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123910-88-3

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Basic Information
CAS No.: 123910-88-3
Name: 4-(4-Hydroxybutyl)benzoic acid Methyl ester
Article Data: 19
Molecular Structure:
Molecular Structure of 123910-88-3 (4-(4-Hydroxybutyl)benzoic acid Methyl ester)
Formula: C12H16O3
Molecular Weight: 208.257
Synonyms: METHYL4-(4-HYDROXYBUTYL)BENZOATE;Methyl 4-(4-hydroxybutyl)benzoate;4-(4-HYDROXYBUTYL)-BENZOIC ACID METHYL ESTER;4-(4-Hydroxybutyl)benzoic Acid Methyl Ester;
Density: 1.092±0.06 g/cm3(Predicted)
Boiling Point: 343.6±35.0 °C(Predicted)
PSA: 46.53000
LogP: 1.78820
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Synthetic route
123910-86-1

4-(4-hydroxy-1-butynyl)benzoic acid methyl ester

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethanol under 2585.7 Torr; for 12h;100%
With hydrogen; palladium on activated charcoal In methanol under 2327.17 - 2585.74 Torr; for 12h;100%
With palladium 10% on activated carbon; hydrogen In dichloromethane at 30℃; under 37503.8 Torr; Flow reactor;98%
106200-41-3

4-(4-carbomethoxyphenyl)butanal

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
With magnesium(II) perchlorate In methanol; acetonitrile at 20℃; for 3h;92%
619-42-1

4-methoxycarbonylphenyl bromide

7681-65-4

copper(I) iodide

927-74-2

1-butyn-4-ol

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
With triphenylphosphine; palladium(II) chloride In water; diethylamine75.8%
...Expand
67-56-1

methanol

79-37-8

oxalyl dichloride

863888-09-9

butyric acid 4-phenylbutyl ester

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
Stage #1: oxalyl dichloride; butyric acid 4-phenylbutyl ester With aluminum (III) chloride In dichloromethane at 0℃; for 4h;
Stage #2: methanol for 48h;		31%
Stage #1: oxalyl dichloride; aluminum (III) chloride In dichloromethane at 0℃; for 0.0833333h;
Stage #2: butyric acid 4-phenylbutyl ester In dichloromethane at 0℃; for 4h;
Stage #3: methanol for 48h; pH=2;		31%
...Expand
79-37-8

oxalyl dichloride

863888-09-9

butyric acid 4-phenylbutyl ester

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
Stage #1: oxalyl dichloride With aluminum (III) chloride In dichloromethane at 0℃; for 0.0833333h;
Stage #2: butyric acid 4-phenylbutyl ester In dichloromethane at 0℃; for 4h;		31%
147291-15-4

methyl 4-pent-4-enylbenzoate

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
With sodium tetrahydroborate; ozone 1.) MeOH, CH2Cl2, -78 deg C, 2.) MeOH, CH2Cl2, from -78 deg C to RT, overnight; Multistep reaction;
619-42-1

4-methoxycarbonylphenyl bromide

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 80 percent / diethylamine; triphenylphosphine; copper(I) iodide / palladium chloride / 20 °C
2: 100 percent / H2 / Pd/C / methanol / 12 h / 2327.17 - 2585.74 Torr
View Scheme
Multi-step reaction with 2 steps
1: 75.8 percent / triphenylphosphine, diethylamine, copper(I) iodide / palladium chloride / 18 h / Ambient temperature
2: 2.60 g / H2 / 5percent palladium-on-charcoal / ethanol / 12 h / 2585.7 Torr
View Scheme
Multi-step reaction with 2 steps
1: 76 percent / palladium chloride, triphenylphosphine, copper(I) iodide, diethylamine / 18 h / Ambient temperature
2: 100 percent / hydrogen / 5percent Pd/C / ethanol / 12 h / 2585.7 Torr
View Scheme
619-42-1

4-methoxycarbonylphenyl bromide

4-bromo-phenyl magnesium iodide

4-bromo-phenyl magnesium iodide

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) Mg, ZnBr2, 2.) (PPh3)4Pd / 1.) THF, 56 deg C, 18 h, 2.) THF, RT, 24 h
2: 1.) O3, 2.) NaBH4 / 1.) MeOH, CH2Cl2, -78 deg C, 2.) MeOH, CH2Cl2, from -78 deg C to RT, overnight
View Scheme
123910-86-1

4-(4-hydroxy-1-butynyl)benzoic acid methyl ester

A

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

B

106200-41-3

4-(4-carbomethoxyphenyl)butanal

Conditions
ConditionsYield
With hydrogen; palladium In ethanolA n/a
B 3.20 g (97%)
3360-41-6

4-phenyl-butan-1-ol

123910-88-3

methyl 4-(4-hydroxybut-1-yl)benzoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: dichloromethane / 36 h
2.1: aluminum (III) chloride / dichloromethane / 0.08 h / 0 °C
2.2: 4 h / 0 °C
View Scheme
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  • Yinghao Pharm Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-519-85390519

    Address:NO4,R&D Port,Changzhou Science&Education Town,18-50 Changwuzhong Road,Wujin Disctrict,Changhzou,Jiangsu

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    4-(4-Hydroxybutyl)benzoic acid Methyl ester

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    Aopharm is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in modes of

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     China (Mainland)  |  Contact Details

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    Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester

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    United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

    United Scientific Company (USC) Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. USC has both the expertise and flexibility

  • Shanghai united Scientific Co.,Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-53535353

    Address:28F No.900 huaihai Road Shanghai China

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  • Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester

  • Casno:

    123910-88-3

    Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester

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    Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

    Chungking Joyinchem Co.,Ltd is a specialized Chinese chemical supplier focusing on product R&D, manufacture and marketing. Our head office locates in Wulong district and the facto

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-23-77778019

    Address:No. 55, Longhu Road, Xiangkou Town, Wulong District, Chungking City, 408500, P.R China

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  • Casno:

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    Methyl 4-(4-hydroxybutyl)benzoate

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    Cool Pharm Ltd, found in 8995,is a high-tech enterprise which provides customer synthesis service for domestic and international pharmaceutical companies according to international standards. Our business includes research , development, process opti

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  • coolpharm Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-531-8233381 86-18678657237

    Address:Room 302,Building 1,Union Fortune Square, No. 2117,Tianchen Road,High-tech Zone,Jinan,Shandong,China

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  • 4-(4-Hydroxybutyl)benzoic acid Methyl ester/High quality/Best price/In stock

  • Casno:

    123910-88-3

    4-(4-Hydroxybutyl)benzoic acid Methyl ester/High quality/Best price/In stock

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    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

  • Taizhou volsen chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

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  • Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester

  • Casno:

    123910-88-3

    Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester

    Min.Order: 0

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    Benzoic acid, 4-(4-hydroxybutyl)-, methyl ester Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shan

    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-025-52181296

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  • 123910-88-3

  • Casno:

    123910-88-3

    123910-88-3

    Min.Order: 0

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    4-(4-Hydroxybutyl)benzoic acid Methyl ester/High quality/Best price/In stock Application:intermediate

    We are Hebei minshang biotechnology co. LTD., mainly deal in pharmaceutical intermediates and various chemicals. We are manufacturers and have our own factory. Products & Usage Ph

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18032092709

    Address:hebei

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  • Methyl 4-(4-hydroxybutyl)benzoate

  • Casno:

    123910-88-3

    Methyl 4-(4-hydroxybutyl)benzoate

    Min.Order: 0

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    1.We have rich experience in the development and production 2.Our factory is in Shanghai of China,We have convenient traffic conditions.3.We have advanced testing equipment and shipping line. Package:5g, 10g, 50g, 100g, 1kg Application:Pharmaceutical

    Shanghai fine pharma co., Ltd. is a professional enterprise with chemical reagents and fine chemical products development, development and trade. The company has a sound research a

  • Shanghai Run-Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-21-31576854/57171705 / 57171706

    Address:second floor, building 3, No.999, jiangyue Road, minghang District, Shanghai, China

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