Detail of "13287-76-8"

CAS Number:
13287-76-8
Name:
Ethanol,2-[(4-nitrophenyl)thio]-
Molecular Structure:
Formula:
C₈H₉NO₃S
Molecular Weight:
199.227
Synonyms:
Ethanol,2-[(p-nitrophenyl)thio]- (7CI,8CI);2-Hydroxyethyl 4-nitrophenyl sulfide;2-Hydroxyethyl p-nitrophenyl sulfide;2-[(p-Nitrophenyl)thio]ethanol;4-Nitrophenyl 2-hydroxyethyl sulfide;
Density:
1.35 g/cm³
Melting Point:
60 °C
Boiling Point:
370.2 °C at 760 mmHg
Flash Point:
177.7 °C
Hazard Symbols:
Xi
Risk Codes:
36/37/38
Safety:
26-36/37/39 Details

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Aminophenyl b-hydroxyethyl sulfones: Aminophenyl b-hydroxyethyl sulfones. Kotera, Norio; Tada, Kazuhiro; Masaki, Shinzaburo; Goto, Kunihisa; Kaneoya, Tatsuo (Sumitomo Chemical Co., Ltd. , Japan). Eur. Pat. Appl. EP 92909 A2 2 Nov 1983, 34 pp. DESIGNATED STATES: R: CH, DE, FR, GB, IT, LI. (English). (European Patent Organization). CODEN: EPXXDW. CLASS: IC: C07C147-12; B01J027-20; B01J025-02; B01J023-74. 13287-76-8 and 5246-58-2 which are cas registry numbers of chemicals are mentioned. APPLICATION: EP 83-301683 25 Mar 1983. PRIORITY: JP 82-57483 6 Apr 1982; JP 82-57484 6 Apr 1982; JP 82-57485 6 Apr 1982; JP 82-57486 6 Apr 1982. DOCUMENT TYPE: Patent CA Section: 25 (Benzene, Its Derivatives, and Condensed Benzenoid Compounds) The etherification of HSCH2CH2OH by chloronitrobenzenes gave sulfides I, which were oxidized and subsequently reduced to yield aminophenyl sulfones II. Thus, 4-O2NC6H4Cl was treated with HSCH2CH2OH and NaOH, the 4-O2NC6H4SCH2CH2OH obtained was treated with H2O2 at 95% to yield 4-O2NC6H4SO2CH2CH2OH, and the latter was hydrogenated over Pd-C to give 4-H2NC6H4SO2CH2CH2OH. .