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CAS No.: | 2432-74-8 | ||
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Name: | 6-AMINO CAPRONITRILE | ||
Article Data: | 50 | ||
Molecular Structure: | |||
Formula: | C6H12 N2 | ||
Molecular Weight: | 112.175 | ||
Synonyms: | 6-Aminocapronitrile;6-Aminohexanenitrile; 6-Aminohexanonitrile; NSC 510; e-Aminocapronitrile; w-Aminocapronitrile | ||
Density: | 0.899g/cm3 | ||
Melting Point: | -31.3°C | ||
Boiling Point: | 231.1°Cat760mmHg | ||
Flash Point: | 93.6°C | ||
Safety: |
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PSA: | 49.81000 | ||
LogP: | 1.72938 |
Conditions | Yield |
---|---|
With manganese(IV) oxide; ammonia at 200℃; under 9750.98 Torr; Reagent/catalyst; Temperature; Pressure; | 99% |
With ammonia; silica gel; copper at 360℃; |
2-Trimethylsilanyl-ethanesulfonic acid (5-cyano-pentyl)-amide
1-amino-5-cyanopentane
Conditions | Yield |
---|---|
With cesium fluoride In N,N-dimethyl-formamide at 95℃; for 40h; | 83% |
C12H21N3
A
caprolactam
B
1-amino-5-cyanopentane
C
ethyl 6-aminohexanoate
Conditions | Yield |
---|---|
With water; titanium(IV) oxide In ethanol at 230℃; under 60006 Torr; | A 80% B n/a C n/a |
Conditions | Yield |
---|---|
With Rh/Al2O3; hydrogen In ethanol at 80℃; for 6h; | A 24.4% B 75.6% |
With hydrogen; active elemental iron component In ammonia at 70 - 220℃; under 75007.5 - 300030 Torr; | |
Stage #1: hexanedinitrile With potassium hydroxide; hydrogen; nickel at 50℃; under 15001.5 Torr; Stage #2: With phosphoric acid Purification / work up; |
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel at 169.9℃; under 760 Torr; | 75% |
With nickel-aluminium oxide; ammonia at 120℃; under 102971 - 154457 Torr; Hydrogenation; | |
With cobalt kieselguhr; ammonia at 120℃; under 102971 - 154457 Torr; Hydrogenation; |
1-azido-5-cyano-pentane
1-amino-5-cyanopentane
Conditions | Yield |
---|---|
With sodium tetrahydroborate; cobalt(II) chloride In water at 20℃; for 1h; | 66% |
hexanedinitrile
A
1,6-Hexanediamine
B
1-amino-5-cyanopentane
C
2-iminocyclopentanecarbonitrile
Conditions | Yield |
---|---|
With potassium hydroxide; hydrogen; nickel at 50℃; under 15001.5 Torr; Purification / work up; | A n/a B n/a C 12% |
Conditions | Yield |
---|---|
With thionyl chloride |
hexanedinitrile
A
hexamethylene imine
B
1,6-Hexanediamine
C
1-amino-5-cyanopentane
Conditions | Yield |
---|---|
With hydrogen; aluminum oxide; nickel at 169.9℃; under 760 Torr; Product distribution; varying space velocity of catalysts; | |
With hydrogen; nickel monophosphide; silica gel In ethanol at 199.85℃; under 760 Torr; Product distribution; Further Variations:; Catalysts; | A 16 % Chromat. B 65 % Chromat. C 19 % Chromat. |
With potassium hydroxide; hydrogen; [Ni0.60Mg0.15Al0.25(OH)2](CO32-)0.09(NO3-)0.18 at 79.85℃; under 18751.5 Torr; Product distribution; Further Variations:; Catalysts; Reagents; Temperatures; |
Conditions | Yield |
---|---|
Kochen des Reaktionsprodukts mit Hydrazinhydrat in wss. Aethanol; |