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15780-28-6

Basic Information
CAS No.: 15780-28-6
Name: sodium deuteride
Article Data: 8
Molecular Structure:
Molecular Structure of 15780-28-6 (sodium deuteride)
Formula: DNa
Molecular Weight: 24.9898
Synonyms: Sodiumdeuteride; Sodium deuteride (NaD); Sodium monodeuteride
EINECS: 239-875-0
PSA: 0.00000
LogP: 0.11250
Synthetic route
7440-23-5

sodium

deuterium hydride

A

7646-69-7

sodium hydride

B

15780-28-6

sodium deuteride

Conditions
ConditionsYield
In neat (no solvent) byproducts: D, H; Na, HD (10 Torr) heated resistively in a stainless steel "cross" oven to 570 K; not isolated, detected by fluorescence spectroscopy;
7440-23-5

sodium

16873-17-9

deuterium

15780-28-6

sodium deuteride

Conditions
ConditionsYield
In further solvent(s) in a satd. hydrocarbon (decane) at 240°C in an autoclave, D2-pressure at begin: 28 atm;;
In neat (no solvent) byproducts: D; Na, HD (1o Torr) heated resistively in a stainless steel "cross" oven to 570 K; not isolated, detected by fluorescence spectroscopy;
In neat (no solvent) on treatment of heated Na with circulating D2 (by reduction of D2O with Fe), 800-810Torr, up to 360°C;;
7646-69-7

sodium hydride

16873-17-9

deuterium

15780-28-6

sodium deuteride

Conditions
ConditionsYield
deuterium uptake of NaH at 250°C; detn. by TG;
15780-28-6

sodium deuteride

{1,1'-(3-oxa-pentamethylene)dicyclopentadienyl}lutetium chloride

(1,1'-(3-oxa-pentamethylene)dicyclopentadienyl lutetium deuteride)2

Conditions
ConditionsYield
In tetrahydrofuran (under Ar), a Schlenk flask is charged with Lu-compd., NaD and THF, mixt. is stirred for 7 days at 45°C; centrifugation, concn., diffusion of pentane at 0°C, washing with pentane, drying in vac., elem. anal.;80.1%
15780-28-6

sodium deuteride

{1,1'-(3-oxa-pentamethylene)dicyclopentadienyl}yttrium chloride

(1,1'-(3-oxa-pentamethylene)dicyclopentadienyl yttrium deuteride)2

Conditions
ConditionsYield
In tetrahydrofuran (under Ar), a Schlenk flask is charged with Y-compd., NaD and THF, mixt. is stirred for 7 days at 45°C; centrifugation, concn., diffusion of pentane at 0°C, washing with pentane, drying in vac., elem. anal.;68.3%
15780-28-6

sodium deuteride

A

deuterium hydride

B

1310-73-2

sodium hydroxide

Conditions
ConditionsYield
In neat (no solvent) exothermic react., react.-enthalpy given;;
Raw Materials
7440-23-5
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