Detail of "13922-41-3"

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CAS Number:
13922-41-3
Name:
Boronic acid,B-1-naphthalenyl-
Superlist Name:
1-Naphthaleneboronic acid
Molecular Structure:
Formula:
C₁₀H₉BO₂
Molecular Weight:
171.99
Synonyms:
NSC78936;a-Naphthaleneboronic acid;a-Naphthylboronic acid;1-Naphthylboric acid;1-Naphthaleneboronicacid (6CI,7CI,8CI);Boronic acid, 1-naphthalenyl- (9CI);(1-Naphthalenyl)boronic acid;
Density:
1.21 g/cm³
Melting Point:
208-214 °C(lit.)
Boiling Point:
381.9 °C at 760 mmHg
Flash Point:
184.8 °C
Solubility:
2.5 g/100 mL in water
Appearance:
Off-white to pink beige powder
Hazard Symbols:
Xi
Risk Codes:
36/37/38
Safety:
26-36-37/39 Details

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Reference

Synthesis of aromatic polyethers by Scholl reaction: Synthesis of aromatic polyethers by Scholl reaction. VII. Oxidative polymerization of 2,2-bis[4-(1-naphthoxy)phenyl]propane and 2,2-bis[4-(1-naphthyl)phenyl]propane. Percec, Virgil; Wang, James H.; Okita, Shigeru (Dep. Macromol. Sci., Case West. Reserve Univ., Cleveland, OH 44106-2699, USA).Some commonly used reagents like 139725-19-2 and 13922-41-3 are used in this experiment. J. Polym. Sci., Part A: Polym. Chem., 30(3), 429-38 (English) 1992. CODEN: JPACEC. ISSN: 0887-624X. DOCUMENT TYPE: Journal CA Section: 35 (Chemistry of Synthetic High Polymers) The synthesis and the mechanism of oxidative polymn. of the title monomers are presented. Both monomers polymerize by 2 different propagation steps. The 1st step represents a cation-radical dimerization of the naphthyl groups to dinaphthyl structure. H+[FeCl4]- generated from the 1st propagation step initiates a transalkylation reaction which provides structural units contg. isopropylidenic groups inserted between Ph and naphthyl, and between 2 naphthyl groups, resp. Since the Ph groups resulting from the 2nd propagation reaction are unreactive in both the oxidative coupling and the transalkylation steps, this polymn. reaction leads to polymers with low mol. wts. contg. Ph chain-ends. .

Synthesis of monocarbenepalladium(0) complexes and their catalytic behavior in cross-coupling reactions of aryldiazonium salts: Synthesis of monocarbenepalladium(0) complexes and their catalytic behavior in cross-coupling reactions of aryldiazonium salts. Selvakumar, Kumaravel; Zapf, Alexander; Spannenberg, Anke; Beller, Matthias (Institut fur Organische Katalyseforschung an der Universitat Rostock e. V.Chemicals with cas numbers 92278-52-9 and 13922-41-3 also play role. (IfOK), Rostock 18055, Germany). Chemistry--A European Journal, 8(17), 3901-3906 (English) 2002 Wiley-VCH Verlag GmbH & Co. KGaA.Several substances are used for example 347-46-6 which is its cas registry number. CODEN: CEUJED. ISSN: 0947-6539. DOCUMENT TYPE: Journal CA Section: 29 (Organometallic and Organometalloidal Compounds) Section cross-reference(s): 21, 25, 75 The first monocarbenepalladium(0) complexes with benzoquinone and naphthoquinone as addnl. ligands were prepd., [PdL[m-(2,3,5,6-h:h1-O)-Q1]]2 and [PdL[m-(2,3-h:h1-O)-Q2]]2 (L = 1,3-dimesitylimidazol-2-ylidene; 2, Q1 = 1,4-benzoquinone; 3, Q2 = 1,4-naphthoquinone). As demonstrated by NMR spectroscopy and x-ray anal., the complexes are dimeric, showing a unique coordination mode with bridged quinone ligands. The monocarbenepalladium(0) complexes 2 and 3, as well as the monomeric [PdL(h2,h2-CH2:CHSiMe2OSiMe2CH:CH2)] (1) described earlier, allow efficient cross-coupling reactions of aryldiazonium salts with olefins (Heck arylation) and arylboronic acids (Suzuki coupling). ..

Detail of "13922-41-3"

Boronic acid,B-1-naphthalenyl-

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