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1829-32-9

Basic Information
CAS No.: 1829-32-9
Name: 3-Chlorosalicylic acid
Article Data: 35
Molecular Structure:
Molecular Structure of 1829-32-9 (3-Chlorosalicylic acid)
Formula: C7H5ClO3
Molecular Weight: 172.568
Synonyms: 3EINECS 217-379-5;NSC 18854;Benzoic acid, 3-chloro-2-hydroxy- (9CI);Salicylic acid, 3-chloro- (8CI);
EINECS: 217-379-5
Density: 1.536 g/cm3
Melting Point: 184-186 ºC
Boiling Point: 291.7 ºC at 760 mmHg
Flash Point: 130.2 ºC
Appearance: White Solid
Hazard Symbols:
Risk Codes: R36/37/38   
Safety: S26;S36
PSA: 57.53000
LogP: 1.74380
Synthetic route
116025-20-8

3-chloro-2-hydroxy-thiobenzoic acid S-methyl ester

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With lithium hydroxide In methanol at 20℃; for 6h;100%
124-38-9

carbon dioxide

27701-22-0

chloro-1 methoxymethylenoxy-2 benzene

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Stage #1: chloro-1 methoxymethylenoxy-2 benzene With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 1.5h;
Stage #2: carbon dioxide In tetrahydrofuran; hexane at -78℃; for 1.5h;
Stage #3: With hydrogenchloride In tetrahydrofuran; hexane at 20℃;
91%
50-45-3

2,3-dichlorbenzoic acid

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With pyridine; copper; potassium carbonate In water for 2h; Heating;85%
With copper(l) iodide; copper; potassium carbonate at 180℃; under 7355.08 Torr;

N-(4-fluorophenyl)glycine potassium salt

A

1829-32-9

3-Chloro-2-hydroxybenzoic acid

B

180911-99-3

N-(4-fluorophenyl)-N-(2-carboxyphenyl)glycin

Conditions
ConditionsYield
Stage #1: N-(4-fluorophenyl)glycine potassium salt With potassium 2,5-dichlorobenzoate; copper; potassium carbonate In water for 20.5h; Heating / reflux;
Stage #2: With hydrogenchloride In water at 75 - 80℃; for 0.5h;
A n/a
B 80.3%
95-57-8

2-monochlorophenol

17201-44-4

sodium ethyl carbonate

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With carbon dioxide at 190℃; under 7600.51 Torr; for 6h; Autoclave; regioselective reaction;68.2%
124-38-9

carbon dioxide

95-57-8

2-monochlorophenol

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Stage #1: 2-monochlorophenol With Mesitol; sodium hydride In mineral oil at 100℃; for 0.0833333h; Glovebox;
Stage #2: carbon dioxide In mineral oil at 185℃; under 3800.26 Torr; for 2h;
55%
With potassium carbonate at 170℃; under 29420.3 Torr;
873975-79-2

3-chloro-2-hydroxy-benzoic acid-(2,2,2-trichloro-1-hydroxy-ethylamide)

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With sodium hydroxide
54-21-7, 13639-21-9, 79211-80-6

salicylic acid disodium salt

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With sodium hypochlorite
97-05-2

5-sulfosalicylic Acid

1829-32-9

3-Chloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With chlorine; acetic acid Behandeln des Reaktionsprodukts mit ueberhitztem Wasserdampf;
With hydrogenchloride; potassium permanganate Behandeln des Reaktionsprodukts mit ueberhitztem Wasserdampf;
56-23-5

tetrachloromethane

507-40-4

tert-butylhypochlorite

69-72-7

salicylic acid

1829-32-9

3-Chloro-2-hydroxybenzoic acid

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Chemistry

IUPAC Name: 3-chloro-2-hydroxybenzoic acid
Synonyms of 3-Chlorosalicylic acid (CAS NO,1829-32-9): 3EINECS 217-379-5 ; NSC 18854 ; Benzoic acid, 3-chloro-2-hydroxy- (9CI) ; Salicylic acid, 3-chloro- (8CI)
CAS NO: 1829-32-9
Molecular Formula: C7H5ClO3
Molecular Weight: 172.5658
Molecular Structure:

Melting Point: 184-186 °C
ProductCategories: Aromatics ; C7 ; Carbonyl Compounds ; Carboxylic Acids 
H bond acceptors: 3
H bond donors: 2
Freely Rotating Bonds: 2
Polar Surface Area: 35.53 Å2
Index of Refraction: 1.629
Molar Refractivity: 39.95 cm3
Molar Volume: 112.3 cm3
Surface Tension: 66 dyne/cm
Density of 3-Chlorosalicylic acid (CAS NO,1829-32-9): 1.536 g/cm3
Flash Point: 130.2 °C
Enthalpy of Vaporization: 56.1 kJ/mol
Boiling Point: 291.7 °C at 760 mmHg
Vapour Pressure: 0.000876 mmHg at 25°C

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 3