Detail of "2417-73-4"

CAS Number:
2417-73-4
Name:
Methyl 2-bromomethylbenzoate
Molecular Structure:
Formula:
C₉H₉BrO₂
Molecular Weight:
229.07
Synonyms:
o-Toluicacid, a-bromo-, methyl ester(6CI,7CI,8CI);2-Bromomethylbenzoic acid methyl ester;2-Bromomethylbenzoic methylester;2-Carbomethoxybenzyl bromide;2-Methoxycarbonylbenzylbromide;Methyl o-(bromomethyl)benzoate;Methyla-bromo-o-toluate;o-Carbomethoxybenzyl bromide;
Density:
1.46 g/cm³
Boiling Point:
293.9 °C at 760 mmHg
Flash Point:
131.5 °C

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Reference

Synthesis of isochroman-4-one and its derivatives: Synthesis of isochroman-4-one and its derivatives. (II). Alkylation and Grignard reaction of isochroman-4-one. Li, Mingzhu; Jiang, Guiji; Gao, Yongjun (Dep. Chem., Yanbian Univ., Yanji, Peop. Rep. China). Gaodeng Xuexiao Huaxue Xuebao, 7(8), 692-4 (Chinese) 1986. CODEN: KTHPDM. 2417-73-4 and 20924-56-5 which are cas registry numbers of substances are two of reagents here. ISSN: 0251-0790. DOCUMENT TYPE: Journal CA Section: 27 (Heterocyclic Compounds (One Hetero Atom)) Alkylation of isochromanones I (R1 = H; R2 = Me, Et) with CH2:CHCH2Br, PhCH2Cl, and Me(CH2)4I gave I (R1 = allyl, PhCH2, pentyl) whereas Grignard reaction of 4-isochromanone with CH2:CHCH2MgBr and PhCH2MgCl gave isochromanols II (R3 = allyl, PhCH2). .

Preparation of pyrrole derivatives for treatment of diabetes: Preparation of pyrrole derivatives for treatment of diabetes. Yoshida, Kozo; Maruta, Katsunori; Nagata, Ryu (Sumitomo Pharmaceutical Co., Ltd., Japan). Jpn. Kokai Tokkyo Koho JP 2006036730 A2 9 Feb 2006, 70 pp. (Japanese).Chemical with cas number 2417-73-4 also plays role. (Japan). CODEN: JKXXAF. APPLICATION: JP 2004-222700 30 Jul 2004. DOCUMENT TYPE: Patent CA Section: 28 (Heterocyclic Compounds (More Than One Hetero Atom)) Section cross-reference(s): 1, 27 The title compds. (I) or prodrugs thereof or pharmacol. acceptable salts of either [R2 = one or a plural no. of groups selected from H, each (un)substituted alkyl and aryl, and halogen atoms; Ar1, Ar2, Ar3 = each (un)substituted aryl or heteroaryl; W2 = each (un)substituted lower alkylene or alkenylene, -Y1-W6- (wherein Y1 = O, S, SO, SO2; W6 = each (un)substituted lower alkylene or alkenylene); W2 = a single bond, each (un)substituted lower alkylene or alkenylene, -Y2-W7-, -W7-Y2- (wherein Y2 = O, S, SO, SO2, NR11, CONR11; R11 = H, (un)substituted lower alkyl; W7 = each (un)substituted lower alkylene or alkenylene); W4 = a single bond, (un)substituted lower alkylene, -W8-Y3- (wherein Y3 = O, S, SO, SO2; W8 = each (un)substituted lower alkylene or alkenylene); R1 = H, (un)substituted lower alkyl] are prepd. These compds. activate or regulate peroxisome proliferator-activated receptor a (PPARa), PPARg, or PPARa/g activity and improve insulin resistance and are useful as antidiabetic agents for safely controlling blood sugar. Thus, a soln. of 3-(3-hydroxyphenyl)thiophene-2-carboxylic acid Me ester 243, [1-(2-Hydroxyethyl)-1H-pyrrol-2-yl](4-methylphenyl)methanone 230, Ph3P 288 mg in THF was treated with 500 mg 40% di-Et azocarboxylate/toluene soln. at 0° and stirred at room temp.There are some reagents like 2417-73-4 is used in this study. for 18 h, after workup and silica gel chromatog., 52% 3-[3-[2-[2-(4-methylbenzoyl)-1H-pyrrol-1-yl]ethoxy]phenyl]thiophene-2-ca rboxylic acid Me ester which (230 mg) was dissolved in THF 3, 2 N aq. NaOH soln. 2, and MeOH 3 mL, stirred at 50° for 6 h, cooled to room temp., concd. under reduced pressure, treated with dil. aq. HCl soln., and filtered to give, after washing with water and drying under reduced pressure, 95% 3-[3-[2-[2-(4-methylbenzoyl)-1H-pyrrol-1-yl]ethoxy]phenyl]thiophene-2-ca rboxylic acid (II). II and 5-[3-[(1E)-3-[2-(4-methylbenzoyl)-1H-pyrrol-1-yl]prop-1-en-1-yl]benzyl]-1 ,3-oxazole-4-carboxylic acid at 10 mM showed 26.4- and 38.8-fold increase in activity of PPARa in COS-1 cells, resp., and 7.2- and 7.5-fold increase in activity of PPARg, resp. ..

Detail of "2417-73-4"

Methyl 2-bromomethylbenzoate

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CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

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CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

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CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

CAS No.2417-73-4 Methyl 2-bromomethylbenzoate

Reference