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| CAS No.: | 2117-24-0 |
|---|---|
| Name: | 1,4-Bis((trimethylsilyl)oxy)benzene |
| Article Data: | 48 |
| Molecular Structure: | |
|
|
|
| Formula: | C12H22O2Si2 |
| Molecular Weight: | 254.476 |
| Synonyms: |
1,4-bis-trimethylsilanyloxy-benzene;Silane, [1,4-phenylenebis(oxy)]bis[trimethyl-;1,4-Bis |
| Density: | 1.139g/cm3 |
| Melting Point: | 52 °C |
| Boiling Point: | 378.8°Cat760mmHg |
| Flash Point: | 182.9°C |
| PSA: | 18.46000 |
| LogP: | 4.11400 |
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- 73296-31-8
phenyltellurotrimethylsilane
- 106-51-4
p-benzoquinone
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 20℃; for 0.5h; reductive silylation; | 100% |
- 123-31-9
hydroquinone
- 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
| Conditions | Yield |
|---|---|
| With 3-methyl-1-sulfonic acid imidazolium hydrogen sulfate at 20℃; for 0.0833333h; Neat (no solvent); | 98% |
| With succinimide-N-sulfonic acid In acetonitrile at 20℃; for 0.0833333h; | 98% |
| With 1,3-disulfonic acid imidazolium hydrogen sulfate In neat (no solvent) at 20℃; for 0.0666667h; Green chemistry; | 98% |
- 1450-14-2
1,1,1,2,2,2-hexamethyldisilane
- 106-51-4
p-benzoquinone
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
| Conditions | Yield |
|---|---|
| With iodine In benzene at 61.9℃; for 7h; | 95% |
| With iodine In benzene at 60℃; for 3h; | 99 % Chromat. |
- 32115-55-2
N,N-Dimethylcarbamidsaeure-trimethylsilylester
- 123-31-9
hydroquinone
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
| Conditions | Yield |
|---|---|
| at 60℃; for 1h; | 94% |
| Conditions | Yield |
|---|---|
| With 1,1,1,3,3,3-hexamethyl-disilazane In acetonitrile for 12h; | 91% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 0.5h; Ambient temperature; | 60% |
| With pyridine |
- 75-77-4
chloro-trimethyl-silane
- 123-31-9
hydroquinone
- 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
| Conditions | Yield |
|---|---|
| In acetonitrile | 91% |
| Conditions | Yield |
|---|---|
| With zinc In tetrahydrofuran for 0.5h; ultrasonic irradiation; | 90% |
| With zinc In diethyl ether for 15h; Ambient temperature; | 77% |
- 81790-10-5
(2-bromoallyl)trimethylsilane
- 106-51-4
p-benzoquinone
A
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
B
- 138786-10-4
2-(2-Bromo-allyl)-1,4-bis-trimethylsilanyloxy-benzene
| Conditions | Yield |
|---|---|
| With lithium perchlorate In diethyl ether | A 12.5% B 75% |
- 106-51-4
p-benzoquinone
- 762-72-1
allyl-trimethyl-silane
A
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
B
- 138786-03-5
2-Allyl-1,4-bis-trimethylsilanyloxy-benzene
| Conditions | Yield |
|---|---|
| With lithium perchlorate In diethyl ether at 40℃; for 15h; further reactions with quinones; | A 12% B 73% |
| With lithium perchlorate In diethyl ether at 40℃; for 15h; | A 12% B 73% |
- 36850-80-3
[(1-methoxyvinyl)oxy]trimethylsilane
- 106-51-4
p-benzoquinone
A
- 2117-24-0
1,4-bis(trimethylsilyloxy)benzene
B
- 27798-63-6
Homogentinsaeure-methylester Bis(trimethylsilyl)ether
| Conditions | Yield |
|---|---|
| With lithium perchlorate In diethyl ether for 0.5h; Ambient temperature; | A 22% B 53% |
- Total:20 Page 1 of 1 1
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