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CAS No.: | 2411-36-1 |
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Name: | TRI-N-HEPTYLAMINE |
Article Data: | 8 |
Molecular Structure: | |
Formula: | C21H45 N |
Molecular Weight: | 311.595 |
Synonyms: | Triheptylamine(6CI,7CI,8CI); Tri-n-heptylamine |
Density: | 0.814g/cm3 |
Melting Point: | -43.15°C (estimate) |
Boiling Point: | 332.4°Cat760mmHg |
Flash Point: | 132.1°C |
Appearance: | clear yellow liquid |
Hazard Symbols: | Xi |
Risk Codes: | R36/37/38 |
PSA: | 3.24000 |
LogP: | 7.19960 |
Conditions | Yield |
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With 5-methyl-1,3,4-thiadiazol-2-amine; potassium hydroxide In ethanol; water at 25℃; for 1h; | 90% |
Conditions | Yield |
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With Co2Rh2/C In toluene at 180℃; under 760.051 Torr; for 18h; Autoclave; Inert atmosphere; | 81% |
Multi-step reaction with 2 steps 1: Co2Rh2/C / toluene / 18 h / 180 °C / 760.05 Torr / Autoclave; Inert atmosphere 2: Co2Rh2/C / toluene / 18 h / 180 °C / 760.05 Torr / Autoclave; Inert atmosphere View Scheme |
Conditions | Yield |
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With Co2Rh2/C In toluene at 180℃; under 760.051 Torr; for 18h; Autoclave; Inert atmosphere; | 80% |
Conditions | Yield |
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With ammonium hydroxide; dodecacarbonyl-triangulo-triruthenium; C23H32N2O; hydrogen In tetrahydrofuran; toluene at 120℃; under 37503.8 Torr; for 20h; Autoclave; Inert atmosphere; regioselective reaction; | 73% |
Conditions | Yield |
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With sodium cyanoborohydride; 1,1,1,3,3,3-hexamethyl-disilazane; ytterbium(III) triflate In tetrahydrofuran; acetonitrile at 20℃; for 72h; Inert atmosphere; | 73% |
Conditions | Yield |
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at 200 - 210℃; Hydrogenation; |
Conditions | Yield |
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With nickel at 200 - 210℃; Hydrogenation; |
Conditions | Yield |
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at 160℃; for 4h; Inert atmosphere; | A n/a B 81 %Chromat. |
Conditions | Yield |
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Stage #1: tri-n-heptylamine; ethyl bromoacetate In ethyl acetate at 20℃; for 96h; Stage #2: With water In methanol | 85% |
tri-n-heptylamine
benzamidine monohydrochloride
benzaldehyde
5-pentyl-2,4-diphenylpyrimidine
Conditions | Yield |
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With di-tert-butyl peroxide; iodine In chlorobenzene at 150℃; for 8h; | 65% |
With di-tert-butyl peroxide; iodine In chlorobenzene at 150℃; for 8h; Sealed tube; | 65% |