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CAS No.: | 119692-59-0 |
---|---|
Name: | 4-Hydroxybutyl acrylate glycidyl ether |
Article Data: | 2 |
Molecular Structure: | |
Formula: | C10H16 O4 |
Molecular Weight: | 200.235 |
Synonyms: | 2-Propenoicacid, 4-(oxiranylmethoxy)butyl ester (9CI); 1,4-Butylene glycol glycidyl etheracrylate; 4-(Glycidyloxy)butyl acrylate; 4-Glycidoxybutyl acrylate;4-Hydroxybutyl acrylate glycidyl ether; 4HBAGE |
Density: | 1.077g/cm3 |
Boiling Point: | 287.531°C at 760 mmHg |
Flash Point: | 123.267°C |
PSA: | 48.06000 |
LogP: | 0.91120 |
1,4-butanediol monoglycidyl ether
ethyl acrylate
4-Hydroxybutyl acrylate glycidyl ether
Conditions | Yield |
---|---|
Stage #1: 1,4-butanediol monoglycidyl ether; ethyl acrylate With titanium(IV) isopropylate at 95℃; under 300.03 Torr; for 4h; Reflux; Stage #2: With 4-methoxy-phenol under 300.03 Torr; | 97% |
With titanium(IV) isopropylate; 4-methoxy-phenol at 95℃; under 300.03 Torr; for 6h; Reflux; |
2-methoxyethyl acrylate
1,4-butanediol monoglycidyl ether
4-Hydroxybutyl acrylate glycidyl ether
Conditions | Yield |
---|---|
With tetrabutoxytitanium; 4-methoxy-phenol In o-xylene at 80 - 90℃; under 75.0075 Torr; | 83.7% |
tetrahydrofurfuryl acrylate
1,4-butanediol monoglycidyl ether
4-Hydroxybutyl acrylate glycidyl ether
Conditions | Yield |
---|---|
With tetrabutoxytitanium; 4-methylisopropylbenzene; 4-methoxy-phenol at 89 - 102℃; under 30.003 Torr; | 70.4% |
1,4-butanediol monoglycidyl ether
acrylic acid methyl ester
4-Hydroxybutyl acrylate glycidyl ether
Conditions | Yield |
---|---|
With tetrabutoxytitanium; 4-methoxy-phenol In hexane; toluene at 72 - 92℃; | 111.1 g |
4-Hydroxybutyl acrylate glycidyl ether
4-Hydroxybenzophenone
acrylic acid 4-[3-(4-benzoyl-phenoxy)-2-hydroxy-propoxy]butyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 24h; Reflux; | |
With sodium hydroxide; potassium carbonate In hexane; dichloromethane; water; acetonitrile | |
With potassium carbonate In acetonitrile for 24h; Reflux; | 5.5 g |
2-Benzoylbenzoic acid
4-Hydroxybutyl acrylate glycidyl ether
2-benzoyl-benzoic acid 3-(4-acryloyloxy-butoxy)-2-hydroxy-propyl ester
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In ISOPROPYLAMIDE; acetonitrile for 16h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In N,N-dimethyl acetamide; acetonitrile for 16h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In N,N-dimethyl acetamide; acetonitrile for 16h; Reflux; | 45.2 g |
2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid
4-Hydroxybutyl acrylate glycidyl ether
acrylic acid 4-{2-hydroxy-3-[2-(9-oxo-9H-thioxanthen-2-yloxy)-acetoxy]-propoxy}-butyl ester
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In ISOPROPYLAMIDE; acetonitrile for 16h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In acetonitrile for 16h; Reflux; | 1.8 g |
4-Hydroxybutyl acrylate glycidyl ether
acrylic acid 4-{2-hydroxy-3-[2-(9-oxo-9H-thioxanthen-2-yloxy)-propionyloxy]propoxy}-butyl ester
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In ISOPROPYLAMIDE; acetonitrile for 16h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In N,N-dimethyl acetamide; acetonitrile for 16h; Reflux; | 3.7 g |
9-oxo-9H-thioxanthen-1-carboxylic acid
4-Hydroxybutyl acrylate glycidyl ether
9-oxo-9H-thioxanthene-1-carboxylic acid-3-(4-acryloyloxy-butoxy)-2-hydroxy-propyl ester
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In dimethyl sulfoxide; acetonitrile for 24h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In dimethyl sulfoxide; acetonitrile for 24h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In dimethyl sulfoxide; acetonitrile for 24h; Reflux; | 2.6 g |
9-oxo-9H-thioxanthene-2-carboxylic acid
4-Hydroxybutyl acrylate glycidyl ether
9-oxo-9H-thioxanthene-2-carboxylic acid-3-(4-acryloyloxy-butoxy)-2-hydroxy-propyl ester
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In ISOPROPYLAMIDE; acetonitrile for 24h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In N,N-dimethyl acetamide; acetonitrile for 24h; Reflux; | |
With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide In N,N-dimethyl acetamide; acetonitrile for 24h; Reflux; | 2.5 g |