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| CAS No.: | 2208-07-3 |
|---|---|
| Name: | Ethyl acetimidate hydrochloride |
| Article Data: | 38 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H10ClNO |
| Molecular Weight: | 123.582 |
| Synonyms: | Acetimidicacid, ethyl ester, hydrochloride (6CI,7CI,8CI);Ethanimidic acid, ethyl ester,hydrochloride (9CI);Ethyl acetoamidatehydrochloride;Ethyl acetocarboximidate hydrochloride;Ethyl acetoimidatehydrochloride;Ethyl ethanimidate hydrochloride;Ethyl iminoacetatehydrochloride; |
| EINECS: | 218-631-7 |
| Density: | 0.89g/cm3 |
| Melting Point: | 112-114 °C(lit.) |
| Boiling Point: | 57.3 °C at 760 mmHg |
| Flash Point: | 22.3 °C |
| Solubility: | Soluble in water (50mg/L). |
| Appearance: | white to light yellow crystal powder |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-36-37/39 |
| PSA: | 33.08000 |
| LogP: | 1.92180 |
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| Conditions | Yield |
|---|---|
| With hydrogenchloride at 0℃; for 0.0833333h; Pinner reaction; Inert atmosphere; | 97% |
| With hydrogenchloride; sulfuric acid at -10 - 35℃; for 8h; | 97% |
| With acetyl chloride at 0℃; for 12h; Pinner Imino Ether Synthesis; Large scale; | 95% |
- 64-17-5
ethanol
- 73233-19-9, 90586-61-1
acetonitrile*2hydrogen chloride
- 2208-07-3
ethyl acetimidate hydrochloride
| Conditions | Yield |
|---|---|
| at -16℃; |
| Conditions | Yield |
|---|---|
| In methanol; tert-butyl methyl ether at 0℃; for 3.5h; | 13 g |
- 2208-07-3
ethyl acetimidate hydrochloride
- 404860-60-2
methyl 2-amino-6-(ethanimidoylamino)-2-methylhex-4-ynoate
| Conditions | Yield |
|---|---|
| Stage #1: methyl 2,6-diamino-2-methylhex-4-ynoate, dihydrochloride With sodium hydroxide In water at 25℃; for 0.166667h; pH=~ 7.95; Stage #2: ethyl acetimidate hydrochloride With sodium hydroxide In water for 3h; pH=8 - 8.5; Stage #3: With hydrogenchloride In water pH=4.1; | 100% |
| Stage #1: methyl 2,6-diamino-2-methylhex-4-ynoate, dihydrochloride; ethyl acetimidate hydrochloride With sodium hydroxide In water for 3.16667h; pH=7.95 - 8.5; Stage #2: With hydrogenchloride In water pH=4.1; | 100% |
- 945217-60-7
tert-butyl (3R,4S)-3,4-diaminopyrrolidine-1-carboxylate
- 2208-07-3
ethyl acetimidate hydrochloride
- 1202067-52-4
cis-(3,6)-2-methyl-3a,4,6,6a-tetrahydro-1H-pyrrolo[3.4-d]imidazole-5-carboxylic acid tert-butyl ester
| Conditions | Yield |
|---|---|
| In ethanol at 80℃; for 2.5h; | 100% |
- 68076-36-8
1-amino-4-[(tert-butyloxycarbonyl)amino]butane
- 2208-07-3
ethyl acetimidate hydrochloride
- 76-05-1
trifluoroacetic acid
| Conditions | Yield |
|---|---|
| Stage #1: 1-amino-4-[(tert-butyloxycarbonyl)amino]butane; ethyl acetimidate hydrochloride With triethylamine at 20℃; Inert atmosphere; Cooling with ice; Stage #2: trifluoroacetic acid | 100% |
- 2208-07-3
ethyl acetimidate hydrochloride
| Conditions | Yield |
|---|---|
| With triethylamine at 5℃; for 2.5h; | 99.1% |
- 21436-03-3
(S,S)-1,2-diaminocyclohexane
- 2208-07-3
ethyl acetimidate hydrochloride
| Conditions | Yield |
|---|---|
| In ethanol at 0 - 20℃; for 8h; Inert atmosphere; | 99% |
| In ethanol at 0 - 20℃; | |
| In ethanol at 20℃; for 9h; |
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Chemistry
Molecular Structure of Ethanimidic acid, ethylester, hydrochloride (1:1) (CAS NO.2208-07-3):
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IUPAC Name: ethyl ethanimidate hydrochloride
Empirical Formula: C4H10ClNO
Molecular Weight: 123.5813
H bond acceptors: 2
H bond donors: 1
Freely Rotating Bonds: 2
Polar Surface Area: 12.24Å2
Flash Point: 22.3 °C
Enthalpy of Vaporization: 28.76 kJ/mol
Boiling Point: 57.3 °C at 760 mmHg
Vapour Pressure: 232 mmHg at 25°C
Melting point: 112-114 °C(lit.)
Storage temp: 2-8°C
Sensitive: Moisture Sensitive
BRN: 3552401
InChI
InChI=1/C4H9NO.ClH/c1-3-6-4(2)5;/h5H,3H2,1-2H3;1H
Smiles
[NH2+]=C(OCC)C.[ClH-]
EINECS: 218-631-7
Product Categories: Amidates/Imidates; Nitrogen Compounds; Organic Building Blocks
Safety Profile
Hazard Codes: 
Xi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36-37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36:Wear suitable protective clothing.
S37/39:Wear suitable gloves and eye/face protection.
WGK Germany: 3
F: 3-10-21
Specification
Ethanimidic acid, ethylester, hydrochloride (1:1) , with CAS number of 2208-07-3, can be called 1-Ethoxyethaniminium chloride ; Ethyl ethanimidoate hydrochloride (1:1) . It is a white to light yellow crystal powder.