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13780-57-9

Basic Information
CAS No.: 13780-57-9
Name: SULPHUR CHLOROPENTAFLUORIDE
Article Data: 12
Molecular Structure:
Molecular Structure of 13780-57-9 (SULPHUR CHLOROPENTAFLUORIDE)
Formula: ClF5 S
Molecular Weight: 162.511
Synonyms: Sulfurchloride fluoride (SClF5) (6CI,7CI); Chloropentafluorosulfur;Monochloropentafluorosulfur; Pentafluorosulfur chloride; Sulfur chloridepentafluoride; Sulfur monochloride pentafluoride; Sulfur pentafluoride chloride
Melting Point: -64°C
Boiling Point: -21°C
Hazard Symbols:
Risk Codes: 23-34
Safety: Poison by inhalation. An irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of Cl, F, and SOx. See also FLUORIDES.
PSA: 25.30000
LogP: 3.43870
Synthetic route
13997-90-5

chlorine fluorosulfate

7783-60-0

sulfur tetrafluoride

A

13780-57-9

pentafluorosulfanyl chloride

B

88548-61-2

trifluorosulfonium fluorosulfate

Conditions
ConditionsYield
In neat (no solvent) ClOSO2F trasferred under vac. to FEP reactor fitted with stainless-steel valve and held at -196°C, SF4 condensed, reactor placed in bath at -90°C and allowed to warm to -40°C for 4 h; reactor cooled to -70°C, volatile materials(SF5Cl) removed, reactor warmed to -40°C and then - to 23°C and held under dynamic vac. for 10 min;A 77%
B 38%

potassium fluoride

87-90-1

trichloroisocyanuric acid

A

640723-20-2, 2699-79-8, 12769-73-2

fluorosulfonyl fluoride

B

13780-57-9

pentafluorosulfanyl chloride

C

7783-42-8

thionyl fluoride

Conditions
ConditionsYield
In acetonitrile at 20℃; Inert atmosphere; Darkness; Sealed tube;A n/a
B 47%
C n/a
7790-91-2

chlorine trifluoride

7783-60-0

sulfur tetrafluoride

13780-57-9

pentafluorosulfanyl chloride

Conditions
ConditionsYield
In neat (no solvent) between 100 - 350°C under exclusion of water at 3 atm;;
In neat (no solvent) between 100 - 350°C under exclusion of water at 3 atm;;
7783-60-0

sulfur tetrafluoride

7790-89-8

chlorine monofluoride

13780-57-9

pentafluorosulfanyl chloride

Conditions
ConditionsYield
In neat (no solvent) at 100 - 300°C and 3 atm;;
In gaseous matrix Kinetics; Irradiation (UV/VIS); photochemical reaction (Ar laser, mean power 10 mW, 450-500 nm, 100 Torr xenon as buffer gas); not isolated; IR monitoring;
In neat (no solvent) at 100 - 300°C and 3 atm;;
5714-22-7

disulfur decafluoride

13780-57-9

pentafluorosulfanyl chloride

Conditions
ConditionsYield
With chlorine In neat (no solvent) passing Cl2 and S2F10 through tube at 350°C;;
With chlorine In neat (no solvent) passing Cl2 and S2F10 through tube under reduced pressure;;>99
10025-67-9

disulfur dichloride

22650-46-0

F5SNCl2

A

13780-57-9

pentafluorosulfanyl chloride

B

25502-15-2

SF5N=SCl2

Conditions
ConditionsYield
In further solvent(s) Cl2S2 is placed in a FEP-trap (dry-box), evacuated and cooled to -196°C, CFCl3 is condensed into trap, mixt. is warmed to room temp., into this mixt. Fe5SNCl2 is condensed (liquid N2), cooling to -100°C, mixt. is allowed to warm; mixt. is stirred under warming to -20°C for several hours, sepn.by fractional condensation in oil vac. in cold traps at -45, -50, -196°C, react. is followed by Raman-spectroscopy;
60563-08-8

dichlorodithionitronium hexafluoroarsenate

7790-89-8

chlorine monofluoride

A

13780-57-9

pentafluorosulfanyl chloride

B

30313-36-1

{SF3}(1+)*{AsF6}(1-)=SF3AsF6

C

difluoro-dithionitronium hexafluoroarsenate(V)

D

7783-60-0

sulfur tetrafluoride

E

7783-42-8

thionyl fluoride

Conditions
ConditionsYield
With fluorosulfonylchloride In not given SO2ClF and ClF were condensed onto (SCl)2NAsF6, mixt. was warmed to room temp. with srirring, 5 h; volatiles were removed, products were not isolated; products were analized by IR;A n/a
B n/a
C 0%
D n/a
E <1

potassium fluoride

87-90-1

trichloroisocyanuric acid

7704-34-9

sulfur

13780-57-9

pentafluorosulfanyl chloride

Conditions
ConditionsYield
With trifluoroacetic acid In acetonitrile at 20℃; for 14h; Inert atmosphere;
13780-57-9

pentafluorosulfanyl chloride

22650-46-0

F5SNCl2

100312-09-2

tris(pentafluorosulfanyl)amine

Conditions
ConditionsYield
In water at 20℃; under 1.50015 Torr; for 3.5h; UV-irradiation;94%
13780-57-9

pentafluorosulfanyl chloride

22675-70-3

pentafuorosulfanyl hypochlorite

42310-84-9

bis(pentafluorosulfur)oxide

Conditions
ConditionsYield
byproducts: SO2F2, SOF4, SF6; Irradiation (UV/VIS); irradn. for 4 h at 22°C; collection in a -196°C trap (dynamic vacuum); fractional condensation; SF5OSF5 and SF5O2SF5 in -111°C trap; mixt. heated in copper reactor at 237°C for 2.5 h;; fractional condensation yielded SF5OSF5 in a -118°C trap; further compounds (from decompn. of SF5O2SF5) in -196°C trap;;72%
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Chemistry

Product Name: Sulphur chloropentafluoride
Synonyms:Chloropentafluorosulfur ; Monochloropentafluorosulfur ; Pentafluorosulfurchloride ; SClF5 ; SF5Cl ; Silfur chloropentafluoride ; Sulfur chloride fluoride ; Sulfur chloride fluoride (SClF5).
CAS: 13780-57-9
Molecular Formula of Sulphur chloropentafluoride (13780-57-9) : ClF5S
Molecular Weight of Sulphur chloropentafluoride (13780-57-9) : 162.51
Molecular Struture of Sulphur chloropentafluoride (13780-57-9) :
EINECS: 237-431-0
Product Categories:
Mol File: 13780-57-9.mol
Melting point: -64°C
Boiling point: -21°C

Toxicity Data With Reference

1.    

ihl-rat LCLo:100 ppm/1H

    BJIMAG    British Journal of Industrial Medicine. 27 (1970),1.

Safety Profile

Hazard Codes  T
Risk Statements  23-34
23:  Toxic by inhalation 
34:   Sulphur chloropentafluoride (13780-57-9) causes burns 
Safety Statements  26-36/37/39-45
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) 
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection  
RIDADR  3308
Hazard Note  Toxic

Standards and Recommendations

OSHA PEL: TWA 2.5 mg(F)/m3
ACGIH TLV: TWA 2.5 mg(F)/m3; BEI: 3 mg/g creatinine of fluorides in urine prior to shift; 10 mg/g creatinine of fluorides in urine at end of shift.
NIOSH REL: (Inorganic Fluorides) TWA 2.5 mg(F)/m3