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123-25-1

Basic Information
CAS No.: 123-25-1
Name: Diethyl succinate
Article Data: 208
Molecular Structure:
Molecular Structure of 123-25-1 (Diethyl succinate)
Formula: C8H14O4
Molecular Weight: 174.197
Synonyms: Butanedioicacid, diethyl ester (9CI);Succinic acid, diethyl ester (6CI,8CI);Butandioicacid diethyl ester;Diethyl butanedioate;
EINECS: 204-612-0
Density: 1.039 g/cm3
Melting Point: -20 °C
Boiling Point: 218.4 °C at 760 mmHg
Flash Point: 99.5 °C
Appearance: clear liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-24/25-22
PSA: 52.60000
LogP: 0.89280
Synthetic route
623-91-6

diethyl Fumarate

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With hexacarbonyl molybdenum; phenylsilane In tetrahydrofuran for 4.5h; Heating;100%
With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane; water In toluene at 80℃; for 24h; Catalytic behavior; Solvent; Temperature; Reagent/catalyst; Schlenk technique; Inert atmosphere;99%
With acetic acid; zinc for 0.5h; Ambient temperature; sonication;98%
1520-50-9

but-2-enedioic acid diethyl ester

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With 5% Pd/C; hydrogen In ethanol at 20℃; for 0.5h; chemoselective reaction;100%
With hydrogen In methanol at 24.84℃; under 760.051 Torr;
With silica gel supported sulfonic acid In acetonitrile at 20℃; Reagent/catalyst; Electrochemical reaction;75 %Spectr.
762-21-0

acetylenedicarboxylic acid diethyl ester

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethyl acetate at 80℃; under 2585.81 Torr; for 0.05h; microwave irradiation;99%
With magnesium chloride electrolysis: large surface area gold wire electrode; 150 W cm-2 ultrasound intensity; Yield given;
With water; zinc In tetrahydrofuran; methanol for 3h; Heating;100 % Spectr.
141-05-9

Diethyl maleate

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With acetic acid; zinc for 2h; Ambient temperature; sonication;98%
With Decaborane; palladium on activated charcoal In methanol at 25℃; for 0.3h; Reduction;98%
With 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-7-methylbenzo-[d]imidazole; [Zr(2,6-bis(5-methyl-3-phenyl-1H-pyrrol-2-yl)pyridine)2] In benzene-d6 for 8h; UV-irradiation;98%
64-17-5

ethanol

110-15-6

succinic acid

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With alumina methanesulfonic acid at 80℃; for 0.133333h; Microwave irradiation;97%
With Fe(SO4)3 * xH2O In toluene for 3h; Heating;95%
With N-dodecanoyl-N-methyl-1-glucamine In water at 45℃; for 6h; Green chemistry;87%
123-56-8

Succinimide

64-17-5

ethanol

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With chloro-trimethyl-silane at 40℃; for 5h;96%
With chloro-trimethyl-silane at 20 - 40℃; for 5h; Inert atmosphere;96%
144150-81-2

1,2-bis(ethoxycarbonyl)vinyl toluene-p-sulfonate

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With sodium tetrahydroborate; nickel dichloride In methanol ice-cooling;92%
141-05-9

Diethyl maleate

A

24766-10-7

diethyl 2-n-butylsuccinate

B

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With aluminium trichloride; lithium di-n-butylcuprate In diethyl ether at -65 - -40℃; for 1h;A 1.8%
B 92%
With lithium di-n-butylcuprate In diethyl ether at -65 - -40℃; for 1h; Product distribution; in the presence of AlCl3 as well; other solvents;A 1%
B 57%
1114-31-4

diethyl meso-2,3-dibromosuccinate

A

623-91-6

diethyl Fumarate

B

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
With sodium hydroxide; sodium tetrahydroborate; 1,2-di(thiophen-2-yl)ditelluride In ethanol; water at 5℃;A 90%
B n/a
64-17-5

ethanol

594815-54-0

C12H24O4Si

123-25-1

succinic acid diethyl ester

Conditions
ConditionsYield
Stage #1: C12H24O4Si With oxalyl dichloride; N,N-dimethyl-formamide
Stage #2: ethanol With pyridine
83%
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    Product Name: Diethyl succinate CAS: 123-25-1 MF: C8H14O4 MW: 174.19 EINECS: 204-612-0 Mol File: 123-25-1.mol Diethyl succinate Structure Diethyl succinate Chemical Properties Melting point -20 °C (lit.) Boiling point

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    Product name: Diethyl Succinate CAS No.:123-25-1 Molecule Formula:C8H14O4 Molecule Weight:174.19 Purity: 99.0% Package: 200kg/drum Description:Colorless or light yellow transparent oily liquid Manufacture Standards:Enterprise Standard

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Chemistry

IUPAC Name: Diethyl butanedioate
Synonyms of Diethyl succinate (CAS NO.123-25-1): Butanedioic acid, diethyl ester ; Diethyl ethanedicarboxylate ; Diethylester kyseliny jantarove ; Ethyl succinate
CAS NO: 123-25-1
Molecular Formula: C8H14O4
Molecular Weight: 174.20
Molecular Structure:
EINECS: 204-612-0 
H bond acceptors: 4
H bond donors: 0
Freely Rotating Bonds: 7
Polar Surface Area: 52.6 Å2
Melting point: -20°C
Boiling Point: 218.4 °C at 760 mmHg 
Flash Point: 99.5 °C 
Index of Refraction: 1.422 
Molar Refractivity: 42.66 cm
Molar Volume: 167.5 cm3 
Surface Tension: 32.4 dyne/cm 
Density: 1.039 g/cm
Enthalpy of Vaporization: 45.48 kJ/mol 
Vapour Pressure: 0.126 mmHg at 25°C 
Appearance: clear liquid
Product Categories of Diethyl succinate (CAS NO.123-25-1): Pharmaceutical Intermediates;Organics;SuccinicSeries;Fatty Acid Esters (Plasticizer);Functional Materials;Plasticizer;ester Flavor;Alpha Sort;D;Volatiles/ Semivolatiles;Plasticizers;Polymer Additives;Polymer Science;Alphabetical Listings;C-D;Flavors and Fragrances

Uses

 Diethyl succinate (CAS NO.123-25-1) is used as a food flavoring agent, solvent, organic synthesis intermediates, gas chromatography stationary phase,and it is also used in the plastics industry.

Production

  Diethyl succinate (CAS NO.123-25-1) is derived from the esterification of Succinic acid with Ethanol.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rat LD50 oral 8530mg/kg (8530mg/kg)   AMA Archives of Industrial Hygiene and Occupational Medicine. Vol. 4, Pg. 119, 1951.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Safety Information about Diethyl succinate (CAS NO.123-25-1):
Hazard Codes: IrritantXi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36-24/25-22 
S22: Do not breathe dust. 
S24/25: Avoid contact with skin and eyes. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 2
RTECS: WM7400000
HS Code: 29171990
Mildly toxic by ingestion. A skin and eye irritant. Combustible liquid. Reaction with ethyl trifluoroacetate + sodium hydride may cause a fire or explosion. When heated to decomposition it emits acrid smoke and irritating fumes. See also ESTERS.

Specification

General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear. Will burn if involved in a fire. Combustible liquid.
Extinguishing Media: Use agent most appropriate to extinguish fire. 
Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.
Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container.