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13078-80-3

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Basic Information
CAS No.: 13078-80-3
Name: 2-Chlorophenethylamine
Article Data: 20
Molecular Structure:
Molecular Structure of 13078-80-3 (2-Chlorophenethylamine)
Formula: C8H10ClN
Molecular Weight: 155.627
Synonyms: Phenethylamine,o-chloro- (6CI,7CI,8CI);2-(2-Aminoethyl)chlorobenzene;2-(2-Chlorophenyl)ethanamine;2-(2-Chlorophenyl)ethylamine;2-Chlorobenzeneethanamine;o-Chlorophenethylamine;o-Chlorophenylethylamine;
EINECS: 235-982-1
Density: 1.128 g/cm3
Melting Point: 145 °C
Boiling Point: 239.9 °C at 760 mmHg
Flash Point: 108.9 °C
Appearance: Clear colorless to yellow liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
Transport Information: UN 2735 8/PG 3
PSA: 26.02000
LogP: 2.54150
Related products
Synthetic route
52085-97-9

3-(2-chlorophenyl)propionyl chloride

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With sodium azide; acetone und Erwaermen des Reaktionsprodukts in Benzol, zuletzt unter Zusatz von wss.Salzsaeure;
134306-93-7

3-(2-chlorophenyl)propionamide

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With alkaline aqueous sodium hypobromite

cyano(2-chlorophenyl)methyl ethyl carbonate

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With hydrogenchloride; platinum Hydrogenation;
2856-63-5

2-Chlorophenylacetonitrile

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride; aluminium trichloride
With borane-THF In tetrahydrofuran at 0 - 20℃;
86423-60-1

Diethyl N-(2-o-chlorophenylethyl)phosphoramidate

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With hydrogenchloride at 80 - 85℃; for 1.5h; Yield given;
497-25-6

dimethylenecyclourethane

108-90-7

chlorobenzene

A

13078-80-3

2-(2-chlorophenyl)ethanamine

B

156-41-2

4-chlorophenylethylamine

C

CO2

CO2

Conditions
ConditionsYield
With aluminium trichloride for 12h; Heating; 2 equivalents of AlCl3; Yield given. Title compound not separated from byproducts;
...Expand
7647-01-0

hydrogenchloride

cyano(2-chlorophenyl)methyl ethyl carbonate

platinum

platinum

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
Hydrogenation;
...Expand

1-chloro-2-(2‘-nitrovinyl)benzene

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether Heating;
64-04-0

phenethylamine

A

13078-80-3

2-(2-chlorophenyl)ethanamine

B

156-41-2

4-chlorophenylethylamine

Conditions
ConditionsYield
With chlorine In tetrachloromethane at 25℃; Product distribution; Further Variations:; Solvents;
89-98-5

2-chloro-benzaldehyde

13078-80-3

2-(2-chlorophenyl)ethanamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether / Heating
View Scheme
Multi-step reaction with 2 steps
1: water
2: platinum; aq.-ethanolic hydrochloric acid / Hydrogenation
View Scheme
Multi-step reaction with 2 steps
1: ammonium acetate; acetic acid / 16 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: ammonium acetate / acetic acid / 0.67 h / Heating / reflux
2.1: lithium aluminium tetrahydride; sulfuric acid / tetrahydrofuran / 0.58 h / 0 - 10 °C / Heating / reflux
2.2: 0.5 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: ammonium acetate; acetic acid / Neat (no solvent); Heating / reflux
2.1: aluminium hydride / tetrahydrofuran / 0.08 h / 0 °C / Heating / reflux
2.2: 0.5 h / 0 - 20 °C / Alkaline aqueous solution
View Scheme
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