.4028 nanhuan road,hanghzou ,zhejiang,china

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  • Ethyl 3-oxo-3-(2,4,5-trifluoro-3-Methoxyphenyl)propanoate

  • Casno:

    112811-68-4

    Ethyl 3-oxo-3-(2,4,5-trifluoro-3-Methoxyphenyl)propanoate

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    The system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin

    SimSon Pharma, a renowned name in pharmaceutical sector, has built high its reputation as a complete solution provider in contract research arena. We are a JAS/ANZ ISO 9001:2015 Ce

  • Simson Pharma Limited

    India  |  Contact Details

    Business Type:Manufacturers

    Tel:+91-22-40068689/ 40148689

    Address:Near Dahisar Toll Naka

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