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Basic Information
| CAS No.: | 15022-08-9 | ||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Name: | DIALLYL CARBONATE | ||||||||||||||
| Article Data: | 33 | ||||||||||||||
| Molecular Structure: | |||||||||||||||
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| Formula: | C7H10 O3 | ||||||||||||||
| Molecular Weight: | 142.155 | ||||||||||||||
| Synonyms: | Carbonicacid, di-2-propenyl ester (9CI); Carbonic acid, diallyl ester (6CI,7CI,8CI);Allyl carbonate; Diallyl carbonate; NSC 19177 | ||||||||||||||
| Density: | 0.986g/cm3 | ||||||||||||||
| Melting Point: | 25°C | ||||||||||||||
| Boiling Point: | 172.3°Cat760mmHg | ||||||||||||||
| Flash Point: | 58.9°C | ||||||||||||||
| Hazard Symbols: |
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| Risk Codes: | 36/37/38 | ||||||||||||||
| Safety: |
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| PSA: | 35.53000 | ||||||||||||||
| LogP: | 1.51160 | ||||||||||||||
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In neat (no solvent) at 80℃; under 760.051 Torr; for 16h; Inert atmosphere; Green chemistry; | 95% |
| With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine at 80 - 120℃; for 48h; | 61% |
| With potassium carbonate at 70℃; for 6h; | 53% |
| With sodium methylate at 60℃; for 1h; Inert atmosphere; | 2 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With copper (I) iodide; dicyclohexyl-carbodiimide at 64.85℃; under 37503 Torr; for 4h; | A 6% B 93% |
| With dicyclohexyl-carbodiimide In toluene at 64.85℃; under 37503 Torr; for 6h; | A n/a B 3.3% |
...Expand
- 124-38-9
carbon dioxide
- 107-18-6
allyl alcohol
- 92954-34-2
O-allyl-N,N'-dicyclohexyl isourea
A
- 557-40-4
Allyl ether
B
- 15022-08-9
diallylcarbonate
Conditions
| Conditions | Yield |
|---|---|
| at 64.85℃; under 37503 Torr; for 2h; | A 7% B 91% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With pyridine In diethyl ether a) 0 deg C, 1 h, b) 25 deg C, 5 h; | 85% |
| With pyridine In diethyl ether at 25℃; for 5h; | 67% |
Conditions
| Conditions | Yield |
|---|---|
| With 2-Cyanopyridine; cerium(IV) oxide at 119.84℃; under 37503.8 Torr; for 48h; Autoclave; | 76% |
| With dichloromethane; caesium carbonate In 1-methyl-pyrrolidin-2-one at 100℃; under 760.051 Torr; for 24h; | 58% |
| With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 18h; | 40% |
| With carbon tetrabromide; tributylphosphine; 2-cyclohexyl-1,1,3,3-tetramethylguanidine In N,N-dimethyl-formamide at 20℃; for 2h; Condensation; | 64.1 % Spectr. |
- 107-18-6
allyl alcohol
- 15022-08-9
diallylcarbonate
Conditions
| Conditions | Yield |
|---|---|
| With lanthanum(III) chloride; urea at 180℃; for 6h; Reagent/catalyst; Autoclave; | 60.7% |
- 298-14-6
potassium hydrogencarbonate
- 106-95-6
allyl bromide
A
- 557-40-4
Allyl ether
B
- 15022-08-9
diallylcarbonate
Conditions
| Conditions | Yield |
|---|---|
| tetrabutyl phosphonium bromide In various solvent(s) at 150℃; Solvent: NMP; | A n/a B 50% |
...Expand
- 107-18-6
allyl alcohol
- 616-38-6
carbonic acid dimethyl ester
A
- 35466-83-2
allyl methyl carbonate
B
- 15022-08-9
diallylcarbonate
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: allyl alcohol; carbonic acid dimethyl ester at 80℃; Stage #2: With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine at 80℃; for 1h; | A 50% B n/a |
| sodium methylate at 23℃; Inert atmosphere of nitrogen; | |
| sodium methylate at 23℃; Inert atmosphere of nitrogen; | |
| With sodium aluminate at 20 - 90℃; for 24h; |
...Expand
- 949895-84-5
(2-oxo-1,3-dioxolan-4-yl)methyl 4-methylbenzenesulfonate
- 107-18-6
allyl alcohol
A
- 15022-08-9
diallylcarbonate
B
- 68404-09-1
allyl glycidyl carbonate
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: allyl alcohol With sodium hydride In tetrahydrofuran Stage #2: (2-oxo-1,3-dioxolan-4-yl)methyl 4-methylbenzenesulfonate With tetrabutylammomium bromide In tetrahydrofuran at -70 - 20℃; | A 12% B 47% |
...Expand
- 102-69-2
tri-n-propylamine
- 124-38-9
carbon dioxide
A
- 15022-08-9
diallylcarbonate
B
- 27031-52-3
propyl N,N-di-propylcarbamate
Conditions
| Conditions | Yield |
|---|---|
| With allyl alcohol; acetylene at 160℃; for 16h; | A 6% B 4% C 21% |
...Expand
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DIALLYL CARBONATE
