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120666-13-9

Basic Information
CAS No.: 120666-13-9
Name: 2,8,9-TRIMETHYL-2,5,8,9-TETRAAZA-1-PHOSPHABICYCLO[3.3.3]UNDECANE
Article Data: 6
Molecular Structure:
Molecular Structure of 120666-13-9 (2,8,9-TRIMETHYL-2,5,8,9-TETRAAZA-1-PHOSPHABICYCLO[3.3.3]UNDECANE)
Formula: C9H21 N4 P
Molecular Weight: 216.266
Synonyms: 2,8,9-Trimethyl-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane;Proazaphosphatrane
Density: g/cm3
Melting Point: 110-115 °C(lit.)
Boiling Point: 263.9°Cat760mmHg
Flash Point: 113.4°C
PSA: 26.55000
LogP: 0.08950
Synthetic route
685-83-6

bis(diethylamino)chlorophosphine

65604-89-9

tris[2-(methylamino)ethyl]amine

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
With potassium tert-butylate In acetonitrile 1) 1h, RT, 2) 1 h, RT;81%

2,8,9-Trimethyl-2,8,9-triaza-5-azonia-1λ5-phospha-tricyclo[3.3.3.01,5]undecane

A

C9H21(2)HN4P(1+)

B

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
With potassium tert-butylate In dimethylsulfoxide-d6 at 20℃;A 31%
B 69%
120710-16-9

2,8,9-Trimethyl-2,8,9-triaza-5-azonia-1λ5-phospha-tricyclo[3.3.3.01,5]undecane; chloride

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
With sodium hydroxide at 200℃;53%
65604-89-9

tris[2-(methylamino)ethyl]amine

1608-26-0

Hexamethylphosphorous triamide

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
In xylene Heating;
65604-89-9

tris[2-(methylamino)ethyl]amine

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 82 percent / ClP(NMe2)2, Et3N / CH2Cl2 / 1 h / Ambient temperature
2: 53 percent / NaOH / 200 °C
View Scheme

C(2)H3O(1-)*C9H21(2)HN4P(1+)

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran / Inert atmosphere
2: tetrahydrofuran / Inert atmosphere
View Scheme

2,8,9-trimethyl-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane

120666-13-9

proazaphosphatrane

Conditions
ConditionsYield
In tetrahydrofuran Inert atmosphere;
103-72-0

phenyl isothiocyanate

120666-13-9

proazaphosphatrane

C16H26N5PS

Conditions
ConditionsYield
In diethyl ether for 0.0833333h;100%
103-72-0

phenyl isothiocyanate

120666-13-9

proazaphosphatrane

C16H26N5PS

Conditions
ConditionsYield
In diethyl ether for 0.0833333h;100%
120666-13-9

proazaphosphatrane

111965-73-2

1-(azidomethyl)-4-vinylbenzene

861891-68-1

C18H30N5P

Conditions
ConditionsYield
In benzene for 12h; Heating / reflux;100%
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    Package:1, 5 g in glass bottle Application:2,8,9-Trimethyl-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane is involved as a reactant in:Studies of N-heterocyclic carbene ligand effects on metal hydride bond energies.Synthesis of heterogen...

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