CAS No.2516-33-8,Cyclopropyl carbinol Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	2516-33-8
Name:	Cyclopropyl carbinol
Article Data:	64

Formula:	C₄H₈O
Molecular Weight:	72.1069
Synonyms:	Cyclopropylcarbinyl alcohol;Cyclopropanemethyl alcohol;Cyclopropanemethanol;Cyclopropylmethyl alcohol;Cyclopropylmethanol;1-Cyclopropylmethanol;Cyclopropyl Methanol;
EINECS:	219-735-5
Density:	1.004 g/cm³
Melting Point:	-60 °C
Boiling Point:	124.3 °C at 760 mmHg
Flash Point:	35 °C
Solubility:	miscible with water
Appearance:	Clear colorless liquid
Hazard Symbols:	Xn, Xi, C, F
Risk Codes:	10-22-36-34
Safety:	16-26-36-45-36/37/39
Transport Information:	UN 1987 3/PG 3
PSA:	20.23000
LogP:	0.38870

Synthetic route

: 1759-53-1
cyclopropanecarboxylic acid

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With sodium tetrahydroborate In tert-butyl methyl ether at 0 - 50℃; for 24h;	95%
With lithium aluminium tetrahydride	83%
With lithium aluminium tetrahydride	67%

: (2-methoxy-ethoxymethoxymethyl)-cyclopropane

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With cerium(III) chloride In acetonitrile for 1h; Heating;	95%

: 6228-73-5
Cyclopropancarbamid

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique;	91%

: 1344115-77-0
2-(cyclopropylmethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With rose bengal; triethylamine In ethanol at 25℃; for 12h; Schlenk technique; Irradiation;	90%

: 2868-37-3
methyl cyclopropylcarboxylate

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With sodium In methanol at 45 - 65℃; for 2h; Inert atmosphere; Large scale;	88%
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 1h;	85%
Stage #1: methyl cyclopropylcarboxylate With methanol; aluminum (III) chloride; sodium tetrahydroborate at 2℃; Stage #2: With ammonium chloride In water Temperature; Reagent/catalyst;	74.3%

: (cyclopropylmethyl)trifluoroboron potassium hydride

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With rose bengal; triethylamine In ethanol at 25℃; for 12h; Schlenk technique; Irradiation;	85%

: 5500-21-0
cyclopropropanecarbonitrile

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With formaldehyd; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water; toluene at 90℃;	77%

: 186581-53-3, 908094-01-9
diazomethane

: 107-18-6
allyl alcohol

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
bis(benzonitrile)palladium(II) dichloride In dichloromethane at 0 - 10℃; catalytic cyclopropanation of other unsaturated compounds;	72%
bis(benzonitrile)palladium(II) dichloride In diethyl ether; dichloromethane at 0 - 10℃; for 0.5h;	72%
bis(benzonitrile)palladium(II) dichloride In dichloromethane at 0 - 10℃;	72%
palladium(II) acetylacetonate In diethyl ether at -10℃;	45%
With bis(benzonitrile)palladium(II) dichloride In dichloromethane at 0 - 10℃; Yield given;

: 75-11-6
diiodomethane

: 107-18-6
allyl alcohol

: 2516-33-8
Cyclopropylmethanol

Conditions

Conditions	Yield
With 1,2-dimethoxyethane; zinc In diethyl ether Heating;	67%
With lanthanum; iodine In tetrahydrofuran for 5h;	67%

: 70458-21-8
cyclobutanecarbonyl m-chlorobenzoyl peroxide

A: 627-27-0
homoalylic alcohol

B: 2516-33-8
Cyclopropylmethanol

C: 70458-29-6
3-butenyl m-chlorobenzoate

D: 70458-27-4
cyclobutyl m-chlorobenzoate

E: 70458-28-5
cyclopropylmethyl m-chlorobenzoate

F: 2919-23-5
cyclobutanol

Conditions

Conditions	Yield
With acetic acid; potassium iodide In tetrachloromethane at 26℃; Rate constant; on silica;	A 4.3% B 9.6% C 19.5% D 11.8% E 45.5% F 6.5%
With acetic acid; potassium iodide In neat (no solvent) at 26℃; Rate constant; on silica;
With acetic acid; potassium iodide In chloroform at 55℃; Rate constant;
With acetic acid; potassium iodide In tetrachloromethane at 55℃; Rate constant;

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Chemistry

IUPAC Name:cyclopropylmethanol
Molecular Formula:C₄H₈O
Molecular Weight:72.105720 g/mol
Appearance:clear liquid
Melting Point:-60 °C
Boiling Point:123-124 °C738 mm Hg(lit.)
Flash Point:95 °F
Solubility:water, alcohol
density:0.89 g/mL at 25 °C(lit.)
refractive index:n20/D 1.431(lit.)
storage temp.:Flammables area
Water Solubility:miscible
BRN:1846846
Synonyms of CYCLOPROPYL CARBINOL(2516-33-8):
CPC-OL;CP-CARBINOL;CPMO;CYCLOPROPYL CARBINOL;CYCLOPROPYLMETHANOL;CYCLPOPROPANEMETHANOL;CYCLOPROPANEMETHANOL;(HYDROXYMETHYL)CYCLOPROPANE
Categories of CYCLOPROPYL CARBINOL(2516-33-8):
Cyclopropanes;Simple 3-Membered Ring Compounds;Cycloalkanes

Uses

CYCLOPROPYL CARBINOL(2516-33-8) is used as a reagent for 0rganic synthesis.

Safety Profile

Safety Information of CYCLOPROPYL CARBINOL(2516-33-8):
Hazard Codes:Xn,Xi

Risk Statements:10-22-36-34
10:Flammable
22:Harmful if swallowed
36:Irritating to the eyes
34:Causes burns
Safety Statements:16-26-36-45-36/37/39
16:Keep away from sources of ignition - No smoking
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:Wear suitable protective clothing
45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
36/37/39:Wear suitable protective clothing, gloves and eye/face protection
RIDADR:UN 1987 3/PG 3
WGK Germany:1
RTECS:GZ2212250
Hazard Note:Irritant
HazardClass:3
PackingGroup:III

Specification

First Aid Measures of CYCLOPROPYL CARBINOL(2516-33-8):
Eyes:Immediately flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get medical aid immediately.
Skin:Get medical aid immediately. Immediately flush skin with plenty of water for at least 15 minutes while removing contaminated clothing and shoes.
Ingestion:If victim is conscious and alert, give 2-4 cupfuls of milk or water. Get medical aid immediately. Do NOT induce vomiting. If conscious and alert, rinse mouth and drink 2-4 cupfuls of milk or water.
Inhalation:Get medical aid immediately. Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen.

Storage of CYCLOPROPYL CARBINOL(2516-33-8):
Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container. Flammables-area.