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CAS No.: | 1794-86-1 |
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Name: | dichloroformoxine |
Article Data: | 28 |
Molecular Structure: | |
Formula: | CH Cl2 N O |
Molecular Weight: | 113.931 |
Synonyms: | Phosgene,oxime (6CI,7CI,8CI); CX; Dichloroformaldehyde oxime; Dichloroformaldoxime;Dichloroformoxime; Phosgene oximine |
Density: | 1.66g/cm3 |
Melting Point: | 39-40 °C |
Boiling Point: | 185.1°C at 760 mmHg |
Flash Point: | 65.7°C |
PSA: | 32.59000 |
LogP: | 1.20920 |
Chloronitroacetyl chloride
dichloroformoxime
Conditions | Yield |
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With urea In diethyl ether for 0.5h; Heating; further reagents (C6H11NH)2CO, (MeNH)2CO, thiourea, (PhNH)2CO; | 75% |
Conditions | Yield |
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With chlorine In water under cooling with ice-water Cl2 is led into the suspension; dichlorofuroxane isolated as oil; dichlorofuroxim extracted with ether; | A n/a B 40% |
With Cl2 In water under cooling with ice-water Cl2 is led into the suspension; dichlorofuroxane isolated as oil; dichlorofuroxim extracted with ether; | A n/a B 40% |
With chlorine In hydrogenchloride | |
With Cl2 In hydrogenchloride |
Conditions | Yield |
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With tin In acetonitrile | 16.8% |
Conditions | Yield |
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With hydrogenchloride; diethyl ether; tin(ll) chloride | |
With ethanol; sulfur dioxide; water | |
With ethanol; hydrogen sulfide | |
With methanol; hydrogen sulfide | |
With methanol; aluminium amalgam |
bromodichloronitrosomethane
dichloroformoxime
Conditions | Yield |
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With methanol; hydrogen sulfide |
Conditions | Yield |
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With sulfuric acid durch elektrolytische Reduktion an einer Zinnkathode; | |
With hydrogenchloride; tin; diethyl ether at 0 - 5℃; | |
(reduction); |
chloropicrin
A
dichloroformoxime
B
N-Methylhydroxylamine
C
trichloronitrosomethane
D
methylamine
Conditions | Yield |
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Bei der elektrolytischen Reduktion entstehen je nach den Bedingungen wechselnde Menge; |
Conditions | Yield |
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With hydrogenchloride; tin; diethyl ether at 0 - 5℃; |
mercury fulminate
dichloroformoxime
Conditions | Yield |
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With water; chlorine | |
With hydrogenchloride; chlorine | |
With chloroethane; chlorine | |
With sodium hypochlorite |
sodium cyanate
dichloroformoxime
Conditions | Yield |
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With sulfuric acid; water; chlorine at 0℃; |