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13818-44-5

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Basic Information
CAS No.: 13818-44-5
Name: 2-Propenoic acid, 2-methyl-, (2-oxo-1,3-dioxolan-4-yl)methyl ester
Article Data: 70
Molecular Structure:
Molecular Structure of 13818-44-5 (2-Propenoic acid, 2-methyl-, (2-oxo-1,3-dioxolan-4-yl)methyl ester)
Formula: C8H10O5
Molecular Weight: 186.164
Synonyms: 2-methyl-acrylic acid 2-oxo-[1,3]dioxolan-4-ylmethyl ester;(2-oxo-1,3-dioxolane-4-yl)methylmethacrylate;1-methacrylate-2,3-propylene carbonate;2-Propenoic acid,2-methyl-,(2-oxo-1,3-dioxolan-4-yl)methyl ester;4-(methacryloyloxymethyl)-1,3-dioxolan-2-one;
Density: 1.219g/cm3
Boiling Point: 337.576oC at 760 mmHg
Flash Point: 152.15oC
PSA: 61.83000
LogP: 0.64110
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Conditions
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With 1-methyl-1-N-propylpyrrolidinium bromide; triflate salt of a tricarbonyl rhenium(I) bipyridine complex at 80℃; under 11251.1 Torr; for 1h;99%
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Conditions
ConditionsYield
Stage #1: methacrylic acid methyl ester With zirconium(IV) acetylacetonate; water; 4-methoxy-phenol Reflux; Large scale;
Stage #2: 4-hydroxymethyl-1,3-dioxolan-2-one at 70 - 105℃; Large scale;		90.1%
With TEMPOL; zirconium(IV) acetylacetonate Product distribution / selectivity; Heating / reflux;80.6%
With TEMPOL; lithium hydroxide; calcium oxide Product distribution / selectivity; Heating / reflux;79.6%
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Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 3h; Cooling with ice;67%
Stage #1: 4-hydroxymethyl-1,3-dioxolan-2-one With dmap; dicyclohexyl-carbodiimide In dichloromethane for 0.5h; Cooling with ice;
Stage #2: poly(methacrylic acid) In dichloromethane at 20℃; Cooling with ice;		67%
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Conditions
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With triethylamine In dichloromethane
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methacrylic acid methyl ester

A

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acetic acid methyl ester

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13818-44-5

(2-oxo-1,3-dioxolane-4-yl)methyl methacrylate

Conditions
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sodium methylate at 75 - 110℃; Product distribution / selectivity;
...Expand
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(2-oxo-1,3-dioxolane-4-yl)methyl methacrylate

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Conditions
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at 20℃;100%
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Conditions
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With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane; water In toluene at 80℃; for 24h; Schlenk technique; Inert atmosphere;93%
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polymer; monomer(s): 2-methyl-acrylic acid 2-oxo-[1,3]-dioxolan-4-ylmethyl ester

Conditions
ConditionsYield
With methanesulfonic acid; 2,2-dimethoxy-2-phenylacetophenone at 25℃; for 0.0833333h; UV-irradiation;
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Conditions
ConditionsYield
at 20 - 66℃; for 168h;
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