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13597-92-7

Basic Information
CAS No.: 13597-92-7
Name: 2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine
Article Data: 15
Molecular Structure:
Molecular Structure of 13597-92-7 (2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine)
Formula: H12N9 P3
Molecular Weight: 231.077
Synonyms: 1,3,5,2,4,6-Triazatriphosphorine,2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro- (7CI,8CI,9CI); Phosphonitrileamide, trimer (6CI);2,2,4,4,6,6-Hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine;Hexaamidocyclotriphosphazine; Hexaaminocyclotriphosphazene;Hexaaminotriazatriphosphorine; NSC 202892; Phosphazene trimer; Phosphonitrileamide, cyclic trimer; Phosphonitrilic hexaamide; Trimer phosphonitrile amide;Triphosphonitrilamide; Triphosphorus trinitridehexamide
Density: 3.83g/cm3
PSA: 222.63000
LogP: 2.09940
Synthetic route
940-71-6

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

7664-41-7

ammonia

A

13597-92-7

hexaaminocyclotriphosphazene

B

ammonium chloride

Conditions
ConditionsYield
In neat (no solvent) direct react. of (PNCl2)3 with a large excess of liquid NH3 under pressure; react. completed after 48 h;;A 36%
B n/a
In neat (no solvent) direct react. of (PNCl2)3 with a large excess of liquid NH3 under pressure; react. completed after 48 h;;A 36%
B n/a
In benzene passing gaseous NH3 in a soln. of (NPCl2)3 in C6H6 for a longer period of time; formation of a mixt. of P3N3(NH2)6 and NH4Cl;;
10026-13-8, 874483-75-7

phosphorus pentachloride

7664-41-7

ammonia

A

13597-92-7

hexaaminocyclotriphosphazene

B

ammonium chloride

Conditions
ConditionsYield
In chloroform addn. of a soln. of PCl5 in CHCl3 to an excess of liquid NH3 at -50 °C;; extraxtion with liquid NH3;;
In chloroform addn. of a soln. of PCl5 in CHCl3 to an excess of liquid NH3 at -50 °C;; extraxtion with liquid NH3;;
10026-13-8, 874483-75-7

phosphorus pentachloride

7664-41-7

ammonia

A

phospham

B

13597-92-7

hexaaminocyclotriphosphazene

C

6954-20-7

P4N12H16

Conditions
ConditionsYield
In not given react. of PCl5 with NH3;;
10026-13-8, 874483-75-7

phosphorus pentachloride

7664-41-7

ammonia

A

13597-92-7

hexaaminocyclotriphosphazene

B

6954-20-7

P4N12H16

Conditions
ConditionsYield
In not given react. of PCl5 with NH3; formation of P4N4(NH2)8 and P3N3(NH2)6 as decompn. products of intermediate P(NH2)5;;
In not given react. of PCl5 with NH3; formation of an excess of P3N3(NH2)6, P4N4(NH2)8 and higher polymers as decompn. products of intermediate P(NH2)5;;
In not given react. of PCl5 with NH3; formation of P4N4(NH2)8 and P3N3(NH2)6 as decompn. products of intermediate P(NH2)5;;
In not given react. of PCl5 with NH3; formation of an excess of P3N3(NH2)6, P4N4(NH2)8 and higher polymers as decompn. products of intermediate P(NH2)5;;
940-71-6

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

7664-41-7

ammonia

13597-92-7

hexaaminocyclotriphosphazene

hexakis(amino)cyclotriphosphazene hemiammoniate

13597-92-7

hexaaminocyclotriphosphazene

Conditions
ConditionsYield
With KNH2 In ammonia NH3 (liquid); High Pressure; react. of semi ammoniate and KNH2 (molar ratio 1:12), 130°C, 110 bar, 5d;
13597-92-7

hexaaminocyclotriphosphazene

154267-29-5

P3N6O3H9

Conditions
ConditionsYield
In water hydrolysis;;
In water hydrolysis;;
13597-92-7

hexaaminocyclotriphosphazene

phospham

Conditions
ConditionsYield
In neat (no solvent) heating in vac. at 380°C for 100 h;;>99
In neat (no solvent) heating for a longer period of time;;
In neat (no solvent) heating in vac. at 220°C for several days;;>99
13597-92-7

hexaaminocyclotriphosphazene

A

phospham

B

7664-41-7

ammonia

Conditions
ConditionsYield
In neat (no solvent) evolution of NH3 on air starting at 125 °C;;
In neat (no solvent) heating; decompn. rate depending on material of the vessel;;
In neat (no solvent) evolution of NH3 on air starting at 125 °C;;
In neat (no solvent) heating in vacuum at 380 °C for 100 h; evolution of NH3 starting in vacuum at 40 °C; evolution of a large amount of NH3 at 200-300 °C; no evolution of NH3 at 400-450 °C;;
13597-92-7

hexaaminocyclotriphosphazene

86119-84-8, 7664-38-2

phosphoric acid

Conditions
ConditionsYield
With HNO3 or acetic acid; H2O In water hydrolysis with acetic acid or diluted HNO3;;
With H2O In water hydrolysis in the heat;;
Downstream Products
7664-41-7
7664-38-2
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