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163520-33-0

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Basic Information
CAS No.: 163520-33-0
Name: ISOXADIFEN-ETHYL
Article Data: 7
Molecular Structure:
Molecular Structure of 163520-33-0 (ISOXADIFEN-ETHYL)
Formula: C18H17 N O3
Molecular Weight: 295.338
Synonyms: AE-F122006; HOE 122006; Isoxadifen ethyl ester; Isoxadifen-ethyl
EINECS: 443-870-0
Density: 1.15g/cm3
Melting Point: 87-88℃ (ethyl ether )
Boiling Point: 407.7°Cat760mmHg
Flash Point: 166.8°C
Solubility: 1.06mg/L at 20℃
Hazard Symbols:
Risk Codes: 22-43-50
Safety:
Hazard Codes Xn,N
Risk Statements 22-43-50
Safety Statements 36/37-61
RIDADR UN3077 9/PG 3
RTECS NY2390000
PSA: 47.89000
LogP: 2.70520
Related products
Synthetic route
67428-04-0, 105561-41-9, 37555-46-7

ethyl 2,2-diphenylcyclopropane-1-carboxylate

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With trifluoroacetic acid; sodium nitrite at 18 - 40℃; for 0.5h; Reagent/catalyst;89%
530-48-3

1,1-Diphenylethylene

626-35-7

nitroacetic acid ethyl ester

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In ethanol at 80℃; for 120h;75%
530-48-3

1,1-Diphenylethylene

623-33-6

glycine ethyl ester hydrochloride

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With tert.-butylnitrite; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium hydrogencarbonate; zinc dibromide In tert-butyl methyl ether at 20℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube;67%
95080-93-6

ethyl chlorooximidoacetate

530-48-3

1,1-Diphenylethylene

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With sodium hydrogencarbonate In isopropyl alcohol at 40℃; for 24h;
5350-57-2

benzophenone hydrazone

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: mercury(II) oxide / Petroleum ether / 16 h / 20 °C
2: Petroleum ether / 0.17 h / 50 °C
3: sodium nitrite; trifluoroacetic acid / 0.5 h / 18 - 40 °C
View Scheme
530-48-3

1,1-Diphenylethylene

ethyl 2-chloro-2-hydroximinoacetate

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With triethylamine In diethyl ether for 2h;12.7 g
530-48-3

1,1-Diphenylethylene

14337-43-0

ethyl 2-chloro-2-(hydroxyimino)acetate

163520-33-0

isoxadifen-ethyl

Conditions
ConditionsYield
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 25 - 30℃; Temperature;13 g
163520-33-0

isoxadifen-ethyl

(5,5-diphenyl-4,5-dihydro-isoxazol-3-yl)-methanol

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol; dichloromethane at 20℃; for 6h;92%
With sodium tetrahydroborate In methanol for 1h; Heating;
163520-33-0

isoxadifen-ethyl

3-chloromethyl-5,5-diphenyl-4,5-dihydro-isoxazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaBH4 / methanol / 1 h / Heating
2: SOCl2 / benzene / 1 h / Heating
View Scheme
163520-33-0

isoxadifen-ethyl

368886-04-8

C-(5,5-diphenyl-4,5-dihydro-isoxazol-3-yl)-methylamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: NaBH4 / methanol / 1 h / Heating
2: SOCl2 / benzene / 1 h / Heating
3: dimethylformamide / 20 °C
4: NH2NH2 / methanol / 2 h / 60 °C
View Scheme
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