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147-82-0

Basic Information
CAS No.: 147-82-0
Name: 2,4,6-Tribromoaniline
Article Data: 175
Molecular Structure:
Molecular Structure of 147-82-0 (2,4,6-Tribromoaniline)
Formula: C6H4 Br3 N
Molecular Weight: 329.816
Synonyms: Aniline,2,4,6-tribromo- (6CI,7CI,8CI); 2,4,6-Tribromoaniline;2,4,6-Tribromobenzenamine; NSC 2216; sym-Tribromoaniline
EINECS: 205-700-1
Density: 2.35
Melting Point: 119 - 122 C
Boiling Point: 300 C
Flash Point: 132.9 °C
Solubility: insoluble AUTOIGNITION
Appearance: White crystal
Hazard Symbols:
Risk Codes: R23/24/25;R33   
Safety: Moderately toxic by intraperitoneal route. When heated to decomposition it emits very toxic fumes of Br and NOx. See also BROMIDES and ANILINE.
Transport Information: 25kgs
PSA: 26.02000
LogP: 4.13750
Synthetic route
106-40-1

4-bromo-aniline

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With 1-benzyl-1-aza-4-azoniabicyclo<2.2.2>octane bromide; calcium carbonate In methanol at 20℃; for 0.166667h;95%
Stage #1: 4-bromo-aniline With sulfuric acid In water for 0.0833333h; Green chemistry;
Stage #2: With sodium bromate; sodium bromide In water at 20℃; for 4h; Green chemistry;
94%
With trans-3,5-dihydroperoxy-3,5-dimethyl-1,2-dioxolane; hydrogen bromide In water at 20℃; for 0.7h;93%
615-36-1

2-bromoaniline

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With methanol; P-benzyltriphenylphosphonium tribromide; sodium hydrogencarbonate In dichloromethane for 0.116667h; Ambient temperature;94%
With dibromamine-T In acetonitrile at 20℃; for 0.166667h;90%
62-53-3

aniline

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With hydrogenchloride; dihydrogen peroxide; sodium bromide In water at 15℃; for 2h;99.9%
With hydrogen bromide; sodium bromide In chloroform; water at 0℃; Electrochemical reaction;98%
With bromine; acetic acid at 20℃; for 1h;98%
106-40-1

4-bromo-aniline

A

615-57-6

2,4-dibromo-aniline

B

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With sodium perborate; ammonium heptamolybdate; potassium bromide In acetic acid at 20℃; for 2.25h; Bromination;
With sodium persulfate; copper(ll) sulfate pentahydrate; sodium bromide In water; acetonitrile at 7 - 25℃; for 24h; Overall yield = 79 percent; Overall yield = 1.44 g; regioselective reaction;A 79 %Chromat.
B 21 %Chromat.
615-36-1

2-bromoaniline

A

615-57-6

2,4-dibromo-aniline

B

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With sodium persulfate; copper(ll) sulfate pentahydrate; sodium bromide In water; acetonitrile at 7 - 25℃; for 24h; Overall yield = 76 percent; Overall yield = 1.38 g; regioselective reaction;A 83 %Chromat.
B 17 %Chromat.
615-57-6

2,4-dibromo-aniline

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With bromine In tetrachloromethane at 20 - 40℃;99%
Bromierung;
62-53-3

aniline

A

615-57-6

2,4-dibromo-aniline

B

147-82-0

2,4,6-tribromoaniline

C

106-40-1

4-bromo-aniline

Conditions
ConditionsYield
Stage #1: aniline With n-butyllithium In diethyl ether; hexane at -78℃; for 1h;
Stage #2: With poly[4-(dibutyliodostannyl)butyl]styrene In diethyl ether; hexane at 20℃; for 18h;
Stage #3: With bromine In diethyl ether; hexane; dichloromethane at -78 - 20℃; for 2h;
A n/a
B n/a
C 76%
With bromine; acetic acid In tetrachloromethane for 0.0833333h; Ambient temperature; other reagent: bromine;A 41%
B 31%
C 21%
With bromine In tetrachloromethane for 0.0833333h; Product distribution; Mechanism; Ambient temperature; other aromatic compounds, other reagents: bromodimethylsulfonium bromide, bromodimethylsulfonium bromide/acetic acid, bromine/acetic acid, other solvents, other reaction temperature and time;A 33%
B 30%
C 19%
118-92-3

anthranilic acid

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With 1-benzyl-1-aza-4-azoniabicyclo<2.2.2>octane bromide; calcium carbonate In methanol at 20℃; for 0.416667h;90%
106-40-1

4-bromo-aniline

1972-28-7

diethylazodicarboxylate

A

4114-28-7

diethyl hydrazodicarboxylate

B

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With ZrBr4 In dichloromethane at 20℃; for 1.5h;A n/a
B 83%
121-57-3

4-aminobenzene sulfonic acid

147-82-0

2,4,6-tribromoaniline

Conditions
ConditionsYield
With water; bromine
With water; bromine
With bromine; acetic acid
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Chemistry

2,4,6-TRIBROMOANILINE's Molecular formula: C6H4Br3N
2,4,6-TRIBROMOANILINE's Molar mass: 329.81
EINECS: 205-700-1
density: 2.35 
Flash Point: 300°C
Boiling Point: 300 °C(lit.)
Melting point: 120-122 °C(lit.)
Appearance: White crystals or powder
Synonyms: TRIBROMOANILINE;1,4,6-tribromobenzenamine;AKOS BBS-00003575;ANILINE TRIBROMIDE;AKOS B028948;2,4,6-TRIBROMOBENZENAMINE;2,4,6-TRIBROMOANILINE;2,4,6-Tribomoaniline

Uses

2,4,6-TRIBROMOANILINE is used for pharmaceutical intermediates, chemical flame retardants etc.

Toxicity Data With Reference

1.   

ipr-mus LD50:500 mg/kg

   NTIS**    National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) AD277-689 .
2.    RTECS  BZ0175000

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by intraperitoneal route. When heated to decomposition it emits very toxic fumes of Br and NOx. See also BROMIDES and ANILINE.
Hazard Codes  T,Xi,Xn 
RIDADR  UN 2811 6.1/PG 2
WGK Germany  3
Hazard Note  Irritant
Risk Statements  23/24/25-33-36/37/38-20/21/22
Safety Statements  28-36/37/39-45-36/37-28A-26