Detail of "2008-75-5"

CAS Number:
2008-75-5
Name:
Piperidine,1-(2-chloroethyl)-, hydrochloride (1:1)
Superlist Name:
2-Piperidinoethylchloride hydrochloride
Molecular Structure:
Formula:
C₇H₁₄ClN^.HCl
Molecular Weight:
184.11
Synonyms:
Piperidine,1-(2-chloroethyl)-, hydrochloride (6CI,7CI,8CI,9CI);1-(2-Chloroethyl)piperidine hydrochloride;1-(2-Chloroethyl)piperidinemonohydrochloride;1-(2-Chloroethyl)piperidinium chloride;1-Chloro-2-piperidinoethane hydrochloride;2-(1-Piperidinyl)-1-chloroethanehydrochloride;2-(Piperidin-1-yl)ethyl chloride hydrochloride;2-Piperidino-1-chloroethane hydrochloride;N-(2-Chloroethyl)piperidine hydrochloride;N-(b-Chloroethyl)piperidine hydrochloride;1-(2-Chloroethyl) Piperidine hydrochloride;
EINECS:
217-920-5
Melting Point:
230-232 °C(lit.)
Boiling Point:
190.3 °C at 760 mmHg
Flash Point:
68.9 °C
Solubility:
soluble in water
Appearance:
Colorless to beige crystals
Hazard Symbols:
T+, Xi
Risk Codes:
28-34-36/37/38
Safety:
26-28-36/37/39-45-24/25 Details
Transport Information:
UN 2928 6.1/PG 2

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Reference

2-[2-(Piperidino)ethyl]-10,10A-dihydro-1H,5H-imidazo[1,5-b]isoquinolin -1,3(2H)-dione: 2-[2-(Piperidino)ethyl]-10,10A-dihydro-1H,5H-imidazo[1,5-b]isoquinolin -1,3(2H)-dione. Schwan, Thomas J. (Morton-Norwich Products, Inc., USA). U.S. US 4001245 4 Jan 1977, 2 pp. (English). (United States of America). CODEN: USXXAM. CLASS: IC: C07D471-14. NCL: 260287000CF. APPLICATION: US 75-636913 2 Dec 1975. DOCUMENT TYPE: Patent CA Section: 28 (Heterocyclic Compounds (More Than One Hetero Atom)) The title compd. I, useful as an inflammation inhibitor, was obtained in 26% yield by cyclization of tetrahydroisoquinoline carboxylic acid with KOCN followed by treatment with N-(2-chloroethyl)piperidine.In this experiment, several chemicals are used like 2008-75-5 and 62373-29-9 HCl. .

Diaryl vinyl sulfoxides, a process for their synthesis, and their use in the preparation of benzothiophene derivatives: Diaryl vinyl sulfoxides, a process for their synthesis, and their use in the preparation of benzothiophene derivatives. Aikins, James A.; Miller, Randal S.; Zhang, Tony Y. (Lilly, Eli, and Co.; Aikins, James A.; Miller, Randal S.; Zhang, Tony Y., USA). PCT Int. Appl. WO 9640691 A1 19 Dec 1996, 45 pp. DESIGNATED STATES: W: AL, AM, AT, AU, AZ, BB, BG, BR, BY, CA, CH, CN, CZ, DE, DK, EE, ES, FI, GB, GE, HU, IL, IS, JP, KE, KG, KP, KR, KZ, LK, LR, LS, LT, LU, LV, MD, MG, MK, MN, MW, MX, NO, NZ, PL, PT, RO, RU, SD, SE, SG; RW: AT, BE, BF, BJ, CF, CG, CH, CI, CM, DE, DK, ES, FI, FR, GB, GR, IE, IT, LU, MC, NL, PT, SE. (English). (World Intellectual Property Organization). CODEN: PIXXD2. CLASS: ICM: C07F007-08. ICS: C07F007-18. APPLICATION: WO 1996-US9163 4 Jun 1996. PRIORITY: US 1995-478706 7 Jun 1995; US 1995-483130 7 Jun 1995. DOCUMENT TYPE: Patent CA Section: 25 (Benzene, Its Derivatives, and Condensed Benzenoid Compounds) Section cross-reference(s): 27, 45 The invention is directed to new diarylvinyl sulfoxides I [R1, R2 = H, alkoxy, arylalkoxy, halo, amino; R3 = thermally labile or acid-labile alkyl, alkenyl, or arylalkyl group], and to a new process for their synthesis. I are useful precursors for 2-aryl-substituted benzothiophenes II, which are in turn intermediates for the drugs III. 178431-37-3 and 2008-75-5 are cas registry numbers of chemicals which are used as reagents here.HX [R1, R2 = H, halo, amino, OH; R4, R5 = alkyl; or NR4R5 = pyrrolidino, piperidino, hexamethyleneimino, morpholino; X = Cl, Br]. For instance, treatment of 4-MeOC6H4CH2COC6H4OMe-4 with TiCl4 in THF and reaction with Me3CSH and Et3N gave the vinyl sulfide (E)-4-MeOC6H4CH:C(SCMe3)C6H4OMe-4 [(E)-IV]. Alternatively, lithiation of 4-MeOC6H4CH2SCMe3 with BuLi and condensation with 4-MeOC6H4CHO gave (Z)-IV. Oxidn. of either isomer of IV with a dil. AcOH soln. of peracetic acid, in PhMe at -20°, gave the corresponding sulfoxide I [R1 = R2 = OMe; R3 = CMe3]. Dehydrative cyclization of, e.g., the (E)-sulfoxide, using p-MeC6H4SO3H catalyst under Dean-Stark conditions in PhMe, gave the benzothiophene II [R1 = R2 = OMe]. This was acylated by 4-(2-piperidinoethoxy)benzoyl chloride HCl in the presence of BCl3 with concomitant demethylation to give the objective compd. III.HCl [R1 = R2 = OH, NR4R5 = piperidino]. .

Detail of "2008-75-5"

Piperidine,1-(2-chloroethyl)-, hydrochloride (1:1)

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CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

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CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

CAS No.2008-75-5 2-Piperidinoethylchloride hydrochloride

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