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| CAS No.: | 15484-46-5 |
|---|---|
| Name: | 2-Propenoic acid,2-(hydroxymethyl)-, methyl ester |
| Article Data: | 69 |
| Molecular Structure: | |
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|
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| Formula: | C5H8O3 |
| Molecular Weight: | 116.117 |
| Synonyms: | Acrylicacid, 2-(hydroxymethyl)-, methyl ester (8CI);Hydracrylic acid, 2-methylene-,methyl ester (7CI);Methyl 2-hydroxymethyl-2-propenoate;Methyl a-(hydroxymethyl)acrylate; |
| Density: | 1.086 g/cm3 |
| Boiling Point: | 184.807 °C at 760 mmHg |
| Flash Point: | 75.041 °C |
| PSA: | 46.53000 |
| LogP: | -0.29210 |
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| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane In 1,4-dioxane; water at 20℃; for 9h; Baylis-Hillman reaction; | 90% |
| With 1,4-diaza-bicyclo[2.2.2]octane In methanol at 20℃; for 9h; Baylis-Hillman reaction; | 90% |
| With 1,4-diaza-bicyclo[2.2.2]octane In 1,4-dioxane; water at 20℃; for 12h; | 90% |
- 50-00-0
formaldehyd
- 1779-58-4
(methyloxycarbonylmethyl)triphenylphosphonium bromide
- 15484-46-5
methyl 2-hydroxymethylacrylate
| Conditions | Yield |
|---|---|
| With potassium carbonate In water at 10 - 20℃; for 6h; | 85% |
- 280-57-9
1,4-diaza-bicyclo[2.2.2]octane
- 292638-85-8
acrylic acid methyl ester
- 15484-46-5
methyl 2-hydroxymethylacrylate
| Conditions | Yield |
|---|---|
| With formaldehyd; paraformaldehyde In diethyl ether; nitrogen | 77% |
| Conditions | Yield |
|---|---|
| Stage #1: formaldehyd With phosphoric acid In water at 90℃; for 5h; Stage #2: trimethyl phosphonoacetate With potassium carbonate In water at 35 - 40℃; for 0.9h; | 62% |
| With potassium carbonate In water at 20℃; for 1h; | 55% |
| With potassium carbonate In water at 20℃; for 2h; | 44% |
| With potassium carbonate at 30 - 35℃; for 1h; |
- 50-00-0
formaldehyd
- 292638-85-8
acrylic acid methyl ester
A
- 15484-46-5
methyl 2-hydroxymethylacrylate
B
- 109669-53-6
dimethyl 2,2′-[oxybis(methylene)]diacrylate
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane at 95℃; for 4h; | A 23% B 60% |
- 50-00-0
formaldehyd
- 5927-18-4
trimethyl phosphonoacetate
A
- 15484-46-5
methyl 2-hydroxymethylacrylate
B
- 292638-85-8
acrylic acid methyl ester
| Conditions | Yield |
|---|---|
| With potassium carbonate In water at 23℃; | A 56% B n/a |
- 280-57-9
1,4-diaza-bicyclo[2.2.2]octane
- 292638-85-8
acrylic acid methyl ester
- 15484-46-5
methyl 2-hydroxymethylacrylate
| Conditions | Yield |
|---|---|
| In cyclohexanol | 45% |
- 50-00-0
formaldehyd
- 140-88-5
ethyl acrylate
A
- 15484-46-5
methyl 2-hydroxymethylacrylate
B
- 109669-53-6
dimethyl 2,2′-[oxybis(methylene)]diacrylate
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane for 19h; Heating; | A n/a B 13% |
- 89533-83-5
2-acetoxymethyl-acrylic acid
- 15484-46-5
methyl 2-hydroxymethylacrylate
| Conditions | Yield |
|---|---|
| With methanol; sulfuric acid |
- 67-56-1
methanol
- 107-19-7
propargyl alcohol
- 13463-39-3, 71564-36-8
tetracarbonyl nickel
- 15484-46-5
methyl 2-hydroxymethylacrylate
| Conditions | Yield |
|---|---|
| (i) AcOH, (ii) /BRN= 506003/, (iii) H2SO4; Multistep reaction; |
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Specification
The Methyl 2-(hydroxymethyl)acrylate with the CAS number 15484-46-5 is also called 2-Propenoic acid,2-(hydroxymethyl)-,methyl ester. The systematic name is methyl 2-(hydroxymethyl)prop-2-enoate. In addition, the molecular formula is C5H8O3 and the molecular weight is 116.12. It is a kind of organics and it should be stored in dry and cool environment.
The properties of Methyl 2-(hydroxymethyl)acrylate are: (1)ACD/LogP: 0.52 ; (2)#H bond acceptors: 3; (3)#H bond donors: 1; (4)#Freely Rotating Bonds: 4; (5)Polar Surface Area: 35.53 Å2; (6)Index of Refraction: 1.438; (7)Molar Refractivity: 28.09 cm3; (8)Molar Volume: 106.9 cm3; (9)Polarizability: 11.13 ×10-24cm3; (10)Surface Tension: 33.7 dyne/cm; (11)Density: 1.085 g/cm3; (12)Flash Point: 75 °C; (13)Enthalpy of Vaporization: 49.01 kJ/mol; (14)Boiling Point: 184.8 °C at 760 mmHg; (15)Vapour Pressure: 0.205 mmHg at 25°C.
You can still convert the following datas into molecular structure:
(1)SMILES: O=C(OC)\C(=C)CO
(2)InChI: InChI=1/C5H8O3/c1-4(3-6)5(7)8-2/h6H,1,3H2,2H3
(3)InChIKey: RFUCOAQWQVDBEU-UHFFFAOYAK