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15862-18-7

Basic Information
CAS No.: 15862-18-7
Name: 5,5'-Dibromo-2,2'-bipyridyl
Article Data: 41
Molecular Structure:
Molecular Structure of 15862-18-7 (5,5'-Dibromo-2,2'-bipyridyl)
Formula: C10H6 Br2 N2
Molecular Weight: 313.979
Synonyms: 5,5'-Dibromo-2,2'-bipyridine
Density: 1.809g/cm3
Melting Point: 225.0 to 229.0 °C
Boiling Point: 357.7°Cat760mmHg
Flash Point: 170.1°C
Safety: 24/25
PSA: 25.78000
LogP: 3.66860
Synthetic route
366-18-7

[2,2]bipyridinyl

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With bromine at 150℃; for 15h;86%
With bromine at 150℃; under 1140.08 Torr; for 15h;86%
Stage #1: [2,2]bipyridinyl With Acetyl bromide In methanol at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: With bromine at 185℃; for 72h; Inert atmosphere;
Stage #3: With ethylene diamine tetraacetic acid tetrasodium salt; sodium hydroxide; sodium sulfite In dichloromethane; water at 20℃; for 2h; Inert atmosphere;
39%
65520-13-0

2,2'-bipyridine dihydrochloride

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With bromine for 72h; Heating; Autoclave;85%
624-28-2

2,5-dibromopyridine

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With hexamethyldistannane; tetrakis(triphenylphosphine) palladium(0) In benzene for 65h; Heating;80%
With tetrakis(triphenylphosphine) palladium(0); hexamethyldistannane In benzene for 72h; Heating;80%
With tetrakis(triphenylphosphine) palladium(0); bis(tri-n-butyltin) In m-xylene at 130℃; for 72h; Darkness;80%
53710-17-1

2,6-diiodo-pyridine

611168-46-8

5-bromo-2-(tri-n-butylstannyl)pyridine

A

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

B

223463-10-3

5,5''-dibromo-2,2',6',2''-terpyridine

Conditions
ConditionsYield
With triphenyl phosphite; palladium(II) acetylacetonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 3h; Stille coupling; Inert atmosphere;A 6 %Spectr.
B 80%
223463-13-6

2-iodo-5-bromopyridine

611168-46-8

5-bromo-2-(tri-n-butylstannyl)pyridine

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With triphenyl phosphite; palladium(II) acetylacetonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 5h; Stille coupling; Inert atmosphere;80%
223463-13-6

2-iodo-5-bromopyridine

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); bis(tri-n-butyltin) In toluene at 125℃; for 72h; Sonogashira coupling;74%
With tetrakis(triphenylphosphine) palladium(0); bis(tri-n-butyltin) In toluene for 120h; Reflux;74%
Stille Cross-Coupling (Migita-Kosugi-Stille Coupling);69%
82799-91-5

5,5'-(2,2'-bipyridine)diacid chloride

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt at 100℃; for 20h; Irradiation;1.09 g
<2,2'>bipyridyl hydrobromide

<2,2'>bipyridyl hydrobromide

A

15862-19-8

5-bromo-2,2'-bipyridyl

B

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With carbon dioxide; bromine at 250℃;
626-05-1

2,6-Dibromopyridine

611168-46-8

5-bromo-2-(tri-n-butylstannyl)pyridine

A

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

B

1042150-70-8

C10H6Br2N2

C

223463-10-3

5,5''-dibromo-2,2',6',2''-terpyridine

Conditions
ConditionsYield
With triphenyl phosphite; palladium(II) acetylacetonate In toluene at 120℃; for 7h; Stille coupling; Inert atmosphere;A 5 %Spectr.
B 7 %Spectr.
C 87 %Spectr.
624-28-2

2,5-dibromopyridine

611168-46-8

5-bromo-2-(tri-n-butylstannyl)pyridine

15862-18-7

5,5'-dibromo-2,2'-dipyridyl

Conditions
ConditionsYield
With triphenyl phosphite; palladium(II) acetylacetonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 6h; Stille coupling; Inert atmosphere;
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522599-21-9
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    Introduction Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical manufacturing for overseas customers, in the field

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     China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    1.place of origin china with super quality by reasonable price. 2.fast delivery by safe express way to all the country. 3.has a number of highly qualified engineers and experts to provide guidance for reagents. 4.when you meet p

    Wuhan New-Rise biochem Co.,Ltd. is a leading provider and manufacturer of pharmaceutical and chemical products. We are dedicated in providing a wide variety of quality API, pharm

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    Business Type:Trading Company

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  • Casno:

    15862-18-7

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    Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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