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192775-97-6

Basic Information
CAS No.: 192775-97-6
Name: 2-[1-(4-BROMOPHENYL)-1-METHYLETHYL]-4,4-DIMETHYL-4,5-DIHYDROOXAZOLINE
Article Data: 2
Molecular Structure:
Molecular Structure of 192775-97-6 (2-[1-(4-BROMOPHENYL)-1-METHYLETHYL]-4,4-DIMETHYL-4,5-DIHYDROOXAZOLINE)
Formula: C14H18BrNO
Molecular Weight: 296.207
Synonyms: QC-2699;
Density: 1.27g/cm3
Boiling Point: 346.1oC at 760 mmHg
Flash Point: 163.1oC
PSA: 21.59000
LogP: 3.36960
Synthetic route
176324-85-9

4-bromo-α-(4,4-dimethyloxazolin-2-yl)toluene

74-88-4

methyl iodide

192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Conditions
ConditionsYield
With CH3I; potassium hexamethylsilazane; acetic acid In dichloromethane; water; isopropyl alcohol4.61 g (0.0156 mmole, 84%)
32454-35-6

2-(4-bromophenyl)-2-methylpropionic acid

124-68-5

2-Amino-2-methyl-1-propanol

192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Conditions
ConditionsYield
Stage #1: 2-(4-bromophenyl)-2-methylpropionic acid With thionyl chloride
Stage #2: 2-Amino-2-methyl-1-propanol With thionyl chloride
41841-16-1

(4-bromo-phenyl)-acetic acid methyl ester

192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride
2: thionyl chloride
View Scheme
192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

628-20-6

4-Chlorobutyronitrile

192775-98-7

4-(4-chloro-1-oxobutyl)-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Conditions
ConditionsYield
With iodine; magnesium In tetrahydrofuran93%
192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

7486-35-3

tri-n-butyl(vinyl)tin

1298022-53-3

4,4-dimethyl-2-(2-(4-vinylphenyl)propan-2-yl)-4,5-dihydrooxazole

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); lithium chloride In N,N-dimethyl-formamide at 70℃; Stille coupling; Inert atmosphere;82%
192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

4635-59-0

4-Chlorobutanoyl chloride

192775-98-7

4-(4-chloro-1-oxobutyl)-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran
75-21-8

oxirane

192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

38385-95-4

2-(4-piperidinyl)-1H-benzimidazole

2-[1-(2-{4-[1-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)-1-methylethyl]phenyl}ethyl)piperidin-4-yl]-1-(2-ethoxyethyl)-1H-benzimidazole

Conditions
ConditionsYield
Stage #1: oxirane; 4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene With n-butyllithium
Stage #2: 2-(4-piperidinyl)-1H-benzimidazole
75-21-8

oxirane

192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

98-59-9

p-toluenesulfonyl chloride

2-{4-[1-(4,4-dimethyl-4,5-dihydrooxazol-2-yl)-1-methylethyl]phenyl}ethyl p-toluenesulfonate

Conditions
ConditionsYield
With n-butyllithium
192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

Bilastine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: n-butyllithium
View Scheme
192775-97-6

4-bromo-α,α-dimethyl-α-(4,4-dimethyloxazolin-2-yl) toluene

2-methyl-2-[4'-(2''-hydroxyethyl)phenyl]propanoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: n-butyllithium / tert-butyl methyl ether; hexane / 10 h / -60 °C / Large scale
1.2: 7 h / -60 - 20 °C / Large scale
2.1: phosphoric acid / water / 30 h / 90 °C / Large scale
View Scheme
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    Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

    Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketi

  •  Hangzhou ZeErRui Chemical Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-82512721

    Address:No 317,Jingling Road,Guali Town,Xiaoshan District

       Inquiry Now

  • 192775-97-6

  • Casno:

    192775-97-6

    192775-97-6

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

    Shanghai Chinqesen Biotechnology Co., Ltd. Company slogan:?Innovation, cooperation and win-win Company introduction:?Shanghai Chinqesen Biotechnology Co., Ltd. is a professional ph

  •  Shanghai Chinqesen Biotechnology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8617316470195

    Address:333 Songze Avenue, Qingpu District, Shanghai

       Inquiry Now

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