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18254-13-2

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Basic Information
CAS No.: 18254-13-2
Name: 2,4,6-Tris(1-phenylethyl)phenol
Article Data: 13
Molecular Structure:
Molecular Structure of 18254-13-2 (2,4,6-Tris(1-phenylethyl)phenol)
Formula: C30H30O
Molecular Weight: 406.568
Synonyms: EINECS 242-128-1;2,4,6-Tris-(1-phenyl-aethyl)-phenol;2,4,6-tris-(1-phenyl-ethyl)-phenol;Opt.-inakt. 2-Hydroxy-1.3.5-tris-(1-phenyl-aethyl)-benzol;
Density: 1.076g/cm3
Boiling Point: 519.3°C at 760 mmHg
Flash Point: 238.4°C
PSA: 20.23000
LogP: 7.84760
Related products
Synthetic route
292638-84-7

styrene

108-95-2

phenol

A

4237-44-9

2-(1-phenylethyl)phenol

B

4237-28-9

2,6-di-(α-methylbenzyl)phenol

C

2769-94-0

2,4-di-(α-methylbenzyl)phenol

D

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
Stage #1: phenol With aluminium at 140℃; for 1h;
Stage #2: styrene at 180 - 190℃; for 5h; Further stages. Further byproducts.;		A 23%
B 46%
C 8%
D 10%
...Expand
672-65-1

(1-chloroethyl)benzene

108-95-2

phenol

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
at 85 - 130℃;
108-95-2

phenol

styrene-xylene mixture

styrene-xylene mixture

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
With sulfuric acid
292638-84-7

styrene

108-95-2

phenol

A

4237-44-9

2-(1-phenylethyl)phenol

B

4237-28-9

2,6-di-(α-methylbenzyl)phenol

C

120346-43-2, 1988-89-2

1-(4-hydroxyphenyl)-1-phenylethane

D

2769-94-0

2,4-di-(α-methylbenzyl)phenol

E

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
With sulfuric acid In water at 50 - 200℃; for 3.83333h; Temperature; Autoclave; Inert atmosphere;
With sulfate ion-supported on titanium dioxide at 80℃; for 6h; Reagent/catalyst; Temperature; Inert atmosphere;
With phosphoric acid; sulfuric acid for 3.5h; Heating;
With 5-SO42-/ZrO2 at 100℃; for 6h; Reagent/catalyst; Inert atmosphere;
...Expand
292638-84-7

styrene

108-95-2

phenol

A

4237-28-9

2,6-di-(α-methylbenzyl)phenol

B

2769-94-0

2,4-di-(α-methylbenzyl)phenol

C

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
With methanesulfonic acid In neat (no solvent) at 120℃; for 6h; Reagent/catalyst; Overall yield = 100 %Chromat.;
With iron(III) chloride; t-butylsulfonic acid In neat (no solvent) at 120℃; for 6h; Catalytic behavior; Reagent/catalyst; Temperature;
...Expand
292638-84-7

styrene

108-95-2

phenol

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

Conditions
ConditionsYield
With copper(I) bromide In neat (no solvent) at 120℃; for 6h;65 %Chromat.
With solid catalyst contain with SiO2, AlCl3, NiCl2 at 120℃; for 6h; Inert atmosphere;
106-92-3

Allyl glycidyl ether

3234-28-4

1,2-epoxytetradecane

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

C49H66O4

Conditions
ConditionsYield
Stage #1: 1,2-epoxytetradecane; 2,4,6-tri-(α-methylbenzyl)phenol With potassium methanolate at 120 - 145℃; for 20.1167h; Inert atmosphere;
Stage #2: Allyl glycidyl ether for 5h; Inert atmosphere;		98.1%
...Expand
106-92-3

Allyl glycidyl ether

18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

122-60-1

Phenyl glycidyl ether

C45H50O5

Conditions
ConditionsYield
Stage #1: 2,4,6-tri-(α-methylbenzyl)phenol; Phenyl glycidyl ether With potassium methanolate at 120℃; for 3.95h; Inert atmosphere;
Stage #2: Allyl glycidyl ether for 17.2167h; Inert atmosphere;		97.9%
...Expand
18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

111-44-4

3-oxa-1,5-dichloropentane

1-(2-chloro-ethoxy)-2-[2,4,6-tris-(1-phenyl-ethyl)-phenoxy]-ethane

Conditions
ConditionsYield
With sodium hydroxide at 130℃;
18254-13-2

2,4,6-tri-(α-methylbenzyl)phenol

111-44-4

3-oxa-1,5-dichloropentane

aqueous NaOH

aqueous NaOH

1-(2-chloro-ethoxy)-2-[2,4,6-tris-(1-phenyl-ethyl)-phenoxy]-ethane

Conditions
ConditionsYield
at 130℃;
...Expand
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