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| CAS No.: | 229625-50-7 |
|---|---|
| Name: | PHOSPHORIC ACI DI-T-BUTYL EXTER CHLOROMETHYL ESTER |
| Article Data: | 58 |
| Molecular Structure: | |
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| Formula: | C9H20ClO4P |
| Molecular Weight: | 258.682 |
| Synonyms: | phosphoric acid di-t-butyl ester chloromethyl ester;di-tert-butyl chloromethyl phosphonate;phosphoric acid di-tert-butyl ester chloromethyl ester;Di-tert-butyl chloromethyl phosphate;di-tert-butyl chloromethylene phosphate ester;chloromethyl di-tert-butyl phosphate;Phosphoric acid di-tert-butyl chloromethyl ester; |
| Density: | 1.115±0.06 g/cm3(Predicted) |
| Boiling Point: | 272.9±23.0 °C(Predicted) |
| PSA: | 54.57000 |
| LogP: | 3.93760 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 593-71-5
Chloroiodomethane
- 68695-48-7
di-tert-butyl phosphoric acid tetra-n-butylammonium salt
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| at 20℃; for 4h; Inert atmosphere; | 97% |
| In benzene at 20℃; for 20h; Time; Darkness; | 91% |
| In benzene at 20℃; for 3h; | 49% |
- 49715-04-0
chlorosulfuric acid chloromethyl ester
- 33494-80-3
potassium di-tert-butylphosphate
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| Stage #1: potassium di-tert-butylphosphate With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water at 0℃; for 0.166667h; Stage #2: chlorosulfuric acid chloromethyl ester In dichloromethane; water at 20℃; for 20h; | 95.3% |
| With potassium hydrogenphosphate trihydrate; tert-butyl methyl ether; tetra(n-butyl)ammonium hydrogensulfate In water at 0 - 20℃; for 2.41667h; | 94% |
| With potassium hydrogenphosphate trihydrate; tetra(n-butyl)ammonium hydrogensulfate In tert-butyl methyl ether; water at 0 - 30℃; for 2.41667h; | 94% |
- 49715-04-0
chlorosulfuric acid chloromethyl ester
- 33494-81-4
phosphoric acid di-tert-butyl ester
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| Stage #1: phosphoric acid di-tert-butyl ester With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In water for 0.166667h; Cooling with ice; Stage #2: chlorosulfuric acid chloromethyl ester In dichloromethane; water at 20℃; for 24h; | 89% |
| With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; | 72% |
| Stage #1: phosphoric acid di-tert-butyl ester With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water at 0℃; for 0.166667h; Stage #2: chlorosulfuric acid chloromethyl ester In dichloromethane; water at 20℃; | 72% |
- 49715-04-0
chlorosulfuric acid chloromethyl ester
- 34075-24-6
tetramethylammonium di-tert-butyl hydrogen phosphate
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| Stage #1: tetramethylammonium di-tert-butyl hydrogen phsophate With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In water for 0.166667h; Cooling with ice; Stage #2: chlorosulfuric acid chloromethyl ester In dichloromethane; water at 20℃; for 24h; | 89% |
| Stage #1: tetramethylammonium di-tert-butyl hydrogen phsophate With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In water for 0.166667h; Cooling with ice; Stage #2: chlorosulfuric acid chloromethyl ester In dichloromethane; water at 20℃; for 24h; | 89% |
- 593-71-5
Chloroiodomethane
- 18281-42-0
di-tert-butyl phosphate silver salt
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| In benzene at 20℃; for 18h; | 71% |
| In toluene at 100℃; | 1.8 g |
| In toluene at 100℃; | 1.8 g |
- 593-71-5
Chloroiodomethane
- 33494-81-4
phosphoric acid di-tert-butyl ester
- 13086-84-5
di-tert-butyl phosphite
- 18281-42-0
di-tert-butyl phosphate silver salt
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| silver carbonate In acetonitrile; benzene | 71% |
- 593-71-5
Chloroiodomethane
- 34075-24-6
tetramethylammonium di-tert-butyl hydrogen phosphate
A
- 229625-50-7
di-tert-butyl chloromethyl phosphate
B
- 427899-56-7
bis-di-tert-butyl methyl phosphate
| Conditions | Yield |
|---|---|
| In 1,2-dimethoxyethane at 85℃; for 1.5h; Heating / reflux; | A 63% B n/a |
| In 1,2-dimethoxyethane for 1.5h; Heating; | A 35% B n/a |
- 427899-56-7
bis-di-tert-butyl methyl phosphate
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| With silica gel Chromatography; | 60% |
- 49715-04-0
chlorosulfuric acid chloromethyl ester
- 1623-08-1
phosphoric acid dibenzyl ester
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water | 59% |
- 593-71-5
Chloroiodomethane
- 13086-84-5
di-tert-butyl phosphite
- 7440-44-0
pyrographite
- 34075-24-6
tetramethylammonium di-tert-butyl hydrogen phosphate
- 229625-50-7
di-tert-butyl chloromethyl phosphate
| Conditions | Yield |
|---|---|
| With potassium hydrogencarbonate In potassium permanganate; 1,2-dimethoxyethane; water; acetone |
