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215788-65-1

Basic Information
CAS No.: 215788-65-1
Name: 1,1 bis(di-isopropylphosphine)ferrocene palladium dichloride
Molecular Structure:
Molecular Structure of 215788-65-1 (1,1  bis(di-isopropylphosphine)ferrocene  palladium  dichloride)
Formula: C22H36 Cl2 Fe P2 Pd
Molecular Weight: 595.648
Synonyms: (1,1'-Bis(diisopropylphosphino)ferrocene)dichloropalladium;Dichloro(1,1'-bis(diisopropylphosphino)ferrocene)palladium;Dichloro[Ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
Melting Point: 282-287 °C
PSA: 27.18000
LogP: 1.89170
Synthetic route
97239-80-0

1,1'-bis(diisopropylphosphino)ferrocene

palladium dichloride

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

Conditions
ConditionsYield
With HCl In diethyl ether; ethanol PdCl2 suspn. in EtOH treated with conc. HCl, stirred at 50°C for30 min, filtered, Fe complex (1 equiv.) soln. in Et2O added at 20°C, stirred for 10 min; crystd. at -35°C, filtered, washed (H2O), dried (vac.); elem. anal.;38%
75-09-2

dichloromethane

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

18103-73-6

4-mercaptopyridine-3-carboxylic acid

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) thionicotinate *0.5 CH2Cl2

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;79%
215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

147-93-3

Thiosalicylic acid

403609-52-9

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) thiosalicylate

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;68%
1121-24-0

ortho-mercaptophenol

75-09-2

dichloromethane

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 2-mercaptophenolate * 0.5CH2Cl2

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;70%
496-74-2

3,4-dimercaptotoluene

75-09-2

dichloromethane

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

403609-49-4

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 3,4-toluenedithiolate * CH2Cl2

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;56%
87314-49-6

3,6-dichlorobenzene-1,2-dithiol

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

403609-50-7

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 3,6-dichloro-1,2-benzenedithiolate

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;49%
215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

17534-15-5

1,2-benzenedithiole

403609-47-2

[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 1,2-benzenedithiolate

Conditions
ConditionsYield
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD;52%
215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

79060-88-1

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

[Pd(dippf)(μ-Cl)]2[tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]2

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique;69%
75-09-2

dichloromethane

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

108-98-5

thiophenol

[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]bis(phenylthio)palladium(II)*CH2Cl2

Conditions
ConditionsYield
With Et3N In toluene byproducts: Et3NHCl; under N2, Pd-complex was added to toluene soln. of thiophenol; Et3NHCl was filtered off, filtrate was evapd. to dryness, residue was recrystd. from CH2Cl2/hexane (1:2), hexane was layered onto CH2Cl2 soln., slow diffusion of hexane at 258 K; elem. anal.;68%
13869-38-0, 21264-32-4, 13869-42-6

bis(acetonitrile)dichloroplatinum(II)

215788-65-1

dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)

635727-62-7

[Pt(dippf)Cl2]

Conditions
ConditionsYield
In dichloromethane under Ar atm. mixt. (PtCl2(MeCN)2) and dippf in CH2Cl2 was stirred at room temp. for 1 h; soln. was concd., hexane was added, ppt. was filtered, washed with etherand dried in vacuo; elem. anal.;32%
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    1,1 bis(di-isopropylphosphine)ferrocene palladium dichloride

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