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13405-60-2

Basic Information
CAS No.: 13405-60-2
Name: 1-Galloyl-glucose
Article Data: 12
Molecular Structure:
Molecular Structure of 13405-60-2 (1-Galloyl-glucose)
Formula: C13H16O10
Molecular Weight: 332.264
Synonyms: [(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl] 3,4,5-trihydroxybenzoate;
Density: 1.85g/cm3
Melting Point: 214℃
Boiling Point: 736.4°C at 760 mmHg
Flash Point: 278.9°C
PSA: 177.14000
LogP: -2.23990
Synthetic route
1195367-79-3

2,3,4,6-tetra-O-benzyl-1-(3’,4’,5’-tri-O-benzylgalloyl)-β-D-glucopyranose

13405-60-2

β-glucogallin

Conditions
ConditionsYield
With 20% palladium hydroxide-activated charcoal; hydrogen In tetrahydrofuran at 20 - 25℃; for 12h;96%
With palladium 10% on activated carbon; hydrogen In methanol; ethyl acetate under 2585.81 Torr; for 5h; Inert atmosphere;95%
2485-62-3

L-Cysteine methyl ester

A

141968-72-1

(R)-1,2,6-Trihydroxy-4,11-dioxo-4,8,9,11-tetrahydro-7H-5,12-dioxa-10-thia-7-aza-benzo[def]chrysene-8-carboxylic acid methyl ester

B

13405-60-2

β-glucogallin

Conditions
ConditionsYield
With ammonium formate In water; acetonitrile at 80℃;A 60%
B 74%

A

141968-72-1

(R)-1,2,6-Trihydroxy-4,11-dioxo-4,8,9,11-tetrahydro-7H-5,12-dioxa-10-thia-7-aza-benzo[def]chrysene-8-carboxylic acid methyl ester

B

13405-60-2

β-glucogallin

Conditions
ConditionsYield
With L-Cysteine methyl ester; ammonium formate In water; acetonitrile at 80℃;A 60%
B 74%
79814-54-3

1-galloyl-2,3,4,6-tetra-O-acetyl-β-D-glucopyranose

13405-60-2

β-glucogallin

Conditions
ConditionsYield
With methanol; sodium methylate
149-91-7

3,4,5-trihydroxybenzoic acid

hairy root cultures of Lobelia sessilifolia

hairy root cultures of Lobelia sessilifolia

A

gallic acid 3-O-β-D-glucopyranoside

gallic acid 3-O-β-D-glucopyranoside

B

13405-60-2

β-glucogallin

Conditions
ConditionsYield
In water for 96h;A 190 mg
B 230 mg

1486-47-1

3,4,5-tris(benzyloxy)benzoyl chloride

13405-60-2

β-glucogallin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere; Molecular sieve
1.2: 3.33 h / Inert atmosphere; Molecular sieve
2.1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 5 h / 2585.81 Torr / Inert atmosphere
View Scheme

1-O-(3,4,5-tribenzyloxybenzoyl)-β-D-glucopyranoside

13405-60-2

β-glucogallin

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; under 2585.81 Torr; for 4h;
With 10 wt% Pd(OH)2 on carbon; hydrogen In ethanol; acetone at 20℃; for 4h;
149-91-7

3,4,5-trihydroxybenzoic acid

13405-60-2

β-glucogallin

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere
2: thionyl chloride / dichloromethane
3: dichloromethane / 72 h / Inert atmosphere
4: perchloric acid; silica gel / acetonitrile / 24 h
5: hydrogen; palladium 10% on activated carbon / ethanol / 4 h / 20 °C / 2585.81 Torr
View Scheme
1486-48-2

3,4,5-tribenzyloxybenzoic acid

13405-60-2

β-glucogallin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: thionyl chloride / dichloromethane
2: dichloromethane / 72 h / Inert atmosphere
3: perchloric acid; silica gel / acetonitrile / 24 h
4: hydrogen; palladium 10% on activated carbon / ethanol / 4 h / 20 °C / 2585.81 Torr
View Scheme
1486-47-1

3,4,5-tris(benzyloxy)benzoyl chloride

13405-60-2

β-glucogallin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dichloromethane / 72 h / Inert atmosphere
2: perchloric acid; silica gel / acetonitrile / 24 h
3: hydrogen; palladium 10% on activated carbon / ethanol / 4 h / 20 °C / 2585.81 Torr
View Scheme
Multi-step reaction with 2 steps
1: N,N,N,N,-tetramethylethylenediamine / dichloromethane / 48 h / Reflux
2: hydrogen; 20% palladium hydroxide-activated charcoal / tetrahydrofuran / 12 h / 20 - 25 °C
View Scheme
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    Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

  • Chemical Co.Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • Beta-Glucogallin

  • Casno:

    13405-60-2

    Beta-Glucogallin

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

       Inquiry Now

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