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13716-10-4

Basic Information
CAS No.: 13716-10-4
Name: Di-tert-butylchlorophosphane
Article Data: 21
Molecular Structure:
Molecular Structure of 13716-10-4 (Di-tert-butylchlorophosphane)
Formula: C8H18ClP
Molecular Weight: 180.658
Synonyms: Phosphinouschloride, bis(1,1-dimethylethyl)- (9CI);Phosphinous chloride, di-tert-butyl-(7CI,8CI);Bis(1,1-dimethylethyl)phosphinous chloride;Bis(tert-butyl)chlorophosphine;Bis(tert-butyl)phosphinous chloride;Chlorodi-tert-butylphosphine;Di-tert-Butylphosphinous chloride;Di-tert-butylchlorophosphine;Di-t-butylchlorophosphine;
EINECS: 237-266-4
Density: 0.951 g/mL at 25 °C(lit.)
Melting Point: 2-3 °C
Boiling Point: 191.6 °C at 760 mmHg
Flash Point: 61.1 °C
Appearance: Colorless to light yellow liquid
Hazard Symbols: CorrosiveC
Risk Codes: 34
Safety: 26-36/37/39-45-25
Transport Information: UN 3265 8/PG 2
PSA: 13.59000
LogP: 4.21910
Synthetic route
5995-06-2

tetra-tert-butyldiphosphane

13716-10-4

di(tert-butyl)chlorophosphine

Conditions
ConditionsYield
With Dichlorophenylphosphine for 2h;83%
819-19-2

di-tert-butylphosphine

13716-10-4

di(tert-butyl)chlorophosphine

Conditions
ConditionsYield
With n-octyl trichloroacetate at 70 - 84℃; for 0.666667h; Product distribution / selectivity;78.2%
With tetrachloromethane at 20℃; for 48h; also at 100 deg C, 30 min.; Yield given;
677-22-5

tert-butylmagnesium chloride

13716-10-4

di(tert-butyl)chlorophosphine

Conditions
ConditionsYield
With phosphorus trichloride In diethyl ether for 0.5h; Heating;60%
With phosphorus trichloride In diethyl ether
With phosphorus trichloride In diethyl ether at 20℃; Inert atmosphere; Schlenk technique;
507-20-0

tertiary butyl chloride

13716-10-4

di(tert-butyl)chlorophosphine

Conditions
ConditionsYield
Stage #1: tertiary butyl chloride With magnesium In diethyl ether at 20℃; Inert atmosphere; Schlenk technique;
Stage #2: With phosphorus trichloride In diethyl ether at -40℃; Inert atmosphere; Schlenk technique;
50%
Stage #1: tertiary butyl chloride With magnesium In diethyl ether at 20℃; Inert atmosphere; Schlenk technique;
Stage #2: With phosphorus trichloride In diethyl ether at -40℃; Inert atmosphere; Schlenk technique;
50%
(i) Mg, Et2O, (ii) PCl3; Multistep reaction;
56-23-5

tetrachloromethane

131551-72-9

2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one

A

13716-10-4

di(tert-butyl)chlorophosphine

B

131551-83-2

tert-butylpivaloylphosphinic acid chloride

C

131551-82-1

tert-butylpivaloylphosphinic acid chloride

D

131551-85-4

1-(tert-Butyl-trichloromethyl-phosphanyl)-2-methyl-propan-1-one

Conditions
ConditionsYield
at 20℃; for 48h;
56-23-5

tetrachloromethane

131551-72-9

2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one

A

13716-10-4

di(tert-butyl)chlorophosphine

B

131551-82-1

tert-butylpivaloylphosphinic acid chloride

C

131551-85-4

1-(tert-Butyl-trichloromethyl-phosphanyl)-2-methyl-propan-1-one

D

125325-14-6

Di-tert-butyl(trichloromethyl)phosphine

Conditions
ConditionsYield
at 20℃; for 48h;
119522-06-4

Di-tert-butylphosphine

A

127-18-4

1,1,2,2-tetrachloroethylene

B

13716-10-4

di(tert-butyl)chlorophosphine

C

1071-38-1

N,N,N',N'-Tetramethylformamidinium chloride

Conditions
ConditionsYield
With tetrachloromethane In diethyl ether at 20℃; for 48h;
3282-30-2

pivaloyl chloride

131551-72-9

2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one

A

13716-10-4

di(tert-butyl)chlorophosphine

B

131551-83-2

tert-butylpivaloylphosphinic acid chloride

C

66199-86-8

di-tert-butylpivaloylphosphine

D

131551-84-3

1-(tert-Butyl-isobutyryl-phosphanyl)-2,2-dimethyl-propan-1-one

Conditions
ConditionsYield
at 20℃; for 48h;
92387-43-4

<(di-tert-butylphosphino)(trimethylsilyl)amino>lithium

13716-10-4

di(tert-butyl)chlorophosphine

Conditions
ConditionsYield
With phosphorus trichloride In diethyl ether; hexane at 20℃;
131551-72-9

2-Methyl-1-(1,2,2-tri-tert-butyl-diphosphanyl)-propan-1-one

A

13716-10-4

di(tert-butyl)chlorophosphine

B

131551-83-2

tert-butylpivaloylphosphinic acid chloride

C

66199-86-8

di-tert-butylpivaloylphosphine

D

131551-84-3

1-(tert-Butyl-isobutyryl-phosphanyl)-2,2-dimethyl-propan-1-one

Conditions
ConditionsYield
With pivaloyl chloride at 20℃; for 48h;
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    CAS No.: 13716-10-4 Molecular formula: C8H18ClP Molecular weight: 180.66 EINECS number: Related Categories: Chlorophosphines; Ligand; Catalysis and Inorganic Chemistry; Phosphorus Compounds; Phosphorus Precursors; Phosphines; Phosphine Compou

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    roduct Name: Di-tert-butylchlorophosphane CAS: 13716-10-4 MF: C8H18ClP MW: 180.66 EINECS: Mol File: 13716-10-4.mol Di-tert-butylchlorophosphane Structure Di-tert-butylchlorophosphane Chemical Properties Melting point 2-3°

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  • 13716-10-4  CAS NO.13716-10-4

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    13716-10-4

    13716-10-4 CAS NO.13716-10-4

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Chemistry

Molecule structure of Phosphinous chloride,P,P-bis(1,1-dimethylethyl)- (CAS NO.13716-10-4):

IUPAC Name: Ditert-butyl(chloro)phosphane
Molecular Weight: 180.655281 [g/mol]
Molecular Formula: C8H18ClP
XLogP3-AA: 2.7
Rotatable Bond Count: 2
Exact Mass: 180.083465
MonoIsotopic Mass: 180.083465 
Melting Point: 2-3 °C
Flash Point: 61.1 °C
Enthalpy of Vaporization: 41.03 kJ/mol
Boiling Point: 191.6 °C at 760 mmHg
Vapour Pressure: 0.71 mmHg at 25 °C
Canonical SMILES: CC(C)(C)P(C(C)(C)C)Cl
InChI: InChI=1S/C8H18ClP/c1-7(2,3)10(9)8(4,5)6/h1-6H3
InChIKey: MCRSZLVSRGTMIH-UHFFFAOYSA-N
Product Categories: Chlorophosphines; Ligand; Catalysis and Inorganic Chemistry; Phosphorus Compounds; Phosphorus Precursors; Phosphines

Uses

 Phosphinous chloride,P,P-bis(1,1-dimethylethyl)- (CAS NO.13716-10-4) is mainly used for asymmetric coupling of the ligand complex catalyst.

Safety Profile

Hazard Codes: CorrosiveC
Risk Statements: 34
R34:Causes burns.
Safety Statements: 26-36/37/39-45-25
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection. 
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) 
S25:Avoid contact with eyes.
RIDADR: UN 3265 8/PG 2
WGK Germany: 3
HazardClass: 8
PackingGroup: II

Specification

 Phosphinous chloride,P,P-bis(1,1-dimethylethyl)- (CAS NO.13716-10-4) is also called Phosphinous chloride, bis(1,1-dimethylethyl)- ; Di-tert-butylchlorophosphane ; Bis(1,1-dimethylethyl)-phosphinous chloride .