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13470-13-8

Basic Information
CAS No.: 13470-13-8
Name: TUNGSTEN TETRACHLORIDE
Article Data: 33
Molecular Structure:
Molecular Structure of 13470-13-8 (TUNGSTEN TETRACHLORIDE)
Formula: Cl4W
Molecular Weight: 325.662
Synonyms: Tungstenchloride (WCl4) (6CI,7CI,8CI); Tetrachlorotungsten; Tungsten tetrachloride;Tungstenyl tetrachloride
Density: 4,624 g/cm3
Melting Point: decomposes [CRC10]
Boiling Point: °Cat760mmHg
Flash Point: °C
Appearance: Black Conforms to Requirement
Hazard Symbols: CorrosiveC
Risk Codes: R34
Safety: S26-27-28-36/37/39-45
Transport Information: UN 3260 8
PSA: 0.00000
LogP: 2.75800
Synthetic route
7647-01-0

hydrogenchloride

tungstic acid

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
strong HCl;100%
strong HCl;100%
13283-01-7

tungsten(VI) chloride

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
With Sn In 1,2-dichloro-ethane byproducts: SnCl4; absence of air and moisture; stirring with Sn-powder at room temp. for 17 h, then at 80-90°C for 2 d; centrifugation, washing (CH2Cl2), drying (vac., room temp.); elem. anal.;98%
With Sb In neat (no solvent) byproducts: SbCl3, WOCl4, WCl5; absence of air and moisture; sealed evacuated glass tube, 75-80°C(12 h), 105°C (12 h), 130°C (12 h); distn. off of byproducts (130°C, 1d; then 160°C, 1 d; then215°C, 1 d); elem. anal.;97%
With red phosphorus In neat (no solvent) byproducts: PCl3, WOCl4, WCl5; absence of air and moisture; sealed evacuated glass tube, slow heating to 200°C (over 12 h), then to 300°C (over further 12 h); sublimation off of byproducts (230-240°C, 1 d, trap at liquid N2-temp.; further byproduct: POCl3); elem. anal.;94%

phosphorous

13283-01-7

tungsten(VI) chloride

A

W4PCl11

B

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) byproducts: PCl3; WCl6 and red P (1:1.34) mixed (Ar), sealed (vac.) in silica tube, heatedat 500°C for 24 h; sublimated, XRD;A 95%
B 5%
13283-01-7

tungsten(VI) chloride

7440-33-7

tungsten

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃; for 17h;93%
7647-01-0

hydrogenchloride

7446-70-0

aluminium trichloride

13283-01-7

tungsten(VI) chloride

7429-90-5

aluminium

7647-14-5

sodium chloride

A

W6Cl8(4+)*4Cl(1-)*7H2O=[W6Cl8]Cl4*7H2O

B

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In neat (no solvent, solid phase) other Radiation; sealing WCl6, Al, AlCl3 and NaCl and Mo into SiO2 ampoule (1E-2 Torr N2), microwave oven (200 W, 60 min, cooling to room temp., further irradiation at 200 W for 60 min), opening, dissoln. in hot concd. HCl; filtration (Celite), crystn. on cooling, washing (cold. concd. HCl, Et2O), drying (overnight); elem. anal.;A 48%
B n/a
13283-01-7

tungsten(VI) chloride

7440-33-7

tungsten

A

13520-78-0, 160797-03-5

tungsten(VI) oxychloride

B

tungsten dichloride

C

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
reaction of WCl6 with W at 270-750°C for 14 h under a vacuum; removal of WCl4 and WOCl4 byproducts by sublimation, intermediate (H3O)2W6Cl14*6H2O obtained after recrystn. from boiling HCl and cooling to -10°C; intermediate heated at 450°C under a dynamic vacuum;A n/a
B 25%
C n/a
56-23-5

tetrachloromethane

tungsten(IV) oxide

A

tungsten(VI) oxychloride

B

13283-01-7

tungsten(VI) chloride

C

13470-13-8

tungsten(IV) chloride

D

13520-76-8

tungsten dioxydichloride

Conditions
ConditionsYield
In neat (no solvent) reaction on heating WO2 with CCl4 to 250°C in a closed tube for 8h;;
In neat (no solvent) reaction on heating WO2 with CCl4 to 250°C in a closed tube for 8h;;
13283-01-7

tungsten(VI) chloride

A

7782-50-5

chlorine

B

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In gas Kinetics; Irradiation (UV/VIS); stationary photolysis in a glass cell; flash photolysis in a sealed quartz cell; vac. distn.;
1333-74-0

hydrogen

13283-01-7

tungsten(VI) chloride

A

13470-14-9

tungsten(V) chloride

B

7782-50-5

chlorine

C

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In gas Kinetics; byproducts: HCl; Irradiation (UV/VIS); flash photolysis in a sealed quartz cell at 388 K and 403 K; stationaryphotolysis in a sealed glass cell at 140°C; vac. distn.;
13283-01-7

tungsten(VI) chloride

7429-90-5

aluminium

13470-13-8

tungsten(IV) chloride

Conditions
ConditionsYield
In neat (no solvent) sealed ampoule (270-280 °C, 15 h), molar ratio WCl6:Al = 1:1.5;
In neat (no solvent, solid phase) reaction in glass ampules at 400°C;
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    CAS: [13470-13-8] Molecular Weight: FW:325.66

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