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1334513-02-8

Basic Information
CAS No.: 1334513-02-8
Name: N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester
Article Data: 26
Molecular Structure:
Molecular Structure of 1334513-02-8 (N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester)
Formula: C18H17F5NO5P
Molecular Weight: 453.302
Synonyms: L-Alanine, N-[(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-, 1-methylethyl ester; N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)Phenoxyphosphinyl]-L-Alanine 1-Methylethyl Ester; N-[(S)-(2,3,4,5,6-Penta fluorophenoxy)phenoxy phosphinyl]-L-alanine 1-methylethyl ester; Sofosbuvir Side Chain; N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-phenoxyphosphinyl]-L-alanine 1-methylethyl ester; N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine1-Methylethyl ester; N-((S)-(2,3,4,5,6-Pentafluoro Phenoxy) Phenoxy Phosphinyl)-L--Alanine-1-Methyl Ethyl Ester; n-((s)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl)-l-alanine1-methylethylester; (2s)-isopropyl-2-((perfluorophenoxyl)(phenoxy)phosphorylamino)Propanoate
EINECS: 695-076-0
Density: 1.405
Boiling Point: 442.6±55.0 °C(Predicted)
PSA: 83.67000
LogP: 5.26860
Synthetic route
771-61-9

2,3,4,5,6-pentafluorophenol

770-12-7

O-phenyl phosphorodichloridate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: 2,3,4,5,6-pentafluorophenol; O-phenyl phosphorodichloridate With triethylamine In chloroform at 0℃; under 11251.1 Torr;
Stage #2: alanine isopropyl ester hydrochloride In chloroform Temperature;
88%
Stage #1: alanine isopropyl ester hydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane at -68℃; for 0.5h;
Stage #2: O-phenyl phosphorodichloridate In dichloromethane at -10℃; for 0.5h;
Stage #3: 2,3,4,5,6-pentafluorophenol With N-ethyl-N,N-diisopropylamine In dichloromethane
78%
Stage #1: O-phenyl phosphorodichloridate; alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at -78 - 20℃; for 2h;
Stage #2: 2,3,4,5,6-pentafluorophenol With triethylamine In dichloromethane at -78 - 20℃; for 3h;
61.6%
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

2263-53-8

sodium pentafluorophenolate

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: phenyl(isopropoxy-L-alaninyl) phosphorochloridate; sodium pentafluorophenolate In tetrahydrofuran at -10℃;
Stage #2: With triethylamine In n-heptane; tert-butyl methyl ether pH=8;
66.81%
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

771-61-9

2,3,4,5,6-pentafluorophenol

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 4h;45.1%
With triethylamine In dichloromethane at 0℃; for 4h; Inert atmosphere;45.1%
17788-07-7

2,3,4,5,6-pentafluorophenyl dichlorophosphate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Stage #1: 2,3,4,5,6-pentafluorophenyl dichlorophosphate With triethylamine; phenol In dichloromethane at 20℃; for 0.5h;
Stage #2: alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at 0℃; for 1h;
261909-49-3

phenyl(isopropoxy-L-alaninyl) phosphorochloridate

771-61-9

2,3,4,5,6-pentafluorophenol

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;
With triethylamine In dichloromethane at -10 - 0℃; for 1.5h;A n/a
B n/a
With triethylamine In dichloromethane at -15 - 5℃; for 1h; Inert atmosphere;A n/a
B n/a
39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloromethane / 0.5 h / -10 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1.5 h / -10 - 0 °C
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / tert-butyl methyl ether / 2 h / -65 - -50 °C / Inert atmosphere; Cooling with acetone-dry ice
2: triethylamine / dichloromethane / 1 h / -15 - 5 °C / Inert atmosphere
View Scheme
770-12-7

O-phenyl phosphorodichloridate

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

1337529-56-2

(S)-2-[(S)-(2,3,4,5,6-pentafluoro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dichloromethane / 0.5 h / -10 °C / Inert atmosphere
2: triethylamine / dichloromethane / 1.5 h / -10 - 0 °C
View Scheme
771-61-9

2,3,4,5,6-pentafluorophenol

770-12-7

O-phenyl phosphorodichloridate

39613-92-8, 62062-56-0, 62062-65-1

alanine isopropyl ester hydrochloride

A

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

B

C18H17F5NO4P

Conditions
ConditionsYield
Stage #1: alanine isopropyl ester hydrochloride With triethylamine In dichloromethane at -70℃; for 0.75h;
Stage #2: O-phenyl phosphorodichloridate In dichloromethane at -70 - 0℃; for 8h;
Stage #3: 2,3,4,5,6-pentafluorophenol With triethylamine In dichloromethane at 0 - 20℃;
770-12-7

O-phenyl phosphorodichloridate

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: triethylamine / ethyl acetate / 1 h / -10 °C / Enzymatic reaction
1.2: 2.5 h / -5 - 25 °C
2.1: triethylamine / ethyl acetate; n-heptane / 4 - 8 h / Resolution of racemate
View Scheme
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 1.5 h / -60 - 25 °C / Inert atmosphere
2.1: tetrahydrofuran / -10 °C
2.2: pH 8
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 20 h / -70 - 20 °C
2: triethylamine / dichloromethane / 20 h / -5 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 1 h / -78 - 20 °C
2: triethylamine / dichloromethane / 4 h / 0 °C
View Scheme
39825-33-7

isopropyl L-alanine

1334513-02-8

(S)-2-[((S)-(2,3,4,5,6-pentafluorophenoxy)(phenoxy)phosphoryl)amino]propionic acid isopropyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: triethylamine / ethyl acetate / 1 h / -10 °C / Enzymatic reaction
1.2: 2.5 h / -5 - 25 °C
2.1: triethylamine / ethyl acetate; n-heptane / 4 - 8 h / Resolution of racemate
View Scheme
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    (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate

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  • Isopropyl N-[(pentafluorophenoxy)(phenoxy)phosphoryl]-L-alaninate  1334513-02-8

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    Isopropyl N-[(pentafluorophenoxy)(phenoxy)phosphoryl]-L-alaninate 1334513-02-8

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    1334513-02-8

    L-alanien,N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)- phenoxy-phosphinyl]-1-Methylethyl ester

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  • SF-1.2

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    SF-1.2

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    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

  •  Afine Chemicals Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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  • (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate

  • Casno:

    1334513-02-8

    (S)-isopropyl 2-(((S)-(perfluorophenoxy)(phenoxy)phosphoryl)amino)propanoate

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • Featured products N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester

  • Casno:

    1334513-02-8

    Featured products N-[(S)-(2,3,4,5,6-pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-Methylethyl ester

    Min.Order: 100 Gram

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    Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

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  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-189 8945 5137

    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

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  • Lower Price N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester

  • Casno:

    1334513-02-8

    Lower Price N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester

    Min.Order: 1 Kilogram

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    Product name: N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)-Phenoxy-Phosphinyl]-1-Methylethyl Ester CAS No.: 1334513-02-8 Molecule Formula:C18H17F5NO5P Molecule Weight:453.30 Purity: 99.0% Package: 25kg/drum Description:White powder Manufactu

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

  •  Siwei Development Group Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-82881840

    Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

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  • N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-methylethyl ester

  • Casno:

    1334513-02-8

    N-[(S)-(2,3,4,5,6-Pentafluorophenoxy)phenoxyphosphinyl]-L-alanine 1-methylethyl ester

    Min.Order: 1 Gram

    FOB Price:  USD $ 1.0-2.0

    Huarong Industrial Group Limited established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World.

    Hangzhou Huarong Pharm Co., Ltd. established since 2009 , has been always focusing on supplying products and services to our clients in the field of small molecule drug. Huarong

  •  Hangzhou Huarong Pharm Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-571-86758373

    Address:Room1707, 7Th Floor, Xin Chuanmei Industry Building , No.58 of Xintang Road, Jianggan District, Hangzhou, China.

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