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16588-75-3

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Basic Information
CAS No.: 16588-75-3
Name: 2-METHOXY-5-TRIFLUOROMETHYLPHENYL ISOCYANATE
Article Data: 17
Molecular Structure:
Molecular Structure of 16588-75-3 (2-METHOXY-5-TRIFLUOROMETHYLPHENYL ISOCYANATE)
Formula: C9H6 F3 N O2
Molecular Weight: 217.147
Synonyms: Isocyanicacid, a,a,a-trifluoro-6-methoxy-m-tolyl ester (8CI);2-Isocyanato-1-methoxy-4-trifluoromethylbenzene;2-Methoxy-5-(trifluoromethyl)phenyl isocyanate
Density: 1.272g/cm3
Boiling Point: 100-103℃ (10 Torr)
Flash Point: 94.592°C
PSA: 38.66000
LogP: 2.68130
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Synthetic route
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2-Methoxy-5-trifluoromethyl-aniline

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trichloromethyl chloroformate

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Conditions
ConditionsYield
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h;88%
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h;88%
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h;88%
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phosgene

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2-Methoxy-5-trifluoromethyl-aniline

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2-methoxy-5-trifluoromethylphenyl isocyanate

Conditions
ConditionsYield
With pyridine In diethyl ether; dichloromethane; toluene
With pyridine In dichloromethane; toluene at 0 - 20℃; for 3.5h;
With sodium hydrogencarbonate In dichloromethane; water at 0℃; for 0.5h;
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4-(4-acetylphenoxy)-5-aminopyridine

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N,N,N',N'-tetramethyl-1,8-diaminonaphthalene

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trichloromethyl chloroformate

16588-75-3

2-methoxy-5-trifluoromethylphenyl isocyanate

Conditions
ConditionsYield
In dichloromethane
...Expand
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bis(trichloromethyl) carbonate

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2-Methoxy-5-trifluoromethyl-aniline

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2-methoxy-5-trifluoromethylphenyl isocyanate

Conditions
ConditionsYield
With pyrographite In ethyl acetate for 2h; Reflux;
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5-(4-aminophenoxy)isoindoline-1,3-dione

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2-methoxy-5-trifluoromethylphenyl isocyanate

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Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 12 - 22h; Product distribution / selectivity;96%
16588-75-3

2-methoxy-5-trifluoromethylphenyl isocyanate

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2-bromo-6-fluoroaniline

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3-(2-bromo-6-fluorophenyl)-1-[2-methoxy-5-(trifluoromethyl)phenyl]urea

Conditions
ConditionsYield
In acetonitrile at 35 - 88℃; for 38 - 45h; Product distribution / selectivity;87.5%
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2-Fluoroaniline

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N-(2-fluorophenyl)-N'-[2-methoxy-5-(trifluoromethyl)phenyl]urea

Conditions
ConditionsYield
In acetonitrile at 82℃; for 4h;86.4%
In acetonitrile for 4h; Reflux; Large scale;85.9%
In acetonitrile at 0℃; for 7.25h; Reflux; Large scale;85.9%
In acetonitrile for 4h; Reflux; Large scale;85.9%
In acetonitrile Reflux;
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N-(4-fluoro-3-methylphenyl)-piperazine

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(2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester

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2-methoxy-5-trifluoromethylphenyl isocyanate

{8-fluoro-2-[4-(4-fluoro-3-methylphenyl)-1-piperazinyl]-3-[6-methoxy-3-(trifluoro-methyl)phenyl]-3,4-dihydro-4-quinazolinyl}-acetic acid methyl ester

Conditions
ConditionsYield
79%
...Expand
791117-28-7

(2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester

16588-75-3

2-methoxy-5-trifluoromethylphenyl isocyanate

methyl (2E)-3-(3-fluoro-2-((((2-methoxy-5-(trifluoromethyl)phenyl)imino)methylene)amino)phenyl)acrylate

Conditions
ConditionsYield
In dichloromethane at 20℃;62%
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  • Casno:

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     China (Mainland)  |  Contact Details

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    Changzhou Run-chem Biotechnology Co., Ltd., established in 2021, is committed to the research and development of pharmaceutical intermediates, especially the customization and prod

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  • 2-methoxy-5-[(4-methyl-1-piperazinyl)sulfonyl]benzenamine

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  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

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