Detail of "18209-60-4"

CAS Number:
18209-60-4
Name:
Silanamine,1-chloro-N,N,1,1-tetramethyl-
Molecular Structure:
Formula:
C₄H₁₂ClNSi
Molecular Weight:
137.68
Synonyms:
Silylamine,1-chloro-N,N,1,1-tetramethyl- (6CI,7CI,8CI);(N,N-Dimethylamino)dimethylchlorosilane;Chloro(dimethylamino)dimethylsilane;Chlorodimethyl(dimethylamino)silane;
EINECS:
242-095-3
Density:
0.924 g/cm³
Boiling Point:
85.1 °C at 760 mmHg
Flash Point:
5.3 °C
Risk Codes:
11-34
Safety:
9-16-26-33 Details

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Assay:98%

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Regioselective Synthesis of Polyfunctionalized Alkyltrisilanes and -Tetrasilanes via Reductive Cross-Coupling Reaction of Aminoalkylsilyl chlorides with Lithium: Regioselective Synthesis of Polyfunctionalized Alkyltrisilanes and -Tetrasilanes via Reductive Cross-Coupling Reaction of Aminoalkylsilyl chlorides with Lithium. Tamao, Kohei; Sun, Guang-Ri; Kawachi, Atsushi; Yamaguchi, Shigehiro (Institute for Chemical Research, Kyoto University, Uji 611, Japan). Organometallics, 16(4), 780-788 (English) 1997 American Chemical Society. CODEN: ORGND7. ISSN: 0276-7333.Some commonly used reagents like 90654-97-0 and 18209-60-4 are used in this experiment. DOCUMENT TYPE: Journal CA Section: 29 (Organometallic and Organometalloidal Compounds) Highly selective cross-coupling reactions promoted by Li metal were achieved between aminodichloromonosilanes R(Et2N)SiCl2 (R = Me, Et, Ph, Et2N) and 2 equiv of Me3SiCl (1) or (Et2N)Me2SiCl (2) and between aminochlorodisilanes (Et2N)nMe3-nSiSiMe(NEt2)Cl (n = 1, 2) and 1 equiv of 1, 2, or (Me2N)nR3-nSiCl (n = 1, R = Et; n = 2, R = Me, Et) in THF at room temp. to form the corresponding sym. and unsym. diamino- to pentaaminotrisilanes in high yields, which are transformed into alkoxy and fluoro derivs. under mild conditions. A tetraaminotetrasilane also was prepd. by reductive homocoupling of (Et2N)Me2SiSiMe(NEt2)Cl and converted into the alkoxytetrasilane. Some special exptl. procedures were employed for the selective coupling reactions. .