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Basic Information
| CAS No.: | 15481-39-7 |
|---|---|
| Name: | BROMINE-1,4-DIOXANE COMPLEX |
| Article Data: | 9 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H8Br2O2 |
| Molecular Weight: | 247.914 |
| Synonyms: | 1,4-DIOXANE-BROMINE COMPLEX;1 4-DIETHYLENE DIOXIDE DIBROMIDE;BROMINE-1,4-DIOXANE COMPLEX;GLYCOL ETHYLENE ETHER DIBROMIDE;DIOXYETHYLENE ETHER DIBROMIDE;DIOXANE DIBROMIDE;DI(ETHYLENE OXIDE) DIBROMIDE;DIETHYLENE ETHER DIBROMIDE |
| Density: | g/cm3 |
| Melting Point: | 66 °C |
| Boiling Point: | 95 °C |
| Flash Point: | 12.2°C |
| PSA: | 18.46000 |
| LogP: | 1.72440 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| at 20℃; for 2h; Cooling with ice; | 65% |
- 123-91-1
1,4-dioxane
- 15481-39-7
dioxane dibromide
Conditions
| Conditions | Yield |
|---|---|
| With bromine at 0 - 23℃; for 3h; | 57% |
| With bromine | |
| With bromine | 10 g |
- 75-21-8
oxirane
- 15481-39-7
dioxane dibromide
Conditions
| Conditions | Yield |
|---|---|
| With bromine im geschlossenen Gefaess; |
- 15481-39-7
dioxane dibromide
- 162976-09-2
2,4-diethoxy-3-methylphenol
- 1061630-50-9
6-bromo-2,4-diethoxy-3-methylphenol
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In dichloromethane at -78 - 20℃; for 0.916667h; | 88% |
- 15481-39-7
dioxane dibromide
- 1374992-44-5
3-bromo-7-(2,3-dibromo-3-phenylpropoxy)-4-methylcoumarin
Conditions
| Conditions | Yield |
|---|---|
| at 0 - 20℃; for 4h; Neat (no solvent); regioselective reaction; | 86% |
- 2555-28-4
4-methyl-7-methoxy-2H-1-benzopyran-2-one
- 15481-39-7
dioxane dibromide
- 75908-67-7
3-bromo-7-methoxy-4-methylcoumarin
Conditions
| Conditions | Yield |
|---|---|
| at 0 - 20℃; for 2h; Neat (no solvent); regioselective reaction; | 85% |
- 90-33-5, 79566-13-5
7-hydroxy-4-methyl-chromen-2-one
- 15481-39-7
dioxane dibromide
- 55977-10-1
3-bromo-7-hydroxy-4-methyl-chromen-2-one
Conditions
| Conditions | Yield |
|---|---|
| at 0 - 20℃; for 3h; Neat (no solvent); regioselective reaction; | 84% |
Conditions
| Conditions | Yield |
|---|---|
| at 0 - 20℃; for 2h; Neat (no solvent); regioselective reaction; | 83% |
Conditions
| Conditions | Yield |
|---|---|
| at 0 - 20℃; for 0.5h; Neat (no solvent); regioselective reaction; | 83% |
- 922509-12-4
bis[4,6-di-tert-butyl-N-(2,6-diisopropylphenyl)-o-amidophenolato]tin(IV) tetrahydrofuratate
- 15481-39-7
dioxane dibromide
Conditions
| Conditions | Yield |
|---|---|
| In acetonitrile exclusion of air and moisture; soln. of Br2*diox (1 mmol) in MeCN added dropwise to soln. of Sn complex (1 mmol) in MeCN; soln. concd., stored at -12°C for 12 h, crystals isolated; elem. anal.; | 82.3% |
- Total:16 Page 1 of 1 1
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BROMINE-1,4-DIOXANE COMPLEX
